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Austrian field test method for anti-sapstain chemicals
1994 - IRG/WP 94-20020
Although Austria is a small country, the annual consumption of anti-sapstain products ranks to approximately 500 tons annually. In 1994, only three products will be approved by the Austrian Wood Preservation Committee (AWPEC). There is demand for a field test method, which demonstrates the efficacy of an anti-sapstain product and consequently implies the acceptance and approval of product by the AWPEC. Present field test was carried out in 1992 and 1993. The results were evaluated after six months storage of test stacks. A TCMTB based product was used as a reference. The results show that the AFPRL method proves very suitable for the simulation of practical situation in Austrian treatment plants, where pine and/or spruce are treated periodically and where different methods of stack storage are applied.
R Gründlinger, M Brandstätter, H Melzer, O Janotta

Progress report on co-operative research project on L-joint testing
1983 - IRG/WP 2192
A F Bravery, D J Dickinson, M Fougerousse

A comparison of soft rot, white rot and brown rot in CCA, CCP, CCF, CCB, TCMTB and benzalkonium chloride treated Pinus radiata IUFRO stakes, after 9-15 years exposure at five test sites in New Zealand
1991 - IRG/WP 1485
The aim of this study was to determine if decay type varies significantly between five field trial test sites of different soil type, aspect and climate in 9-15 year old, replicate CCA, CCF, CCP. CCB, TCMTB and AAC treated IUFRO stakes. A visual on-site assessment of decay type on every test stake was made and observations confirmed by microscopical examination. Regression analyses were used to determine significant differences of percentage frequency of occurrence of each rot type between sites and preservatives. Large differences in percentage frequency of occurrence of rot type were evident between sites. One site was dominated by brown rot (85%) and two were dominated by soft rot (99 and 91%). The fourth site had intermediate proportions of brown rot (40%) and soft rot (71%) but had the second highest occurrence of white rot (32%) (highest = 37%; lowest = 11%). The fifth site was distinct in that a large proportion of stakes (69%) had both well established brown rot and soft rot. Stakes at the other four sites tended to have only one rot type. Some highly significant preservative effects were also found. Possible causes of these differences are discussed in terms of inter-site soil type, climate and other differences.
R N Wakeling

Wood preservatives: Field tests out of ground contact. Brief survey of principles and methodology
1976 - IRG/WP 269
This paper contains the following spots: 1.: The general need for field tests. 2.: Interests and limits of field tests in ground contact. 3.: Various methods in use for out-of-ground contact field tests. 4.: Fungal cellar tests are they an alternative to above-ground decay exposure tests? 5.: Conclusions.
M Fougerousse

Field test evaluation of preservatives and treatment methods for fence posts
1985 - IRG/WP 3347
This work presents the field test results after fifteen years exposure of Eucalyptus saligna fence posts treated with six different preservatives and five treatment methods. All the combinations with oil-borne preservatives presented the best results and among the waterborne preservatives, the fence posts treated by immersion method were with the lowest performance in the field test.
G A C Lopez, E S Lepage

A rapid field bioassay technique with subterranean termites
1983 - IRG/WP 1188
Details are summarised of a field procedure which is designed to ensure continuous exposure to a replenishing termite biomass. After pre-baiting to determine the presence and identification of a termite hazard, test specimens (35 x 35 x 250 mm³) are installed vertically in the ground adjacent to and in contact with bait specimens of the same dimensions and interconnected by susceptible feeder strip.
C D Howick, J W Creffield

Performance of treated fence posts after 6 years in five test plots in the State of Sao Paulo - Brazil
1976 - IRG/WP 376
Fence posts treated with creosote, pentachlorophenol and creosote/ pentachlorophenol mixtures showed good performance after 6 years of exposure in five test plots located in the State of Sao Paulo - Brazil. Good results were also achieved with copper sulphate/sodium arsenate and copper sulphate/potassium dichromate mixtures. Fungi and termites were the main destroying agents found attacking the posts.
M S Cavalcante

Protocol for evaluation and approving new wood preservative
1985 - IRG/WP 2159
M E Hedley, J A Butcher

Trials on the field control of the Formosan subterranean termite with Amdro® bait
1982 - IRG/WP 1163
Amdro® - treated paper towels were introduced into two field colonies of the Formosan subterranean termite in Hawaii. At the concentration of 180 ppm, the toxicant bait was ineffective one month after the introduction. At higher concentrations (> 6,400 ppm), the baits were eaten initially; however, one week after introduction, termites avoided or covered the baits. The 15,000 ppm baits supressed the activity of one colony but did not affect the other.
N-Y Su, M Tamashiro, J R Yates III

Results of stake tests on wood preservatives (Progress report to 1974)
1975 - IRG/WP 361
A number of field stake trials on preservative-treated wood have been carried out at Princes Risborough Laboratory from 1928 to the present day, and many of the tests still continue. This paper presents in detail the results obtained to date, covering about 15 000 individual test stakes exposed over the period.
D F Purslow

Field tests out of ground contact in France: Definition of the test procedure and preliminary results after 18 months
1981 - IRG/WP 2161
M Fougerousse

Effect of a penta emulsion on the service life of Douglas fir, heartwood posts
1978 - IRG/WP 3112
C S Walters

Wood furfurylation process and properties of furfurylated wood
2004 - IRG/WP 04-40289
The first processes for “furfurylation” of wood (wood modification with furfuryl alcohol) were developed several decades ago. Furfuryl alcohol is a renewable chemical since it is derived from furfural, which is produced from hydrolysed biomass waste. Over the last decade modernised processes for furfurylation of wood have been developed. These new processes are based on new catalytic systems and process additives. Two main processes for production of furfurylated wood have been developed for WPT (Wood Polymer Technology ASA) by the authors – Kebony 100 for high modification levels of hardwoods and VisorWood for lower modification levels of pine. Commercial production according to the Kebony process has been running since August 2000, mainly for flooring. A small Kebony production plant is now in operation in Lithuania. A larger Kebony/VisorWood production plant started up in September 2003 in Porsgrunn, Norway. Several new plants operating according to the VisorWood process, each with an annual capacity of 10 000 m³ or more, are under construction. The properties of furfurylated wood depend on the retention of grafted/polymerised furfuryl alcohol (PFA) in the wood. At high modification levels (high retention of PFA) the enhancement of a wide variety of properties are achieved: an exceptional hardness increase, exceptional resistance to microbial decay and insect attack, high resistance to chemical degradation, increase in MOR & MOE, and high dimensional stability. At lower modification levels many property enhancements also occur, however to slightly lower extent. Notable are resistance to microbial decay and insect attack, increase in MOR & MOE, and relatively high dimensional stability.
M Westin, S Lande, M Schneider

Durability of pine modified by 9 different methods
2004 - IRG/WP 04-40288
The decay resistance was studied for pine modified by nine methods of wood modification: 1) Acetylation, 2) Treatment with methylated melamine resin (MMF), 3) Acetylation followed by post-treatment with MMF-resin, 4) Thermal modification, 5) Furfurylation, 6) Maleoylation (using water solution of MG or ethanol solution of maleic anhydride), 7) Succinylation, 8) NMA-modification and 9) modification with reactive linseed oil derivative (UZA), Wood blocks of Scots pine (Pinus sylvestris L.) sapwood were modified in pilot plants. Methods 1-5 were performed by the authors at Chalmers University of Technology or at BFH in Hamburg. Methods 5-9 were part of a European research project (the Chemowood project, FAIR-CT97-3187) and therefore each of these modifications was performed by the project participant responsible for the method. For laboratory testing in TMCs (modified European standard ENV 807) and pure basidiomycete culture bioassays, smaller test specimens were cut from the modified wood blocks. Most of the modification methods were applied on test specimens for marine field testing (EN 275) and some methods to produce mini-stakes for field tests in five Swedish fields. Some modification methods result in modified wood with poor durability, whereas other methods (acetylation, furfurylation and MMF-treatment) seem to provide excellent resistance to microbial decay.
M Westin, A O Rapp, T Nilsson

In-ground performance of two formulations of chlorothalonil after five years of exposure at three test sites in Australia
1996 - IRG/WP 96-30101
Sapwood specimens of Pinus radiata D. Don and Eucalyptus regnans F. Muell. were each treated to three retentions of each of two preservative formulations (chlorothalonil in oil; chlorothalonil plus chlorpyrifos in oil) and installed in-ground at three field test sites in Australia. Specimens were treated with each formulation to achieve 3.2, 6.4 and 12.8 kg/m³ of chlorothalonil a.i. and 3.2 + 0.2, 6.4 + 0.4 and 12.8 + 0.8 kg/m³ of chlorothalonil plus chlorpyrifos a.i. For comparison, specimens of each timber species, treated to a commercial in-ground retention of a copper-chromium-arsenic (CCA) formulation, were also installed. Treated specimens (including controls) have been rated for their condition annually for attack by subterranean termites and fungal decay using a scale ranging from 4 (sound) down to 0 (failed). After five years of exposure, mean termite and decay scores for replicate test specimens at each site reveal that the performance of all three retentions of each formulation, particularly the two highest retentions, is comparable to CCA.
J W Creffield, T L Woods, N Chew

In search of alternative antisapstain chemicals for use in Papua New Guinea
1988 - IRG/WP 3472
The paper presents results of antisapstain field trials from three locations in Papua New Guinea as part of the Research Centre's programme to find suitable antisapstains to replace the hazardous sodium pentachlorophenate. Effectiveness of seven tested chemicals varied between indigenous pines (Araucaria cunninghamii, Araucaria husteinii) and white coloured hardwoods (Alstonia scholaris, Pterocymbium beccarii) but not between sites. The indigenous pines required lower chemical concentration for same level and period of protection than white coloured hardwoods like amberoi and white cheesewood. Period of protection ranged from four weeks to a maximum of 16 weeks depending on chemical concentration and species of timber. Potential chemicals recommended for use as antisapstain include Celbrite T, Busan 1009, Penacide and Woodguard E.S. and Woodguard E.C.
A Oteng-Amoako

Quantitative assessment of the condition of field specimens
1981 - IRG/WP 2154
Suggestions for a discussion on the desirability of an extension to the existing procedure of assessment of the condition of field specimens by adding more objective, reproducible methods in order to obtain earlier and more specific information than at present on the effect of biological attack on strength and other properties of the specimens as well as the time aspect.
H Friis-Hansen

Short-term field test method with accelerated infection of Basidiomycetes in wood
1981 - IRG/WP 2155
In the ŠIPAD - IRC Wood Protection Laboratory an attempt has been made to develop a simple short-term method for field testing out-of-ground contact wood using accelerated infections with Basidiomycetes. This method makes it possible to obtain a preliminary assessment of a preservative's quality and to estimate the possibility of achieving promising results in more expensive long-term tests. The idea was to use water traps (reservoirs) and 50 x 25 x 15 mm³ laboratory infected pine blocks as the substrate to improve the possibility of inoculation of L-joints.
N Vidovic

What information can we glean from field testing
1995 - IRG/WP 95-20057
To mathematically compare the performance of preservatives in a field test, equations were formulated to describe the relation between log score and time and between rate of decay and retention. By combining these equations, a model was derived for the performance of a number of waterborne preservatives. Some relations between the estimated parameters for different preservatives were noted and these were used to develop a universal model to encompass a variety of patterns of deterioration. An attempt was then made to relate these common parameters to the factors known to affect preservative performance. As a result it may be possible to distinguish and quantify parameters specific to the efficacy of the preservative, the aggressiveness of the test site and the characteristics of the wood substrate.
P I Morris, S Rae

Preservative treatment of Eucalyptus saligna fence posts by the double-diffusion method
1982 - IRG/WP 3196
Eucalyptus saligna fence posts treated by the double-diffusion method with two chemical combinations showed average lives of 11.2 years (copper sulphate and potassium dichromate at 10.5 kg/m³ retention)and of 14.3 years (copper sulphate and sodium mono-H arsenate at 7.1 kg/m³ retention), as determined in five test sites in the State of Sao Paulo, Brazil. The exponential model was the best fit when expressing average life by the Decay Index (DI) as a function of time.
E S Lepage, A R De Freitas

Termite and decay protection - A superficial barrier field test
1983 - IRG/WP 3257
Samples of Pinus radiata were given a superficial barrier treatment and installed in the ground at two sites for five years to observe termite and fungal attack. The three best treatments of the series were Denso petroleum tape, Koppers hot dip tar enamel, and Arquad 2C/75 alkyl ammonium compound. As new fungicides and insecticides become available they are being added to the test using the same system of treatment and exposure.
R S Johnstone, W D Gardner

Soil blocks versus field test for evaluating and standardizing wood preservatives: A commercial view
1994 - IRG/WP 94-20024
On the basis of technical considerations, experience, costs and applicability, the author concludes that the soil block test and other laboratory tests have little meaning in a wood preservative standardization process and almost no merit in the commercialization of a wood preservative system. Field tests at sites known to be aggressive to preservative treated wood are strongly recommended.
W S McNamara

IRG test of preservative-treated hardwoods with particular reference to soft rot. Report on condition of specimens installed in Victoria, Australia
1982 - IRG/WP 3207
J Beesley

Update on lab and field test results for polymeric alkylphenol polysulfide treated wood
2002 - IRG/WP 02-40240
The possibility of using Polymeric Alkylphenol Polysulfide (PXTS) as a wood preservative has been undergoing evaluation in our laboratories for the past four years. Various formulations prepared from this compound have been tested and found to be effective against wood decay fungi and insects in field stakes after 42 months exposure. In accelerated soil bed tests, PXTS has been shown to be considerably more effective than creosote against both soft-rot and basidiomycete decay fungi. PXTS has also been shown to be effective against marine organisms and after 18 months exposure appears to have about the same efficacy as creosote. Preliminary treatment trials indicate that southern pine can be readily treated by the empty cell process
J Goswami, A Abramson, R Buff, D D Nicholas, T Schultz

Factors affecting leaching of preservatives in practice
1978 - IRG/WP 3113
At the 7th Meeting of the IRG in Poland in May 1975, the findings of collaborative laboratory leaching techniques were discussed, and the dangers inherent in using such results to predict the behaviour of preservative-treated components in service were emphasised. In order to improve our understanding of the factors governing leaching of preservatives in practice, and to identify areas where further research is required, it was agreed that a literature review should be prepared. This is presented below. Some points may be made regarding its format and content. First, the review shows that a large number of factors are of importance, including the properties of the wood, the leach water, the preservative and method of application and the nature of the environment to which the product is exposed. In many situations these factors interact and it is clearly impossible within the scope of this short paper to discuss all aspects of the problem in detail. However, the compilation of references will give ready access to the literature on particular topics. For ease of collation, the findings are discussed under a number of different headings. Secondly, less than one-third of the references cited deal with the results of service or field trials, while the others describe laboratory experiments designed to provide comparative data. The reservations expressed above concerning such small-scale experiments must be borne in mind when considering the validity of these findings. The information available on this topic up till 1964 was comprehensively reviewed by Wallace who identified and commented upon many of the factors discussed below. Her paper contained discussion on the performance of individual preservatives and on the mechanism of their fixation within the wood. These topics will not be considered here in any detail except insofar as they reflect general trends.
R Cockcroft, R A Laidlaw

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