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Estimation of mycelial biomass by determination of the ergosterol content of wood decayed by Coniophora puteana and Fomes fomentarius
1989 - IRG/WP 1415
The mycelial biomass of fungi decomposing wood materials may be estimated by the use of an ergosterol assay technique.ln decay tests, essentially according to EN 113, estimates made by HPLC analyses on wood decayed by Coniophora puteana and Fomes fomentarius show the increase in biomass in the wood blocks. The ergosterol contents were correlated with dry weight loss determinations. Degradation of ...
K Nilsson, J Bjurman


Determination of the amine to copper ratio remaining in wood after leaching
2002 - IRG/WP 02-30285
The effectiveness of the protection and the environmental impact of the treated wood are two of the most important aspects that need to be understood for all preservatives. Both are particularly influenced by the loss of biocidal components from treated wood. For amine copper preservatives, copper fixation determines the leaching resistance of the copper and amine compounds formed in wood. Previou...
N Lucas, J N R Ruddick


Computerized axial tomography. A non-destructive method for three-dimensional wood density/moisture content measurement
1987 - IRG/WP 2285
Computerized Axial Tomography (CAT-scanning) - used for medical investigations of the brain - has been evaluated as a nondestructive method of three-dimensional wood density/moisture content measurements. Density can be measured with an accuracy of ±3 kg/m³, and the accuracy in average moisture content is ±1% below and above fibre saturation point. It is theoretically possible that measurements...
L O Lindgren


Optimisation of an analytical method for the determination of total fluoride in preservative-contaminated soils using water steam distillation and an ion-selective electrode
1999 - IRG/WP 99-20153
This paper describes a simple modified procedure for the quantitative fluoride determination of different origin in a soil matrix using a water steam distillation and an ion-selective electrode. Distillation methods generally require a preliminary preparation step like fusing. The modified method presented here is based on the direct distillation of fluoride so that no further sample preparation i...
E Melcher


The quantitative determination of N-cyclohexyl-diazeniumdioxide (HDO) containing compounds in treated wood using TD-GC-MS
2001 - IRG/WP 01-20223
Last year we presented the paper (IRG/WP/00-20201) "Determination of N-cyclohexyl-diazeniumdioxide (HDO) containing compounds in treated wood using GC-MS". Based on the intensive discussion at the meeting, the first experiences made with the calibration of the system for this application will be reported. For the quantitative determination of N-cyclohexyl-diazeniumdioxide in treated wood, milled m...
P Jüngel, J Wittenzellner, E Melcher


The accelerated L-joint test method for determination of the out of ground natural durability
1998 - IRG/WP 98-20146
The accelerated L-joint test incorporates a moistening device and uses a close end water trap in an open joint connection with a laminated tenon member consisting of the perishable reference wood species scots pine sapwood and beech. After one year of exposure it is possible to show a distinct identification of natural durability classes 4 and 5 against the more durable wood species. Both weight ...
J Van Acker, C Brauwers, M Stevens


Investigation of CCA fixation in wood by sequential extraction. I Determination of CCA component fixation and preliminary extraction results
2002 - IRG/WP 02-50188
The fixation of CCA-C preservative was investigated in sapwood of red pine (Pinus resinosa Ait.), trembling aspen (Populus tremuloides Michx.) and red maple (Populus tremuloides Michx.) at target retentions of 4.0, 6.4, 9.6 and 30.0 kg/m3. Treated wood sawdust was water extracted at close time intervals during the fixation and analyzed for the contents of unfixed hexavalent chromium, total Cr, Cu ...
S Radivojevic, P A Cooper


Determination of corrosive effect of liquid wood preservatives to metals – First experiences with a National Standard which is in revision
2006 - IRG/WP 06-20321
The development of standards is an essential tool to characterise different kind of materials and products. An important aspect during the development of a new product is to check the corrosion behaviour with other materials. Corrosion can cause several problems like pitting corrosion. Consequently the knowledge concerning the corrosive effect of liquid wood preservatives is important due to the s...
E Melcher


Determination of fungitoxic value of preservatives in laboratory wood-block tests. Part 2: Statistical estimation
1989 - IRG/WP 2327
Laboratory modified agar-block tests were made to determine the fungitoxic value of the wood preservative CCA against the test fungus Serpula lacrymans using statistical methods. With the aid of statistical computer programmes based on the least square method. the regression equation was found for the dependence between sample mass loss and preservative retention both in terms of percentage and fo...
J Wazny, J D Thornton, K J Krajewski


Determination of fungitoxic value of preservatives in laboratory wood-block tests. Part 1: Standard procedures
1989 - IRG/WP 2326
By applying a modified agar-block method, a comparative analysis was made on the toxic value of the wood preservative CCA against the test fungus Serpula lacrymans. The procedure applied to determine the results accounted for different standards: EN (Toxic limit), ASTM (threshold retention), GOST (threshold retention and protection probability), PN (toxic doses) and JIS (value of efficiency). Desp...
J Wazny, J D Thornton


Inter-laboratory comparison of assessment methods for wood preservatives against subterranean termites: Determination of protection threshold limits for CCA
1999 - IRG/WP 99-10317
In 1996, several institutes conducted laboratory bioassays on the efficacy of unleached Pinus radiata specimens treated with copper-chromium-arsenic (CCA) and copper naphthenate (Cu Naph) at retentions of 0.5, 1.0, 2.0 and 4.0 kg/m3 (total salt for CCA; elemental copper for Cu Naph) against a range of species of subterranean termites (IRG/WP/96-10174). Each participant employed the standard test m...
J W Creffield, M Lenz


Determination of toxicity data for preservatives against Basidiomycetes by measuring the reduction in compression strength of wood
1988 - IRG/WP 2297
Blocks of Pinus radiata D. Don were treated to 12 retention levels with CCA and NaPCP. These were exposed for 12 weeks in agar jars to the dry rot (brown rot) Serpula lacrymans (Schum. ex Fr.) S.F. Gray. After mass loss determination, the same blocks were tested for reduction in compression strength parallel to the grain. Using both these parameters, together with interpolated 6 week strength loss...
J Wazny, J D Thornton


The use of low cost X-ray fluorescence instruments in the determination of copper chromium and arsenic in preservative treated wood
1987 - IRG/WP 2278
Internal quality control in timber treatment plants can be pursued by analysis of preservative treatment solutions and treated timber. Treaters must proceed with costly and lengthy analyses through analytical laboratories. An alternative approach for the timber treater, is to use low cost analysers (L.C.A.'s) based upon x-ray fluorescence. Detailed comparisons have been made between stand...
J Norton, L E Leightley


Determination of thermal degradation of isothiazolone treated wood
1997 - IRG/WP 97-30154
Wood treated with 4,5-dichloro-2-n-octyl-4-isothiazolin-3-one was the subject of thermal degradation study. The study included burning isothiazolone treated wood under various temperatures with and without oxygen. The result showed that no harmful combustion products, such as polychlorinated dibenzo-p-dioxins, polychlorinated dibenzo-p-furans and polychlorinated biphenyls, were detected. These fin...
Bing Yu


A determination of the toxic level of ACQ2100 wood preservative for the powder post borer Lyctus brunneus (Stephens)
1994 - IRG/WP 94-20029
The sapwood of two Lyctus susceptible Australian hardwoods, messmate (Eucalyptus obliqua L'Herit.) and black bean (Castanospermum australe A. Cunn. et Fraser ex Hook) were pressure impregnated with ACQ2100, a wood preservative, to produce replicates of a range of retentions. Preservative retentions were determined by solution weight uptake at treatment and chemical analyses of selected sa...
A R Moffat


Quantitative Determination of Cyproconazole in Wood treated with Tanalith CY
2007 - IRG/WP 07-20369
The HPLC method has been widely applied to quantitative determination of cyproconazole in preservative solutions. However, HPLC assay has not been successfully employed to determine cyproconazole content in treated wood. Some extractives from treated wood hinder cyproconazole determination because they have a similar retention time to that of cyproconazole on an HPLC chromatogram. In addition, ...
I Momohara, T Miyauchi, M Mori


Determination of a fixation time of wood preservatives: A discussion paper
2010 - IRG/WP 10-20436
The intention of that paper is to initiate a discussion on the basis of a French method in combination with a German approach regarding the need of a method for the determination of a fixation time and especially to obtain input as well as ideas concerning a possible test design. Since no harmonised European approach exists up to now concerning the determination of a fixation time, CEN TC 38 (2009...
E Raphalen, E Melcher


Service life prediction of wooden components – Part 1: Determination of dose-response functions for above ground decay
2010 - IRG/WP 10-20439
Scots pine sapwood (Pinus sylvestris L.) and Douglas fir heartwood (Pseudotsuga menziesii Franco) specimens were exposed in double layer field trials at 24 different European test sites under different exposure conditions (in total 28 test sets). The material climate in terms of wood moisture content (MC) and wood temperature was automatically recorded over a period of up to eight years and compar...
C Brischke, A O Rapp


Determination of Equilibrium Moisture Content (EMC) of wood in the neighboring Countries of Iran
2011 - IRG/WP 10-40540
The mean value of annual temperature and relative humidity of 33 cities in Azerbaijan, Armenia, Turkmenistan, Afghanistan, Pakistan, Oman, United Arab Emirates, Bahrain, Qatar, Kuwait, Iraq and Turkey were determined using climatic data of the past 11 years. The EMC values were calculated using the Hailwood-Horrobin sorption model and its annual fluctuation, together with Temperature and relati...
A A Enayati, H Z Hosseinabadi


Determination of Izod Impact Strength on Wood: A Suitable Method to Detect Fungal Decay in Protective Effectiveness-Screenings of Wood Preservatives
2012 - IRG/WP 12-20484
For testing a large number of different substances regarding fungicide properties, the reduction of the decay test duration is advantageous. In the present paper the suitability of a method for testing plastics using an impact testing machine was examined. The results clearly show that the fungal attack of European beech by the white-rot fungus Trametes versicolor leads to a decrease of izod imp...
H Delenk, M Zauer, A Wagenführ


Determination of the natural durability of solid wood against wood-destroying fungi - a European round-robin test
2013 - IRG/WP 13-20511
In Europe the durability of wood against wood-destroying basidiomycetes is tested according to CEN/TS 15083-1 (2005). Hitherto existing experience with this standard is quite heterogeneous and results from previous round-robin tests have stayed unreported or have been reported incompletely. In particular the need for natural pre-weathering of the test specimens to allow potential detoxification of...
C Brischke, C R Welzbacher, A Gellerich, S Bollmus, M Humar, K Plaschkies, W Scheiding, G Alfredsen, J Van Acker, I De Windt


Developing Analytical Methods for Determination of Quaternary Ammonium Compounds (DDAC) using HPLC and HPLC-MS (Application to treating solution and preservatives treated wood)
2013 - IRG/WP 13-20516
Korea preservative treating industry has mainly used alkaline copper quaternary (ACQ) expected over 80% of market share in Korea. ACQ employs dodecyl dimethyl ammonium chloride (DDAC) and benzyl dimethyl dodecyl ammonium chloride (DBAC) for active ingredient along with copper. The strongly increasing domestic applications for wood preservatives require developing accurate and reproducible analytic...
Sung-Mo Kang, Kwon-Min Kim, Won-Mo Koo, Myeong-Won Cho


Extraction and analysis of DNA from green and seasoned timber as basic methods for determination of wood species and origin
2013 - IRG/WP 13-20523
Against the background of the European timber trade regulation EUTR, commenced to law by March 2013, the determination of wood species and tracing of its origin is getting a great importance. A promising approach for establishing fast and reliable tracking systems for wood products is DNA analysis. A critical point is the extraction of analysable DNA from the wood and its lignified cell walls. Thu...
K Jacobs, H Mende, W Scheiding


Assessment of Scots pine sapwood susceptibility to moulds by determination of fungi growth and ergosterol content in infested wood
2014 - IRG/WP 14-20540
The susceptibility of wood to filamentous fungi (mould) attack is determine mainly by laboratory methods with descriptive grading of fungal growth on the surface of the wood specimens. It is a lot of different grading scale of fungi growth, but determination of the size of fungi growth is many times not easy, not clear and often difficult. Although the filamentous fungi are not included to microor...
A Fojutowski, A Koziróg, A Kropacz


The anatomical determination of wood samples found in the “Fürstengräber” from Lübsow (Poland)
2018 - IRG/WP 18-10930
The paper presents the results of anatomical research identifying three wooden fragments from the “Princes Graves” (“Fürstengräber”) in Lübsow, Poland. The research demonstrates that the wooden fragments are typical of wood harvested from European forests. The physicals conclusions are important for the research of Jan Schuster, from the University of Lodz, Institute of Archeology, Pol...
J Schuster, W Unger, T L Woods


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