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Permeability measurements on surface layers for detecting wood with abnormally high permeability
1988 - IRG/WP 2298
Wet storage of timber during the warm period of the year may lead to an increased permeability of the wood, an undesirable phenomenon for several wood industries and also for many end-uses. Neither before nor after drying, such wood with "wet storage damage" can be visually distinguished from wood with a normal permeability. A non-destructive method for inspecting the permeability of surface layers has been tested and has proved to be useful for detection of damage to timber due to wet storage. The principle of the method is that air from a compressor is pressed into the wood via a nozzle and that the air flow and/or pressure decrease is recorded. A large air flow or a large pressure decrease indicates high permeability.
J B Boutelje, G Hägglund

Aspects of diffusion of boron through wood
1984 - IRG/WP 3298
Boron compounds have been shown to be toxic to a wide range of wood destroying insects and fungi. They are cheap, have low mammalian toxicity and their application in the treatment of wood does not demand specialized equipment. These attributes make them specially attractive to developing countries. Currently, however, little is known about the mechanism of diffusion of boron through wood. Effective treatment with boron preservatives requires good understanding of how the preservatives diffuse through wood. This paper presents a research proposal with the overall objective of determining the relative importance of structural wood components in determining diffusion rates.
S Iddi

Comparison of cubic and plug samples for preparation and data assembly in permeability study
2000 - IRG/WP 00-20197
In order to determine if plug experimental samples (PES: 30 x 15 mm2 diameter) could be used for inspection of wood permeability characteristics, radial and longitudinal flow directions were prepared according to either PES or cubic experimental samples (CES: 100 x 20 x 20 mm3) from the sapwood zone of Sitka spruce and treated by tanalith-C according to full-cell process. Results from the two preparation techniques agreed in the test to determine the mean percentage of void volume filled by liquid both radially and longitudinally, while the preparation process (i.e. machining, sealing, etc.) of the experimental samples and the period of the data collection was quite longer in CES than that for PES in either flow direction.
I Usta

New technique to analyze impregnation processes
1988 - IRG/WP 2304
Equipment has been developed to measure liquid flow in wood during impregnation processes. Basic principles of flow measurements using directly heated negative temperature coefficient thermistors, and some characteristics of the hardware developed are presented in this paper.
J P Hösli

Health aspects concerning the use of bifluorides in wood
1981 - IRG/WP 3173
An attempt has been made to find a correlation between the quantities F¯ and HF present among other ions in an 'Improsol' solution consisting of NH4F.HF and KF.HF, the quantity absorbed by the wood from this after immersion and the toxicological effects of this treated wood when it is used in rooms destined for the residence of people or animals or for the storage of foodstuffs.
H F M Nijman

A review of the configuration of bordered pits to stimulate the fluid flow
2005 - IRG/WP 05-40315
As the bordered pits have generally been thought to have an influence on the refractory nature of softwoods, structural behaviour of this conducting pathways is discussed according to the published literature. Various theories on the role of bordered pits to axial flow are expounded in respect to preservative treatment. Pit aspiration is also reviewed.
I Usta

Borate thermal treatments
1992 - IRG/WP 92-3715
Green, partially seasoned (air-dried, steam conditioned), or kiln-dried southern pine timbers were treated thermally using 15% disodiumoctaborate tetrahydrate solution. After treatment, sections were stored under non-drying conditions to allow for diffusion. Results showed that effective treatment meeting the AWPA minimum retention (0.17 B203 pcf [2.72 kg/m³] in the outer inch) and penetration (2.5-in [64-mm] or 85% of the sapwood) could be obtained only with certain combinations of seasoning, treatment, and diffusion storage. The best results in terms of both retention and penetration were obtained with material steamed and stored prior to treatment using a 10-min hot bath time. Kiln-dried timbers could not be treated effectively. The results suggest that non-conforming treatment of green or partially seasoned timbers will require higher solution concentrations, higher hot bath temperatures, and/or longer diffusion periods to meet required standards. Results also indicated that treatment of smaller stock in dimension sizes (up to 2-in [50-mm]) should be feasible.
H M Barnes, R W Landers, L H Williams

Direct measurement of fluid flow within wood
1986 - IRG/WP 2248
The problematics of fluid flow mechanism within wood using a permeability concept are highlighted, and the non-feasibility of a practical and versatile model is explained. An alternative method using a negative temperature coefficient thermistor to measure flow velocity directly is presented. The method has been verified in living trees and shows extreme sensitivity for flow above 1 meter/hour. For measuring lower velocities, the method needs improvement.
J P Hösli

Checking of sodium pentachlorophenate fixation in wood
1990 - IRG/WP 3620
In order to estimate the volatilization of sodium pentachlorophenate from treated wood, wood samples treated with pentachlorophenate were analysed after various durations of an EN 73 weathering The results giving no clear evidence of volatilization, treated wood samples were put in a test chamber with precise climatic conditions, the air used in the experiment being analysed. The pentachlorophenate content in air was quantified: 1.8 µg/m³
M Lamour, H Sageot

Preservative treatment of Pinus elliottii
1987 - IRG/WP 3435
The treatment of Pinus elliottii with copper-chrome-arsenic preservative by four alternative seasoning and treatment methods is investigated. Steam conditioning followed by either alternating pressure method (APM) or 'Q' treatment resulted in inadequate preservative penetration. Air drying or high temperature drying followed by the Bethell process resulted in a high standard of treatment.
P Vinden, L Carter

Survey of conditioning treatment practices in India
1978 - IRG/WP 3127
India has 75.3 million hectares (ie about 24% of total land area) under forests out of which the area of productive forests, from which industrial wood is available, is about 60 million ha. The Task Force on Forest Resources Survey has tentatively estimated that the total growing stock in Indian Forests is 24,000 million cubic metres (m³). The total recorded production of wood in the country is roughly estimated as 25 million m³ annually of which approximately 10 million m³ is demanded by various industries and the remaining is used as fuel. India, with developing economy needs very large resources of timbers for diverse purposes. There is already shortage of timber in the country for various wood based industries and it is expected this will progressively increase with the rapid pace of industrialisation. However, suitable measures are being taken to bridge the gap between demand and supply. The entire 10 m³ of industrial wood requires some sort of protection against wood-destroying agencies. Timber awaiting conversion during storage needs prophylactic treatment while for use as poles, fence posts, sleepers, building material, in cooling towers, boats, ships, in mines, in sea-water, etc., timber should be adequately treated with suitable wood preservatives to obtain satisfactory service life. Both heart and sapwood of non-durable species and only sapwood of durable species need protection against wood-destroying agencies. Wood Preservation on scientific and modern lines was introduced in India by Sir Ralph Pearson of the Indian Forest Service in the year 1908. In India, the first wood preservation plant was established at Bally in Howrah in 1854. Of the total timber extracted in India, only a very small proportion, estimated at about 5% is treated. This amounts to 0.45-0.50 million m³ of wood per annum. The total annual capacity of 140 preservation units, existing in the country at present, is estimated at 0.43 million m³ on single shift basis. IS: 401-1967 (Indian Standard - Code of Practice for Preservation of Timber) covers types of preservatives, their brief descriptions, methods of treatment, and the type and choice of treatment for different species of timber for a number of uses. This standard includes only such preservatives and methods of treatment which have given satisfactory results under Indian condition of service. According to this standard, whatever process of treatment is adopted, timber for treatment should be sound and should be dried to an appropriate moisture content (generally not more than 15% for open tank and 25% for pressure processes). All the wood working etc should be done prior to treatment. In case of timbers, specially some conifers having non-durable heartwood which is refractory to treatment, when treating thick members like railway sleepers, beams, piles, etc, incision of all the surfaces, other than the ends, to a depth of 12-20 mm is necessary.
M C Tewari

Exposure monitoring of creosote vapors
1989 - IRG/WP 3511
Creosote oils contain hundreds of compounds. During impregnation and handling of treated wood the main component in the vapors released in air is naphthalene. Other main components are alkyl naphthalenes, indene, phenol and its methyl derivatives, benzothiophene, diphenyl, acenaphthalene and fluorene. In the measurement of creosote vapors, naphthalene can be used as an indicator agent. One of the major urinary metabolites of naphthalene is 1-naphthol. To explore the relation between naphthalene concentration in the air and 1-naphthol in the urine of exposed workers we monitored air concentrations and collected urine samples from six men over a working week. 1-Naphthol concentrations in urine samples were analyzed by GC as a pentafluorobenzylbromide derivative. The average concentration of 1-naphthol in the Monday morning samples was 0.1 mg/l, in the Monday afternoon 3.1 mg/l, in the Friday morning 0.4 mg/l and in the Friday afternoon 2.9 mg/l.
P Heikkilä, M Loutamo, V Riihimäki, M Romo

Analysing the characteristic role of moisture content for drying and fluid flow in Sitka spruce. - Part 1: The drying process of sapwood and heartwood of two different thickness of Sitka spruce using a kiln. - Part 2: Effects of moisture content on longitudinal permeability of Sitka spruce in vertical variation of the tree
2000 - IRG/WP 00-40173
The characteristic role of the moisture content in Sitka spruce (Picea sitchensis (Bong.) Carr.) that grown in the United Kingdom was examined by this study on the basis of (1) the reduction of moisture content in two different thickness of sapwood and heartwood by kiln drying process, and (2) the effects of moisture content to the longitudinal void volume filled of tanalith-C by the full-cell process from base (1 m) to apex (3 m) of the tree in sapwood zone. Accordingly, conclusions on indication of the drying process of sapwood and heartwood, and vertical variation of longitudinal flow with effects of moisture were listed separately: (1) Comparison of Drying Characteristic of Sapwood and Heartwood: The two different thickness (300x30x30 mm3 and 300x20x20 mm3) of sapwood and heartwood of Sitka spruce was dried using the suggested drying schedule in kiln. The reduction of moisture was schematically diagrammed according to sapwood and heartwood stakes. The reduction of moisture followed the same downward trend that sapwood (S) loses more moisture than heartwood (H) although the small stakes of S and H lost moisture rapidly compared with the large ones. (2) Vertical Variation of Moisture Content and Longitudinal Permeability: The 90 kiln dried defect free sapwood stakes (150x25x25 mm3) of Sitka spruce was taken from base to apex of the trees at 1, 2 and 3 m above ground level. After having the determination of moisture content in each experimental stake, the treatment was carried out by the full-cell process with CCA preservative (Tanalith-C) using a model pressure treatment plant. Significant differences observed among the tree heights from 1 to 3 m showing that slightly increases of moisture content from base to apex and conversely decreases of longitudinal void volume filled by preservative fluid.
I Usta

Fixation of CCA in Pinus sylvestris after kiln-drying
1990 - IRG/WP 3594
Tanalith C Paste is 98% fixed and Tanalith Oxide C is 99% fixed irrespective of whether treated Pinus sylvestris is kiln or air dried. A schedule suitable for kiln drying of CCA treated Pinus sylvestris is described.
P Warburton, J A Cornfield, D A Lewis, D G Anderson

Creosote movement from treated wood immersed in fresh water: Initial PAH migration
2003 - IRG/WP 03-50201
Creosote has a long history of successful use as a wood preservative, but polycyclic aromatic hydrocarbons (PAHs) in this preservative have raised environmental concerns, particularly when creosote-treated wood is used in aquatic environments. A number of models have been developed to predict the risk of creosote use in aquatic environments, but one limitation of these models is a lack of data on the initial rates of creosote migration from treated wood. We examined the effect of flow rates on creosote migration from freshly treated wood immersed in fresh water. Creosote component levels declined to a steady state within 7 days, suggesting that creosote migration decreased sharply after an initial spike. The data will be used to enhance existing predictive models.
Sung-Mo Kang, J J Morrell, J Simonsen, S T Lebow

Measurement of VOC emissions from curative treated wood: A new emission test chamber
2001 - IRG/WP 01-50166-13
A poor indoor air quality (IAQ) is now recognized as a potential factor affecting occupants health. There are three basic strategies to improve IAQ: source control, improvement of the ventilation and use of air cleaners. Usually, the most efficient way to improve IAQ is to eliminate the different pollutant sources or to reduce their emissions. In order to precisely measure emissions from building products and estimate the potential heath impact of emitted pollutants, standardised analytical methods are needed. The aim of this paper is to present the new standards prepared by the European Committee for Standardization (CEN) and the International Organization for Standardization (ISO) for the measurement of indoor air pollutants and their application to the characterization of emissions from wood products. The prestandard ENV 13419, subdivided in three parts, has been prepared by the CEN technical committee 264 : ??ENV 13419-1 : Building products - Determination of the emission of volatile organic compounds - Part 1 : Emission test chamber method, ??ENV 13419-2 : Building products - Determination of the emission of volatile organic compounds - Part 2 : Emission test cell method, ??ENV 13419-3 : Building products - Determination of the emission of volatile organic compounds - Part 3 : Procedure for sampling, storage of samples and preparation of test specimens. The two first parts of the prestandard ENV 13419 specify a general laboratory test method for the determination of the area specific emission rate of volatile organic compounds (VOCs) from newly produced building products under defined climate conditions in a test chamber (Part 1) or cell (Part 2). The third part specifies for solid, liquid or combined products, the sampling procedure, transport and storage conditions and preparation of test specimens. In France, those European prestandards have been translated by the French Normalisation Association (AFNOR) in three experimental standards : XP ENV 13419-1, XP ENV 13419-2 and XP ENV 13419-3 [1-3]. In parallel to the ongoing work at CEN, the technical committee 146 of International Organization for Standardization (ISO) has prepared the draft international standard ISO/DIS 16000 related to indoor air. Part 6 of this standard specifies a method for the determination of the emission of single volatile organic compounds (VOCs) and total volatile organic compounds (TVOC) from building materials using test chambers and cells [4]: ??ISO/DIS 16000-6 : Indoor air - Part 6 : Determination of volatile organic compounds in indoor and chamber air by active sampling on TENAX TA sorbent, thermal desorption and gas chromatography using MS/FID. It is intended that, after the final voting stage, the CEN prestandards (Parts 1-3) will be taken over by ISO and that Part 6 of the ISO standard will be taken over by CEN as the fourth part of the ENV 13419 prestandard. As an example, the volatile organic compounds emissions from preservative treated wood samples were characterised according to the CEN ENV 13419-1 prestandard describing the emission test chamber method and to the ISO/DIS 16000-6 prestandard for the analytical method. Two representative wood preservatives (hydrodispersable and petroleum solvent formulation) were tested for this purpose. The VOCs concentrations in the test chamber were monitored during 6 days following a simulated curative wood treatment.
F Maupetit, O Ramalho, C Yrieix

Observations on the uptake and penetration of various liquids in clear heartwood and sapwood of Pinus radiata D.Don
1983 - IRG/WP 3224
Volumetric uptake of water (aqueous copper-chrome-arsenic (CCA)) or methanol, applied by bulk hydrostatic pressure to air dried clear heartwood specimens of Pinus radiata D. Don, far exceeds that of a wide variety of polar and non-polar solvents. In air dried sapwood, the volumetric uptake of CCA tends to be less than that achieved for most solvents including methanol. No comprehensive explanation of the penetration mechanism in these two substrates can yet be offered. High temperature drying effects a significant increase of volumetric uptake of all liquids by heartwood, but not by sapwood, possibly because air dried material is nearly saturated after pressure treatment.
J E Barnacle

Flow charts for termite and decay tests to determine the natural durability of Japanese cedar (Cryptomeria japonica D. Don)
2008 - IRG/WP 08-20385
This paper deals with the experimental flow charts that were used for determination the effects of fungal decay and termite attack on Sugi heartwood during the course of the study of “Comparative studies of natural durability of Japanese cedar (Cryptomeria japonica D. Don) among the geographic cultivate”, which was carried out by Usta et al (2006).
I Usta, S Doi

Volumes and weights of different CCA-C treated wood poles, anchor logs and crossarms of REB at air dry condition
1996 - IRG/WP 96-40073
Researches revealed the unit volumes and weights at air-dry condition (12% MC) of different poles, anchor logs and crossarms species of REB from this world. The softwood products are lighter than hardwood products. Inversely the unit volumes of softwood poles are higher than those of hardwood poles. Red pine (Pinus resinosa), radiata pine (Pinus radiata), blue pine (Pinus wallichiana), fir (Abies densa) and spruce (Picea spineelosa) are the lightest poles and anchor logs with higher unit volumes (Poles). Sundri (Heritiera minor) is the heaviest timber species out of all listed timber species and raintree (Samanea saman) is the lightest timber species among hardwood species.
A K Lahiry

Remedial treatment of wood attacked by insects
1981 - IRG/WP 3175
A review is presented of remedial treatments against wood-boring insects in wood in service. Preconditions and fundamental principles of insect control are compared with the control of fungal attack and reasons are given for the fact that remedial treatments against insects are more commonly applied than against fungi. With regard to insect control measures with a simultaneous preventive effectiveness, information is given on preservatives, control measures as well as on testing the effectiveness of preservatives with eradicant action. An evaluation of 40 tests according to EN 22 or DIN 52164 revealed that a mean depth of effectiveness of 15 mm is obtained at mortality rates of 80-84% of Hylotrupes larvae. At a mortality rate of below 75% the mean depth of effectiveness was about 10 mm and above 90% it was about 27 mm. Among the control measures without any preventive effectiveness fumigation and hot-air treatments are referred to. With regard to biological control measures, practical results are not yet available.
H Kühne

Dynamics of pressure changes in wood during impregnation
1990 - IRG/WP 3615
Conventional methods of impregnation have to be improved for achieving better penetration of refractory wood species. Basic requirements for an adjustment of treatment schedules are, amoung others, a profound knowledge of the course of pressure changes in the wood during treatment. A new method of pressure measurement was developed which supplies exact and reproducible data. The results show that air pressure spreads more rapidly in wood than water pressure. In pine, water pressure is built up in radial direction within hours an declines slowly after pressure release. In spruce, air and water pressure spread more rapidly in green wood than in dry wood. Water pressure of 5 bar applied in radial direction is not achieved within 8 hours time. 5 minutes successions of pressure and pressure release have no effects at 10 mm depth. These findings call into question the conventional OPM technique of rapid successions of pressure and vacuum, and possibly allow easier treating techniques.
R D Peek, S Goetsch

The treatment of sawn whitewood with organic solvent wood preservative
1982 - IRG/WP 3192
The impregnation schedules approved in the UK for the treatment of sawn European whitewood (Picea abies) with organic solvent borne preservatives result in comparitively high loadings relative to the limited depth of penetration they achieve. Results are presented, which show how substantial reduction in the overall loading may be achieved without concomitant reduction in penetration. A model for organic solvent behaviour is postulated as a basis to account for these findings.
L D A Saunders

Improvement of some technological and biological properties of poplar wood by impregnation with aqueous macromolecular compounds
1992 - IRG/WP 92-3721
Poplars (Populus spp) belong to the most important tree species in afforestation programs of the Netherlands. Due to their rapid growth, the wood quality is usually low. Therefore, studies were performed to elucidate whether some technological properties and the resistance against fungal attack could be improved by impregnation with water-soluble resins. The results showed that swelling and shrinkage of poplar wood may considerably be reduced by a treatment with certain resins. The anti-shrink efficiency (ASE) strongly depends upon the resin type. An air-curing alkydresin based on polybutadiene and an air-curing acrylate modified alkydresin emulsion caused the best effects. Additions of wood preservatives to the resins further improved the ASE. Some disadvatages of the tested resins may be seen in their leachability with consequent loss of the dimension-stabilizing effects. The resins by themselves don't reveal fungistatic properties but an impregnation of poplar wood with these materials led in all cases to a better durability against Coniophora puteana and Coriolus versicolor. Leaching procedures influenced the durability in various ways. With resin/fungicide combinations, a good resistance against Coriolus versicolor could be reached even after leaching. SEM and EDXA methods were used to localize the resins in the cell walls and lumina and to detect the growth of mycelium in the specimens.
R D Peek, H Militz, J J Kettenis

Probing red maple pit membrane pore size at FSP and OD using polystyrene macromolecules
2001 - IRG/WP 01-40217
A modified solute exclusion technique was used to pressure impregnate a polystyrene molecular weight (MW) series dissolved in styrene into red maple samples at approximately the fiber saturation point (FSP) and oven dry (OD). Radial penetration was less than tangential and FSP less than OD. There was a marked penetration change with MW in the tangential direction, although there appeared to be a slight decrease in FSP penetration at the higher MW tested.
A Omidvar, M H Schneider, A R P Van Heiningen

Efficiency of wood impregnation processes
1980 - IRG/WP 3151
Many wood impregnation processes have been in use for a very long time, up to 150 years, but they have not been progressively modified. This paper considers impregnation processes in relation to current requirements, particularly impregnation efficiency and energy consumption. The term 'pore' is used throughout in its physical sense and is not confined to botanical 'pores'. SI units are used and, for convenience, atmospheric pressure is assumed to be exactly 100 N/m²; complete vacuum is 0 N/m². These observations and conclusions summarise an extensive programme of investigation at Penarth Research Centre involving creosote and water-borne preservatives, as well as a range of organic solvent preservatives.
B A Richardson

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