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CCA removal from treated wood by chemical, mechanical and microbial processing
1998 - IRG/WP 98-50101-26
Most preservative-treated wood produced and consumed in the U.S. is treated with toxic inorganic compounds containing copper, chromium, and arsenic. Because chromated copper arsenate (CCA) is fixed to the wood, treated wood has not been considered toxic or hazardous and is currently landfilled. Increasing public concern about environmental contamination from treated wood combined with increasing q...
C A Clausen, R L Smith


Strength loss associated with steam conditioning and boron treatment of radiata pine framing
1987 - IRG/WP 3438
The combined effect of included defects and wood moisture content on the strength loss of second rotation radiata pine framing following conventional steam conditioning is investigated. The green Modulus of Elasticity (MOE) is reduced by approximately 13% after steaming. When dried after steaming, however, neither the MOE nor MOR is significantly different from unsteamed dried controls....
M J Collins, P Vinden


Borate thermal treatments
1992 - IRG/WP 92-3715
Green, partially seasoned (air-dried, steam conditioned), or kiln-dried southern pine timbers were treated thermally using 15% disodiumoctaborate tetrahydrate solution. After treatment, sections were stored under non-drying conditions to allow for diffusion. Results showed that effective treatment meeting the AWPA minimum retention (0.17 B203 pcf [2.72 kg/m³] in the outer inch) and penetration (2...
H M Barnes, R W Landers, L H Williams


Options for accelerated boron treatment: A practical review of alternatives
1985 - IRG/WP 3329
Boron wood preservatives are almost exclusively applied by momentary immersion and block diffusion storage. Alternative techniques are described which can be used to accelerate boron treatment. Diffusion coefficients have been derived to define the acceleration of diffusion with increasing temperature. Schedules are described for pressure impregnation of green timber, involving steam conditioning,...
P Vinden, T Fenton, K Nasheri


The effect of treatment method on CCA efficacy in Corsican pine
1992 - IRG/WP 92-3723
As part of a study into the influence of application method on preservative efficacy Corsican pine (Pinus nigra) samples (50 x 50 x 400 mm³) were treated with a CCA formulation using Bethel, Steam/Bethel or Lowry processes. Full penetration of the preservative at a gross level was confirmed using a copper disclosing reagent. The preservative was allowed to fix and then samples were converted into...
P R Newman, R J Murphy


Steam conditioning of partially dried radiata and Corsican pine roundwood
1988 - IRG/WP 3499
The effect of partial air drying prior to steam conditioning and its effect on subsequent preservative treatment by the Bethell treatment process was investigated. A high standard of preservative treatment was obtained in both radiata and Corsican pine, irrespective of whether a period of partial drying was imposed before or after steam conditioning....
P Vinden, D R Page, K Nasheri


Effects of pretreatments for the amelioration of preservative impregnability using the Oscillating pressure method (OPM)
1995 - IRG/WP 95-40044
For the purpose of an amelioration of preservative impregnability, three types of pretreatment: the steaming, the explosion and the boiling, were tested. The specimens were prepared by the domestic four species: Itajii, Ryukyumatsu, Sugi and Hinoki, and 1 refractry imported species: Douglas-fir. The dimension of specimens was 20 x 20 x 300 mm³ and were treated with CCA in a laboratory OPM machine...
K Suzuki, I Asaoka, S Tani, K Okada, T Hidaka


Copper naphthenate-treated Southern Pine pole stubs in field exposure. -Part 2: Chemical characterization of full size pole stubs 12 years after treatment
2000 - IRG/WP 00-30246
This study examines the influence of pre-treatment and post-treatment steaming on the character and physio-chemical nature of copper naphthenate in hydrocarbon solvent treated pine in larger, pole diameter, pole stub-length samples. This work is the continuation of two projects that began almost a decade ago. Previous reports indicated that certain morphological changes might occur in small labora...
H M Barnes, D P Kamdem, M H Freeman


The effect of steam conditioning on Southern yellow pine treated with copper naphthenate
1997 - IRG/WP 97-40086
The current study was undertaken to investigate the influence of steam conditioning on Southern yellow pine treated with copper naphthenate (Cu-N). Pre-steamed and /or kiln-dried Southern yellow pine were pressure treated with Cu-N. After treatment, one group of samples were post-steamed. It was found that samples changed color from green to dark-brown after post-steaming. To elucidate the effect ...
Jun Zhang, D P Kamdem, M H Freeman, R D Arsenault


Determination of total fluoride in preservative-treated wood by ion selective electrode, without steam distillation
1996 - IRG/WP 96-20086
An analytical method was developed to determine total fluoride in wood treated with aqueous fluoride or borate-fluoride formulations. Ground wood was mixed with 60% sodium hydroxide solution and oven-dried overnight before furnacing at 600°C. The cool fused product was dissolved in warm water before adding a powerful complexant/buffer solution containing sulphosalicylic acid and EDTA. Fluoride wa...
M J Kennedy


Attractive factors of steam-treated larch wood to termite feeding
1998 - IRG/WP 98-10256
The hot water extractives from steam-treated Japanese larch wood were studied to understand the chemical properties of attractive factors of the treated wood to feeding behavior of a subterranean termite, Coptotermes formosanus. Hot water extractives were fractionated and analyzed using chromatography, gel filtration, and NMR methods. The stimulants yielded by the steam treatment were comprised o...
S Doi, Y Kurimoto, W Ohmura, M Aoyama, S Ohara


Protection of rubberwood with modified creosote
1998 - IRG/WP 98-30165
Creosote is a renowned wood preservative but has certain disadvantages like obnoxius odour and colour, with its unpaintability and bleeding from wood surface may create environmental hazards. An effort has been made to isolate chemical fractions from creosote to obtain clean odourless preservative formulations by subjecting to steam distillation (SVC). Rubberwood treated with SVC and tested for it...
H C Nagaveni, H S Ananthapadmanabha, G Vijayalakshmi, M N Sharma, K H Shankaranarayana


Determination of total fluoride and boron in preservative-treated wood fluoride by ion selective electrode without steam distillation, and boron colorimetrically using azornethine-h
1998 - IRG/WP 98-20135
An analytical method was developed to determine total fluoride and boron in wood treated with aqueous or solid diffusing fluoride or borate-fluoride formulations. Ground wood was mixed with 30% sodium hydroxide solution and oven-dried for 2 hours before furnacing at 600° C for 1 hour. The cool fused product was dissolved in hot water, transferred to a plastic beaker and neutralised. Fluoride was ...
P A Collins, M J Kennedy


Copper naphthenate-treated Southern Pine pole stubs in field exposure: - Part 1: Gradient & biodeterioration analysis 12 years after treatment
2000 - IRG/WP 00-30242
Naphthenates have been used for the preservation of timber and cellulose since their original identification in Russia in the early 1880's as part of a series of petroleum characterizations. Later work in the development of copper naphthenate as a heavy-duty preservative for poles led to the development of various treating cycles similar to other oil-borne systems. Recent work concerning ...
H M Barnes, M H Freeman


Steam/hold/APM boron treatment - Treatability trials with green gauged radiata pine
1987 - IRG/WP 3439
Freshly sawn 100 x 50 mm radiata pine was green gauged, steam conditioned and preservative treated with a mixture of borax and boric acid using a modified Alternating Pressure Method (APM) treatment schedule. A 12 hour holding period between steam conditioning and treatment resulted in the necessary moisture loss and moisture re-distribution to facilitate treatment to NZ Timber Preservation Author...
P Vinden


Treatment application method and CCA efficacy in Corsican pine - Assessment by serial exposure and soil burial tests
1993 - IRG/WP 93-40006
A previous report on this research (Newman and Murphy, 1992) identified possible variation in the efficacy of a CCA preservative applied to Corsican pine (Pinus nigra var. maritima) dependant upon the treatment application method (Bethel, Lowry or Steam/Bethel). This paper presents further data from biological testing of CCA treated Corsican pine using serial exposure and unsterile soil techniques...
P R Newman, R J Murphy


Acceleration of boric acid uptake into the subterranean termite, Coptotermes formosanus Shiraki using steamed larch wood
2000 - IRG/WP 00-10353
Laboratory tests were done to measure the efficacy of addition of steamed larch (Larix leptolepis (Sieb. et Zucc.) Gord.) heartwood extracts for the uptake of boric acid against the termite, Coptotermes formosanus Shiraki. Paper discs were treated with the water-soluble fraction obtained from hot-water extracts of steamed larch wood (S-Water) with or without 0.01-2.0% boric acid, followed by expos...
W Ohmura, S Doi, S Ohara


Fundamentals on steam fixation of chromated wood preservatives
1988 - IRG/WP 3483
Weathering of treated wood directly after impregnation leaches up to 2% of copper-chromate-containing wood preservatives. Almost total fixation of Cr+6 is achieved by steaming the treated wood at 100°C to 120°C, preferably 110°C. To initiate such spontaneous fixation 85°C to 90°C inside the wood are essential, which requires heating times ranging from 20 to 80 min, depending on timber species...
R-D Peek, H Willeitner


Accelerated diffusion treatment of sawn Sitka spruce grown in the UK
1986 - IRG/WP 3395
The treatment of 'green' sapwood and heartwood of Sitka spruce by diffusion methods was investigated. Steam/dip treatment processes gave increased solution uptakes and depths of penetration of copper in comparison with a simple dip treatment. Further investigation is required to reduce diffusion gradients with copper based formulations and to improve the penetration of '...
R J Murphy, D J Dickinson


Optimisation of an analytical method for the determination of total fluoride in preservative-contaminated soils using water steam distillation and an ion-selective electrode
1999 - IRG/WP 99-20153
This paper describes a simple modified procedure for the quantitative fluoride determination of different origin in a soil matrix using a water steam distillation and an ion-selective electrode. Distillation methods generally require a preliminary preparation step like fusing. The modified method presented here is based on the direct distillation of fluoride so that no further sample preparation i...
E Melcher


Biological resistance of steam-compressed wood pretreated with boric compounds
1999 - IRG/WP 99-30190
Wood compression under heating is aimed to enhance dimensional stability and surface hardness. Preservative treatment with an appropriate chemical is additionally required for the protection of wood against biological agents under hazardous service conditions. Boron pretreatment of compressed wood was targeted to a mutual benefit of increasing biological resistance of compressed wood as boron was ...
M K Yalinkilic, W Dwianto, Y Imamura, K Tsunoda, M Takahashi


Less pollution due to technical approaches on accelerated steam fixation of chromated wood preservatives
1988 - IRG/WP 3487
Steaming of freshly treated wood at 100°C to 120°C initiates a spontaneous fixation of copper-chromate-containing wood preservatives. For the performance, a suitable anticorrosive equipment is necessary. Good results can be achieved using a separate steaming equipment which allows a rapid heating of the wood. While warming-up, in the wood some preservative solution extends and can be partly extr...
H Willeitner, R-D Peek


Underwater shock treatment for improvement of penetration of wood
2006 - IRG/WP 06-40325
Many of conifers including Beimatsu (Pseudotsuga menziesii Franco; Dougras fir, Oregon pine), Akamatsu (Pinus densiflora Sieb. et Zucc.; Japanese red pine), Dafurica Karamatsu (Larix gmelinii Gordon; Dahurica larch) and Karamatsu (Larix leptolepis GORDON; Japanese larch) generally contains the high moisture content. Although subjected to the drying process, it is difficult to be dried up completel...
S Itoh, H Maehara, K Tanaka, T Echigo, K Morioka, E Shirai, K Nishimoto


Effect of steam on fixation of Cu-amine preservative treated wood
2008 - IRG/WP 08-50251
The rates of copper fixation in copper amine preservative treated wood were investigated with different fixation conditions (20° with drying and 50° without drying) and post-steaming. We also measured the degree of leaching for other biocide components (azoles, quatz, and Cu-HDO). Treatments conditioned at 20° with drying required 50 days or more to fix in woods. While copper was stabilized i...
Sung-Mo Kang, In-Yong Hwang, Suk-Kuwon Kim


Direct estimation of the durability of high-pressure steam modified wood by ESR-spectroscopy
2010 - IRG/WP 10-40508
Heat generated persistent free radicals have been detected by electron spin resonance measurement of thermally modified wood, prepared by high pressure superheated steam treatment. The specific density of these radicals have been correlated with the durability against basidiomycetes, as measured by the European standard EN113 test. In the lower range of specific radical densities, the found correl...
W Willems, A Tausch, H Militz


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