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Determination of N-cyclohexyl-diazeniumdioxide (HDO) containing compounds in treated wood using GC-MS
2000 - IRG/WP 00-20201
Beside the biological effectiveness the approval of a chemical wood preservative requires also techniques for the analytical determination of active ingredients in different matrices. Fulfilling of the last requirement is particularly difficult in the case of impregnated timber treated with wood preservatives containing organic compounds. This paper describes a procedure for the determination of t...
P Jüngel, J Wittenzellner, E Melcher


Need to develop processing technologies (for value addition) of the species evaluated for their properties and uses
2005 - IRG/WP 05-40307
The demand of timber in India for different industrial as well as domestic applications is ever increasing mostly due to urbanization and industrialization. This demand can only be met either from the imported timber or from the plantation resources outside the reserved and natural forests. There are a number of timber species grown under plantation forestry have their heartwood refractory to any ...
S R Shukla, S K Sharma, Y M Dubey, P Kumar, R V Rao, K S Shashidhar


Investigation of the suitability of silver fir (Abies alba Mill.) for thermal modification
2004 - IRG/WP 04-40275
In this study the suitability of silver fir (Abies alba Mill.) was examined for thermal modification. Comparative experimental investigations were performed with silver fir and Norway spruce (Picea abies Karst.) after thermal treatments. Besides properties, which characterize the quality of heat treatments, like dimensional stability and resistance against fungal attack, strength properties of the...
C Brischke, A O Rapp


Durability aspects of (hydro)thermal treated wood
2000 - IRG/WP 00-40160
Samples of several wood species were treated in a two steps process, subsequently hydrothermal and dry heat-treated, by the so-called PLATO-process and analysed for their resistance against fungal attack. Both PLATO-treated and dry heat-treated specimen were prepared and analysed, in order to study the influence of moisture during hydrothermal treatment of wood. The resistance against all of the s...
B F Tjeerdsma, M Stevens, H Militz


The identification of organic compounds in wood using thermal desorption GC-MS - possibilities and limitations
2001 - IRG/WP 01-20224
There is a clear need for the analytical characterisation and identification of organic compounds and their derivatives in different phases especially in timber. In this context the paper describes a rapid and powerful gas chromatographic method for the determination of insecticides, biocides and "other" organic substances in treated and/or modified wood. The main advantage of this procedure is th...
P Jüngel, E Melcher


Influences of the hydro-thermal treatment on physical properties of beech wood (Fagus orientalis)
2005 - IRG/WP 05-40303
Influences of the hydro-thermal treatment on physical properties of beech wood were studied. Wood specimens (2×2×2cm) were treated in two steps. At first step, samples were treated at 160,180 & 200ºC for 4, 5 & 6 hours. At second step, treated samples were cured based on their first step treatment temperatures (160,180 & 200ºC) for 16 hours. The treated samples were soaked in water...
B Mohebby, I Sanaei


Thermal modification of non-durable wood species 2. Improved wood properties of thermal treated wood
1998 - IRG/WP 98-40124
Properties of wood treated in a new heat-treatment process called the PLATO-process have been studied. Several wood species have been treated using this new thermal modification process using a range of process conditions (mainly time and temperature). In this study the characteristics of the treated wood were determined using samples from whole planks treated on pilot plant scale. The modified ch...
B F Tjeerdsma, M J Boonstra, H Militz


Make ready of a detection system for insect attack by acoustical method
1996 - IRG/WP 96-10183
A contract CRAFT of European research allowed to build a detector prototype able to diagnose on site the presence of Hylotrupes bajulus and termites, even during the first stages of infestation when no sign of activity is visible. Based on non destructive control technics, the device picks up the acoustical waves emitted by the insects in the wood fibers. The amplification and the filtering of the...
M Hyvernaud, F Wiest, M-M Serment, M Angulo, O Winkel


Ammoniacal wood preservatives for use in non-pressure treatment of spruce and aspen poplar. Part 2
1984 - IRG/WP 3274
A series of thermal diffusion treatments were carried out on unseasoned white spruce (Picea glauca (Moench) Voss) lumber and air dry aspen poplar (Populus tremuloides Michx.) timbers using an ammoniacal copper arsenate wood preservative. Under the specific conditions described, certain charges of lumber met the present Canadian Standards Association Wood Preservation Committee's requireme...
C D Ralph, J K Shields


The quantitative determination of N-cyclohexyl-diazeniumdioxide (HDO) containing compounds in treated wood using TD-GC-MS
2001 - IRG/WP 01-20223
Last year we presented the paper (IRG/WP/00-20201) "Determination of N-cyclohexyl-diazeniumdioxide (HDO) containing compounds in treated wood using GC-MS". Based on the intensive discussion at the meeting, the first experiences made with the calibration of the system for this application will be reported. For the quantitative determination of N-cyclohexyl-diazeniumdioxide in treated wood, milled m...
P Jüngel, J Wittenzellner, E Melcher


Comparison of thermally modified wood originating from four industrial scale processes – durability
2002 - IRG/WP 02-40229
This study examined the differences in biological wood properties of heat treated wood originating from four different European industrial heat treatment plants. The manufacturers of heat treated material were: PLATO Hout B.V./Netherlands, Thermo Wood/Finland, New Option Wood/France and Menz Holz/Germany where Oil-Heat treated Wood (OHT) is produced. The results of miniblock tests with basidiomyc...
C R Welzbacher, A O Rapp


Determination of bis-(N-cyclohexyl-diazeniumdioxy)-copper in different matrices by photometer, thermal energy analyzer and HPLC
1999 - IRG/WP 99-20179
For the quantitative analysis of bis (N-cyclohexyl-diazeniumdioxy)-copper (Cu-HDO) three analytical methods are used. The employment of the different methods depends on the matrices involved. For several years now, the colorimetric determination of Cu-HDO by photometer has been applied to solutions and concentrates of wood preservatives. In principle, the technique consists of a quantitative conve...
J Wittenzellner, W Hettler, M Maier


Effect of post-treatment processing on leachability of ACZA-treated douglas-fir lumber
1998 - IRG/WP 98-50109
The effect of post-treatment procedures that more rapidly precipitate copper, zinc, and arsenic in douglas-fir treated with ammoniacal copper zinc arsenate (ACZA) on subsequent leaching resistance were investigated at two retentions (6.4 and 40 kg/m3). Total leaching was greater from boards treated to the higher retention. At both levels, copper was lost at the highest rate. Post-treatment process...
J J Morrell, C S Love, S Kumar, C M Freitag


Environmental characterisation of retification process by-products (liquid and gaseous wastes)
2005 - IRG/WP 05-50224-10
In order to reduce environmental risks during the service life of the treated wood and to find new alternative developments on the durability of wood, some research and technology development have been made on thermal treatment. The retification process is one of these processes. The retification process induces chemical modification of the lignin and cellulosic components and modifies the intrins...
G Labat, E Bucket, S Legay, C Yriex, P Marchal, E Raphalen, M Vernois, R Guyonnet, H Besset, E Fredon), G Vilarem, L Rigal, C Raynaud


Characteristics of thermally modified wood in vacuum
2004 - IRG/WP 04-40287
In commercial thermal wood modification processes nitrogen, steam or oil has been used for the reduction of oxygen content in the reactor atmosphere. In present study no special heating medium, but an initial vacuuming step has been used for this purpose. Mass loss, resistance to fungal decay, dimensional stability, bending strength and modulus of elasticity of heat treated wood were evaluated and...
G Rep, F Pohleven, B Bucar


Wood injurers found at wood processing plants in SR Sloveni
1981 - IRG/WP 1140
This report describes the stating of damages on wood and taking stock of wood injurers found in the warehouses of wood processing plants in SR Slovenia. The results of this research show that in the process of manufacture vast quantities of spruce-wood, pine-wood, beech wood, oak-wood, and poplar-wood are exposed to numerous injurers, both fungi and insects. The reasons for such a state lie in con...
R Benko


PCP in aquatic environments arising from historic contamination at wood processing and preservation sites
1995 - IRG/WP 95-50040-14
Three different studies are reported that assess the impacts of Pentachlorophenol (PCP) in aquatic environments arising from its historic use at sawmilling and wood preservation sites. These studies involved New Zealand wood processing facilities, and collectively they aimed to measure the transport of PCP from sawmill sites into the aquatic environment, determine the background environmental conc...
J S Gifford, P N McFarlane, M C Judd, S M Anderson


CCA removal from treated wood by chemical, mechanical and microbial processing
1998 - IRG/WP 98-50101-26
Most preservative-treated wood produced and consumed in the U.S. is treated with toxic inorganic compounds containing copper, chromium, and arsenic. Because chromated copper arsenate (CCA) is fixed to the wood, treated wood has not been considered toxic or hazardous and is currently landfilled. Increasing public concern about environmental contamination from treated wood combined with increasing q...
C A Clausen, R L Smith


Determination of thermal degradation of isothiazolone treated wood
1997 - IRG/WP 97-30154
Wood treated with 4,5-dichloro-2-n-octyl-4-isothiazolin-3-one was the subject of thermal degradation study. The study included burning isothiazolone treated wood under various temperatures with and without oxygen. The result showed that no harmful combustion products, such as polychlorinated dibenzo-p-dioxins, polychlorinated dibenzo-p-furans and polychlorinated biphenyls, were detected. These fin...
Bing Yu


High-energy multiple impact (HEMI)-test – Part 2: A mechanical test for the detection of fungal decay
2006 - IRG/WP 06-20339
The suitability of the high-energy multiple impact (HEMI)-test for detection of early fungal decay was examined. The HEMI – test characterizes the treatment quality of thermally modified wood by stressing the treated material by thousands of impacts of pounding steel balls. This method differentiates between heat treatment intensities, which are expressed by structural changes of the wood. Simil...
C R Welzbacher, C Brischke, A O Rapp


High-energy multiple impact (HEMI)-test – Part 1: A new tool for quality control of thermally modified timber
2006 - IRG/WP 06-20346
Thermal modification processes improve durability and dimensional stability of wood, but the strength properties, especially the dynamic ones, are compromised and need to be considered with respect to industrial quality control. Results from standard dynamic strength testing, such as impact bending tests, suffer from high variability, and therefore require a high number of replicates. To overcome ...
C Brischke, A O Rapp, C R Welzbacher


The commercialisation of ThermoWood® products
2006 - IRG/WP 06-40339
The concept of thermally modifying timber is well established, which has achieved a limited market breakthrough to date. Commercial application has mainly occurred within Finland, though recent years has seen market gain in several other European countries. This paper reviews the known properties of ThermoWood® timber, based on the combined work of the Finnish ThermoWood® Association, alongside ...
D Jones, E Suttie, J Ala-Viikari, N Bergstrom, D Mayes


The Effect of Flavonoids on Colour and Spectral Changes of the Wood Surface Caused by Heat Treatment or Ultra-violet Irradiation
2006 - IRG/WP 06-40341
Both heat treatment and UV irradiation can cause discolouration and change in the spectral properties of wood surface. Some of the characteristic flavonols have significant role on colour and spectral changes, despite of their relative small quantities in wood. Colour changes and spectral properties of natural and extracted black locust (Robinia pseudoacacia L.) and poplar (Populus nigra L.) were...
R Csonka-Rákosa, L Molnár-Hamvas, E Börcsök, J Molnár, K Németh


Thermal decomposition behavior of CCA-treated wood for safe disposal and the safe recovery of heavy metals through pyrolysis
2006 - IRG/WP 06-50238
If we could estimate the chemical changes in heavy metals by temperature in chromated copper arsenate (CCA)-treated wood during pyrolysis, it is expected that we could solve the environmental problems of heavy metals, which may occur during pyrolysis, and therefore, the thermal decomposition behavior of effective elements of CCA-treated wood was examined to find a safe disposal method. First, CCA-...
Dong Won Son, Dong-heub Lee, Sun-hae Cheon, Myung Jae Lee


Photo-degradation of modified and non-modified wood, coated with water borne acrylic coatings during artificial light exposure
2007 - IRG/WP 07-30416
A series of experiments were carried out to investigate photo-degradation of thermally modified (at 210oC and – 0.9 bars for two hours) and non-modified spruce wood (Picea abies L (Karst)), coated with transparent and semitransparent (with 3% pigment content) acrylic coatings during artificial UV light irradiation for 200 hours. Photo-degradation was evaluated in terms of colour changes througho...
M Deka, M Tomažic, M Petric


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