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Preventive effectiveness of petrol derivatives against blue-stain fungi
1992 - IRG/WP 92-3716
A possible application of fractions obtained on petrol pyrolysis is their use as a wood preservative against wood-decay and sap-stain fungi. From two of these fractions were prepared three different products (ST, STL and SST). The aim of this work has been the possibility of utilizing these products in the treatment of wood used for external joinery, determining their effectiveness against blue-stain fungi and their compatibility with existing surface coatings. Test blocks of Pinus sylvestris and Pinus pinaster were used, treated with a brushed application of the above products, and then two different kinds of coating. The wood blocks were then exposed to 3 months of weathering. After this time they were placed in contact with pure cultures of Pullularia pullulans and Sclerophoma pityophila in sterile conditions, for 6 weeks. After the period of weathering the degree of varnish adherance was evaluated. The effectiveness of the preservatives was assesed by determining the penetration depth of the hypha into the wood face. The results obtained revealed that only ST and SST were effective against blue-stain fungi for wood in service, whereas the degree of compatibility with the coatings varied.
A M Navarrete, M T De Troya, E Sanchez, A Guijarro

Comparative study of blue stain resistance of various types of wood stains after artificial and natural weathering
1992 - IRG/WP 92-2411
For the determination of the protective effectiveness of a preservative treatment against blue stain in service, artificial weathering has been proposed as an alternative for the natural weathering period of 6 months in the European standard EN 152. Research on a range of products and on complete finishing systems for external joinery was conducted during 1986-1990. It revealed that the decisions drawn after 4 weeks Xenontest do not always confirm those of the EN 152 natural weathering test. Results were influenced by the nature of the formulation, the resin binder and the product combination (treatment system). However the variation among the ageing methods generally does not effect the practical conclusions on the blue stain resistance when well-defined limits are considered.
J Van Acker, M Stevens, M Nys

EN 152: Is this Standard Relevant for today’s Wood Preservatives? A Critical Review.
2006 - IRG/WP 06-20331
The paper critically reviews the Blue stain test method described in EN 152 including possible test variables. Whereas EN 152 has been successfully used for solvent borne wood preservatives, it appears that the methodology is not suited for modern water borne products, where the majority fail. The paper will show that there exist different quality claims not concordant with EN 599-1 within different European countries. This contradicts the requirement for unification in Europe, especially with the implementation of the Biocidal Products Directive. It is further shown, that water based products and other product systems not passing the EN 152-1 can be successfully used and evaluated according to EN 927-3 and other practical exposure trials. The main conclusion of this review is that EN 152 is not reflecting the practical performance of water borne wood preservatives. The standard should be used only to assess the blue stain barrier in wood and not fungal surface growth. It is proposed that EN 927 testing replaces EN152 concerning surface growth assessment
B Jensen, F Imsgard, J Larsen

Comité International Permanent pour la Recherche sur la Préservation des Matériaux en Milieu Marin. Information from the Wood Group
1980 - IRG/WP 460
E G B Jones

Insect resistance of preservative treated tropical plywood against Lyctus
1990 - IRG/WP 1453
Seven plywood types composed of tropical wood species, vulnerable to Lyctus, were treated with various commercial water-borne and oil-borne preservatives. A wide range of preservative retentions was obtained by treating boards with dip treatment, steeping, double-vacuum and vacuum-pressure impregnations. Selected samples were subsequently tested for their insect resistance against Lyctus africanus during 6 to 8 months according to European Standard EN 20. All control samples were attacked, except one Obeche plywood exhibiting only 50% attack. Water-borne preservative solutions containing arsenic, boron or fluoride could not prevent attack at common retention levels for interior use e.g. lower than 5 kg/m³. Quaternary ammonium compounds showed no insecticidal efficiency, up to 3 kg/m³. TCMTB at 1.5-1.7 kg/m³ proved to be able to reduce slightly the susceptibility for insect attack. Organic insecticides gave the best results, with nearly no attack for plywood treated with lindane or cypermethrin. In spite of a preservative uptake of 25 to 30 kg/m³, endosulfan only could reduce attack by 50%. Protection by permethrin at 0.1% a.i. required a retention of 28 kg/m³. Besides the fact that variability in wood species and composition of the plywood are leading to different retention levels, variation in penetration and distribution of a.i., and as a consequence to a different insect resistance of the impregnated boards, some poor results were directly related to inadequate insecticidal activity and/or concentration of a.i. in some commercial formulations for Lyctus control.
J Van Acker, M Stevens, M Pallaske

Studies on accelerated ageing procedures with TBTO-treated wood
1985 - IRG/WP 2244
The efficacy of various procedures for accelerated ageing of organotin based wood preservatives in treated wood has been investigated. It was found that leaching of the treated wood samples in water according to the European Standard EN 84 was not satisfactory for organotin based preservatives and is probably also unsuitable even for other types of organic solvent preservatives. Keeping tributyltin oxide (TBTO) treated samples in a heating cabinet at 70°C for five weeks, however, had a considerable effect on the breakdown of TBTO and the subsequent decay test. Therefore, an ageing procedure involving a heating period should be considered for all organic solvent wood preservatives. The investigation also confirmed that elevated temperatures accelerate the degradation of TBTO and that there is a strong correlation between the percentage of TBTO in the wood and its resistance against decay.
J Jermer, M-L Edlund, B Henningsson, W Hintze

Interspecific variability of European oak durability against white rot fungi (Coriolus versicolor): Comparison between sessile oak and peduncle oak (Quercus petraea and Quercus robur)
2001 - IRG/WP 01-10393
The knowledge of wood natural durability against biologic predators enable its external use. The resistance of European oak wood was reported like durable according to the EN 350-2. However, some individuals may contain high durable wood. Our research was focused to understand this variability in oak population that represent the first french species (4.1 millions of ha). Natural durability of European oak heartwood (Quercus petraea and Quercus robur) against white rot fungi (Coriolus versicolor) was tested according to european standard EN 113. The experimental material consists in 23 oaks robur and 26 petraea oaks sampled from 9 French regions. For each tree, 3 twin samples were taken off from heartwood situated at 1.30 m from the bottom of the tree. Different effects were tested by hierarchic variance analysis: "species", "forest within species" and "tree within forest". The tree effect is very significant for biologic natural resistance. Variability between species was also demonstrated. Although the species effect is significant, it's relatively weak compared with tree differences (it was declared significant 5%). Durability classification was determined according European standard EN 350-1. 69.2% of petraea oak trees are classified as high durable, 19.2% durable, 7.7% moderately durable and 3.8% slightly durable. In the case of robur oak 91.3% of trees are classified as high durable and 8.7% durable.
N Ayadi, B Charrier, M Irmouli, J P Charpentier, C J Allemand, F Feuillat, R Keller

Temperature influence on the growing velocity and cellulolytic activities of Poria placenta strains from several locations
1986 - IRG/WP 2263
The differences observed on the FPRL 280 Poria Placenta strain at several Research European Laboratories for determining up the fungicide effectiveness of wood preservative has carry us to do a comparative study about the cellulolytic activity and growth velocity of each of this strains at different temperatures (22, 24 and 28°C). The results show significative differences when the temperature is changed.
A M Navarrete, M T De Troya

Working Group I 'Biological Problems' Sub-group 'Insects in dry wood (other than termites)', Scope of work
1976 - IRG/WP 152
S Cymorek

Possibility of use of wood species per class of biological risks. Attempt to determine criteria based on Pr EN 350-1/2/3
1992 - IRG/WP 92-2409
M Rayzal

Depletion of boron and copper from CCB treated test specimens using different leaching protocols
2004 - IRG/WP 04-50208
The objective of this study was to measure the depletion of inorganic wood preservative components regarding the proposed OECD guideline "Estimation of emissions from preservative-treated wood to the environment: laboratory method for wooden commodities exposed in the use class 4 and 5" as part of the project "Investigations concerning the influence of test parameters on the release of biocidal actives from treated timber in leaching tests". Pine sapwood specimens (50x10x150) were pressure impregnated with CCB according to European Use Class 4. Before leaching all samples were stores 4 weeks for fixation. In addition leaching tests were performed according to the European Standard EN 84 by means of EN 113 blocks. Parallel investigations were carried out between two laboratories to assess the repeatability and comparability of the methods. The results of chemical analysis of leachates taken at different time intervals show that similar depletion rates were determined for copper and boron independent on the leaching protocol used. However, the loss of copper as well as chromium in short term dipping experiments was often lower than the detection limit. Furthermore it can be stated that the difference between parallels was higher for the results which were obtained for the OECD guideline that EN 84. A comparison of both laboratory results indicate that a quite good repeatability is given in case of the CCB treated material.
E Melcher, R-D Peek, U Schoknecht, R Wegner

Resistance of the wood of Eucalyptus saligna and Paulownia tomentosa against some wood rotting fungi
1997 - IRG/WP 97-10238
Paulownia tomentosa and Eucalyptus saligna are not autochthonous species in Slovenia and we determined the resistance of their wood against our most common wood rotting fungi. The resistance against Coniophora puteana, Gloeophyllum trabeum and Trametes versicolor was determined according to EN 113 and compared to the resistance of beech (Fagus sylvatica) wood. It was stated, that both paulownia and eucalypt wood samples are much more resistant than beech wood. Especially paulownia wood was outstanding by its natural resistance against tested basidiomycetes.
F Pohleven, M Petric

Determination of the preventive efficacy against wood destroying basidiomycetes fungi, EN V 839 - CEN/TC 38 WG 9
1993 - IRG/WP 93-20015
The WG 9 of CEN TC/38 has presented to EC a mycological test to assess efficacy of preservatives applied by surface process. This method is now an experimental standard (EN V 839) which has to be approved by the different european delegations. The following paper is not the standard as it has been proposed but is a presentation of the principle of the method. The experimental standard specifies a laboratory method of test which gives a basis of the assessment of the preventive action of a wood preservative when applied as a surface treatment against Basidiomycetes fungi. This method is applicable to formulations of preservatives in a ready to use form (organic formulations, organic water-dispersible formulations, water-soluble materials). Series of susceptible wood species specimens are treated on longitudinal faces whith the preservative in test using brushing as surface procedure. Test specimens are then exposed by an intermediate mesh to feeder blocks infestedby pure culture of Basidiomycetes fungi in sterile conditions and penetration of fungi is assessed on cross section sawn in the samples at the end of the test.
D Dirol

Tebuconazole, a new wood-preserving fungicide
1990 - IRG/WP 3634
TEBUCONAZOLE, an anti-fungal triazole compound, has been tested to assess the effectivness as wood preserving fungicide. Tests were made with the active ingredient and also in formulations against basidiomycetes, blue-staining fungi and mould. Results of the DESOWAG laboratories and also from official institutes will be presented. In addition to this there were made different toxicological and ecotoxicological trials according to OECD and EPA guidelines
B Wüstenhöfer, H-W Wegen, W Metzner

Rapport sur l'activité du CEN/TC 38
1983 - IRG/WP 2204
M Pottevin

CEN Draft Standard (38 N 460F): Méthode d'essai pour determiner l'efficacité d'un produit de préservation du bois en milieu marin
1986 - IRG/WP 4132 F
G Castan

Rapport sur l'activité du Comité CEN/TC 38 "Méthodes d'essais des produits de préservation des bois" du Comité Européen de Normalisation (CEN)
1986 - IRG/WP 2266
G Castan

Proposals for collaborative work on laboratory soft rot testing
1986 - IRG/WP 2265
Proposals for collaborative experiments based on soil burial are presented. It is intended to study the use of defined horticultural loams with a view to obtaining more reproducability in laboratory soft rot tests.
D J Dickinson, S M Gray

A comparison of the effectiveness of a vacuum oven and a wind tunnel in the accelerated ageing of treated wood by evaporation
1989 - IRG/WP 2334
R J Orsler, G E Holland

Report of field test results for dichloro-n-octyl-isothiazolone: A potential new wood preservative
1988 - IRG/WP 3495
In a previous report (IRG/WP/3306) we presented preliminary laboratory test results on 4,5-dichloro-2-n-octyl-4-isothiazolone (RH 287). Laboratory data indicated toxic threshold values for RH 287 ranging from 0.37 to 0.50 kg/m³. In this report we present field test results on an IRG L-joint test and an in-ground stake test for RH 287, pentachlorophenol and biocide free test units. (a) L-joint test: After 39 months exposure (Starkville MS.) units pressure treated with 0.05 kg/m³ RH 287 rated 9.7 out of 10. Units dip treated in a 0.5% ai solution of RH 287 rated 10 out of 10. Biocide free controls exposed in the same series rated 5.3 out of 10 after 39 months (b) Stake test: After 48 months exposure in two southern US test plots stakes treated with neat RH 287 in toluene at 4.6 kg/m³ rated between 8.6 to 8.8 out of 10 for decay and 9.1 to 9.8 out of 10 for termite attack. Biocide free control stakes rated O out of 10 for decay and 1.1 to 4.8 out of 10 for termite attack after 48 months. RH 287 continues to show promise as a potential new wood preservative. Results to date were obtained in samples treated with neat RH 287, Formulation of RH 287 into treatment systems specifically designed for above ground or ground contact applications should only improve the already excellent activity seen with RH 287.
D E Greenley, B M Hegarty

Climate indices at work: Above ground decay L-joint tests (EN 330 and AWPA E9) at two sites 12000 km apart and with Scheffer climate indices of 60-65 and 300-330
1996 - IRG/WP 96-20095
Matched sets of Scots pine sapwood (Pinus sylvestris) L-joints were exposed above ground at two field sites for approximately five years. One site, at Garston, Watford, UK has a climate index between 60 and 65 while the other, close to Hilo, HI, USA has an index between 300 and 330. The joints were treated with a range of organic solvent treatments applied either by three minute dip immersion or by double vacuum. Untreated joints were installed at each site as control material. All samples were assessed at approximately annual intervals at both sites. After five years, decay at the Hilo site is well advanced with failure apparent in many joints, both untreated and treated. As would be expected given the climatic differences, decay at the Garston site has progressed more slowly than in Hilo. Differentiation in treatment performance was apparent after one year's exposure in Hilo with similar differentiation becoming apparent after five years' exposure in Garston. This acceleration correlates well with the difference in Climate Index for the two sites as calculated using the Scheffer method. Encouragingly, the performance ranking of the different treatments at the two sites was very similar. The results of this test suggest that the concept of using high decay hazard sites for field testing of treated wood products for use in above ground situations can provide meaningful results in a short period, and may offer a timely and realistic alternative to relative preservative testing to that achieved in laboratory test regimes. The results also show that above ground field testing at both of the sites included provide valuable information on preservative performance, and this information is likely to provide a greater degree of realism than is possible using pure culture laboratory test procedures.
A F Preston, K J Archer, D M Roberts, J K Carey, A F Bravery

A natural exposure weathering test for the evaluation of preservative performance
1992 - IRG/WP 92-2400
Natural exposure weathering tests were carried out by externally exposing treated wood samples for varying periodes of time up to 36 months. In the laboratory these samples were assayed for residual preservative effeciveness using Coniophora puteana FPRL 11E. The results indicated a loss in efficacy over and above that determined using artificial ageing procedures such as EN73 (evaporative ageing) and EN84 (water leaching). Results for two TBT based preservatives indicated a gradual loss in efficacy. Results for the organic biocide 2-thiocyanomethyl-thio benzothiazole (TCMTB) gave a more rapid loss in effeciveness indicative of the high levels of microbial actifity present in the samples. This test provides an intermediate evaluation of preservative performance and permanence between artificial laboratory ageing procedures and the necessary field evaluation using an L-joint type test.
J Brown, G R Williams

Bibliographie sur les produits organiques en solvant pour la préservation du bois
1971 - IRG/WP 38
H Alliot

Checking of sodium pentachlorophenate fixation in wood
1990 - IRG/WP 3620
In order to estimate the volatilization of sodium pentachlorophenate from treated wood, wood samples treated with pentachlorophenate were analysed after various durations of an EN 73 weathering The results giving no clear evidence of volatilization, treated wood samples were put in a test chamber with precise climatic conditions, the air used in the experiment being analysed. The pentachlorophenate content in air was quantified: 1.8 µg/m³
M Lamour, H Sageot

Final proposals for collaborative work on laboratory soft rot testing
1987 - IRG/WP 2292
In this paper proposals are made to scope, timbers, preservatives, leaching, drying, soil type, moisture content, soil burial (blocks and stakes), incubation and dry weight determination and the expression of results.
D J Dickinson, S M Gray

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