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Dynamics of pressure changes in wood during impregnation
1990 - IRG/WP 3615
Conventional methods of impregnation have to be improved for achieving better penetration of refractory wood species. Basic requirements for an adjustment of treatment schedules are, amoung others, a profound knowledge of the course of pressure changes in the wood during treatment. A new method of pressure measurement was developed which supplies exact and reproducible data. The results show that air pressure spreads more rapidly in wood than water pressure. In pine, water pressure is built up in radial direction within hours an declines slowly after pressure release. In spruce, air and water pressure spread more rapidly in green wood than in dry wood. Water pressure of 5 bar applied in radial direction is not achieved within 8 hours time. 5 minutes successions of pressure and pressure release have no effects at 10 mm depth. These findings call into question the conventional OPM technique of rapid successions of pressure and vacuum, and possibly allow easier treating techniques.
R D Peek, S Goetsch

The effect of pretreatments on the impregnation of air-dried sawn Belgian spruce
1988 - IRG/WP 3490
In general the impregnation of airdried spruce results in a variable treatment and limited penetration. This is the result of pit aspiration that occurs during drying of the spruce sapwood and heartwood. Spruce timber is becoming of greater importance in Belgium and hence research for better treatment of this vulnerable wood species is needed. Squared airdried timber of different dimensions were extracted from 10 winter-felled logs (Picea abies (L.) Karst) and impregnated with preservative used for constructional purposes. Partly the material was presteamed or waterlogged. Prior to the preservative treatment both groups were reconditioned to the same moisture content as the reference material (airdried). Retention and different penetration parameters showed better figures when only modifying the treating cycle rather than using a pretreatment. Both pretreatments seemed to have no positive effect on the treatability of airdried material. Increasing the strength of the initial vacuum parameters of the full-cell processes improved the degree and homogenity of the penetration of the preservative components.
J Van Acker, M Stevens

A new vacuum/pressure plant system
1988 - IRG/WP 3479
In the subtropical regions, the problem of wood supplying becomes more and more difficult to be solved. In that context, the Centre Technique Forestier Tropical had paid a particular attention to the valorization of products issued from plantations in dry zones of Africa. In these plantations, the products of clearings can be used as fencing, stakes or for traditional construction. However in these trunks of small diameter, the sapwood which represents a large proportion of the ligneous matter utilized, possesses a poor natural resistance as much as in regard to decay as in regard to wood-destroying insects and particularly termites. For that reason a rational use of the round woods cannot be considered without the help of wood preservation. The single dipping or brushing being insufficient mainly for the timber in ground contact and the traditional vacuum-pressure treatment being considered too expensive by local authorities, the Centre Technique Forestier Tropical tried to imagine a new system of treatment.
C Dalois, R Schwartz, G R Y Déon

Redistribution of boric acid in radiata pine during drying after preservative treatment
1993 - IRG/WP 93-40010
Samples of 100 x 50 mm² radiata pine were processed with a variety of options to produce dry, boron-treated wood. Concentrations of boric acid in the central one-ninth and in the whole of the wood cross-sections were determined by chemical analysis and compared. Diffusion treated material was dried by air, conventional kiln (70/60°C), or high temperature kiln (120/70°C). Four different predrying, pressure treatment, and redrying combinations were also evaluated, using a low net absorption (nominally 200 l/m³) treating process. Drying after diffusion treatment resulted in substantial redistribution of preservative towards the surface of the wood samples. In addition, a net loss of preservative from kiln-dried, diffusion-treated wood was observed. Pressure treated wood was much less affected. Mechanisms which may account for observations about the various processing options are postulated. Results are compared with those produced by Vapour Boron Process treatment of the same material. The advantages of this process are discussed, particularly in view of the recent extension of the New Zealand specifications for preservative treatment to include retention requirements for dry, boron-treated wood.
A J Bergervoet, D R Page, J A Drysdale

Danish wood preservatives approval system with special focus on assessment of the environmental risks associated with industrial wood preservatives
2001 - IRG/WP 01-50166-01
The following is a description of the procedure used by the Danish Environmental Protection Agency to assess the environmental risks associated with preservatives used in the pressure impregnation of wood. The risk assessment covers issues considered to be of significance for the environment and which are adequately documented so as to allow an assessment. Such issues are persistence and mobility in soils, bioaccumulation and the impact on aquatic and terrestrial organisms. Unless required in special circumstances, the assessment does not apply to birds and mammals as the normal use of preservative treated wood is not expected to involve any noteworthy exposure of these groups. Approval of wood preservatives will be based on a general assessment of the environmental risk associated with the normal use of wood treated with the preservative in a realistic worst case situation. The assessment may address other aspects such as disposal and total life cycle.
J Larsen

Status of the research and development of a new preservative system (EFPL) for pressure treatment of spruce in Canada
1975 - IRG/WP 348
Our work has been to develop a system which would have the stability of the ACA system and the formulation flexibility of the CCA system enabling properties such as fixation of arsenic, water repellency, appearance and cost to be controlled. Our permeability studies of spruce using a method previously developed indicated that an ammoniacal solution of copper arsenate is an excellent candidate for the treatment of spruce. Studies of the permeability of spruce sapwood microsections to CCA preservative and to an ammoniacal solution of copper arsenate proved that the ammoniacal system penetrates 1.7 to 1.8 times faster than the CCA system, in the radial direction. The permeability in the tangential direction was on the average 3.8 times better. These results were confirmed by pressure treatments of spruce lumber and spruce roundwood with both preservatives.
J Rak, M R Clarke

Manual of a mini treating plant for waterborne preservative treatment of timber and bamboo
1999 - IRG/WP 99-40130
This contributional article includes machinaries and equipments necessary for a small wood treating plant for the pressure treatment of tim bers with waterborne preservatives along with the cost and design. The preservative treatment limitations, treatment schedules and specifications for different products have been described. The cost of a mini treating plant will be 6,00,000 Tk. (13,000 US$), suitable for preserving timber and bamboo products for indoor and outdoor uses and will out last teak wood. The additional durability of timber and bamboo will create economically and environmentally safe conditions.
A K Lahiry

The use of pressure cycling to improve heartwood penetration in Pinus radiata (D. Don)
1995 - IRG/WP 95-40050
This study investigates the effect of cycling pressure on the treatability of radiata pine heartwood. The results indicate that liquid penetration into the heartwood is affected by the preconditioning method used and pressure treatment time. There is no significant improvement in the penetration of Pinus radiata (D. Don) heartwood when a cycling or pulsation process is used.
P R S Cobham, P Vinden

Health aspects concerning the use of bifluorides in wood
1981 - IRG/WP 3173
An attempt has been made to find a correlation between the quantities F¯ and HF present among other ions in an 'Improsol' solution consisting of NH4F.HF and KF.HF, the quantity absorbed by the wood from this after immersion and the toxicological effects of this treated wood when it is used in rooms destined for the residence of people or animals or for the storage of foodstuffs.
H F M Nijman

Non-pressure treatability of plywood by CCA, CCB and boron
2005 - IRG/WP 05-40295
Study on diffusibility and absorbability of CCA, CCB and boric acid in 3 mm thick 3-ply hardwood plywood at water saturated and air-dry conditions and dipped at same concentration (5%) and same duration of time (12 hours) revealed complete diffusion of all the preservatives at water saturated condition. Only the CCA-C was found absorbed by the plywood at air-dry condition. The rate of absorption and diffusion of CCA-C was found about 4.5 times higher than CCB and boric acid.
A K Lahiry

Improved equipment and technique for high pressure sap displacement impregnation of natural round wood
1972 - IRG/WP 309
Hitherto the main problem in the practical application of high pressure sap displacement impregnation (HPSD) has been in devising a satisfactory cap. Such a cap must be easily fitted to different size log ends to give a leak proof seal. The present contribution describes a new type of cap and sealing system designed to meet these requirements.
C G W Mason, F B Shorland

An investigation of the effects of pre-steaming on the treatment of sawn spruce timber with Celcure A, a copper-chrome-arsenic preservative
1981 - IRG/WP 3150
Difficulties in the treatment of spruce using standard vacuum/pressure techniques with both water-borne and organic solvent preservatives are well known. We have evaluated the influence of steaming on treatability with a waterborne CCA preservative.
C R Coggins

Effects of various preservative treatments on the mechanical and physical properties of plywood
1993 - IRG/WP 93-40007
The technical properties of plywood are related to both the intrinsic characteristics of its composing wood species and the quality and performance of the glue bond which acts as an interface between veneer sheets. Consequently mechanical and physical testing and glue bond strength analysis offer an appropriate means for studying the effect of preservative treatments on the overall quality of plywood. A range of boards was treated with waterborne and oilborne preservatives. Changes in modulus of elasticity, modulus of rupture and tensile strength were noted as well as variations in physical properties. Analysis of the glue bond strength was done by shear strength testing and determination of the amount of wood failure after different ageing procedures.
J Van Acker, M Stevens

Borate thermal treatments
1992 - IRG/WP 92-3715
Green, partially seasoned (air-dried, steam conditioned), or kiln-dried southern pine timbers were treated thermally using 15% disodiumoctaborate tetrahydrate solution. After treatment, sections were stored under non-drying conditions to allow for diffusion. Results showed that effective treatment meeting the AWPA minimum retention (0.17 B203 pcf [2.72 kg/m³] in the outer inch) and penetration (2.5-in [64-mm] or 85% of the sapwood) could be obtained only with certain combinations of seasoning, treatment, and diffusion storage. The best results in terms of both retention and penetration were obtained with material steamed and stored prior to treatment using a 10-min hot bath time. Kiln-dried timbers could not be treated effectively. The results suggest that non-conforming treatment of green or partially seasoned timbers will require higher solution concentrations, higher hot bath temperatures, and/or longer diffusion periods to meet required standards. Results also indicated that treatment of smaller stock in dimension sizes (up to 2-in [50-mm]) should be feasible.
H M Barnes, R W Landers, L H Williams

Radical changes in the requirements for more safe pressure impregnation in the Nordic countries in 1988
1990 - IRG/WP 3581
After introduction of quality control schemes and standards in the Nordic countries during the seventies, the first radical change of the standards and practice of work took place after pressure from the labor unions and authorities in 1988 and 1989 in Denmark and in Sweden. A new class of preservation with less retention for out of ground contact use was introduced, fixation times were prolonged to 6 and 14 days, and branding became a requirement. At the same time, treating companies replaced CCA with arsenic-free preservatives, and started using processes for accelerated fixation. Drying of treated wood was started to be used widely.
B Moldrup

Recycling of pressure impregnated timber and preservatives - incineration techniques
2001 - IRG/WP 01-50166-19
The object of the recycling research projects is to determine the technical and economical requirements of the recycling of CCA-impregnated wood. In the first recycling of impregnated timber project the amount and location of recyclable treated wood in Finland was determined and the costs of recycling were calculated. An incineration test was also made (1998). The conclusion of the first project is that it is possible to design a full scale plant for burning CCA-treated wood, to treat condensate water, to purify the gases using a very effective method, and to treat the ash in a copper smelter. The object of the second recycling research project in Finland is to determine the technical and economical requirements of incinerating CCA-impregnated timber so that an investment decision can be taken on whether to build an incineration plant. Thus far in the course of the second project a trial has been established for collecting impregnated sawn timber at waste treatment plants and for cleaning the material of large metal constituents. The first part of the incineration trial was carried out in November 2000 and this will continue in the spring of 2001, after which an interested investor can reach a decision on a possible investment.
T Syrjänen, E Kangas

Light organic solvent preservative treatment schedules for New Zealand-grown radiata pine
1986 - IRG/WP 3379
The influence of pressure differential and treatment time on preservative uptake and distribution in radiata pine heartwood and sapwood is investigated. Treatment schedules are defined which minimise solvent usage but ensure complete sapwood penetration and optimise heartwood penetration.
P Vinden

Creosoted radiata pine by non-pressure methods
1988 - IRG/WP 3486
Posts of Pinus radiata have been impregnated with creosote by immersion for 1, 3, and 7 days, and by hot-and-cold open tank with hot bath temperatures at 40°C and 60°C. On the basis of the retention rates obtained, suitable procedures are described for wood elements that are going to be in ground contact, and an analysis is made of the way in which the variables tested affect the results.
M V Baonza Merino, C De Arana Moncada

Report on the treated piles and fenders in the wharves in Port Moresby harbour, and the Huon Gulf, Lae
1977 - IRG/WP 433
To investigate the resistance of Papua New Guinea timber, vacuum pressure impregnated with Copper-Chrome-Arsenic salts, to marine borer attack in the waters of Papua New Guinea.
S M Rayner, C R Levy

Imprégnation de bois ronds par déplacement de sève à Madagascar
1975 - IRG/WP 352
M Fougerousse, P Guéneau

Survey of conditioning treatment practices in India
1978 - IRG/WP 3127
India has 75.3 million hectares (ie about 24% of total land area) under forests out of which the area of productive forests, from which industrial wood is available, is about 60 million ha. The Task Force on Forest Resources Survey has tentatively estimated that the total growing stock in Indian Forests is 24,000 million cubic metres (m³). The total recorded production of wood in the country is roughly estimated as 25 million m³ annually of which approximately 10 million m³ is demanded by various industries and the remaining is used as fuel. India, with developing economy needs very large resources of timbers for diverse purposes. There is already shortage of timber in the country for various wood based industries and it is expected this will progressively increase with the rapid pace of industrialisation. However, suitable measures are being taken to bridge the gap between demand and supply. The entire 10 m³ of industrial wood requires some sort of protection against wood-destroying agencies. Timber awaiting conversion during storage needs prophylactic treatment while for use as poles, fence posts, sleepers, building material, in cooling towers, boats, ships, in mines, in sea-water, etc., timber should be adequately treated with suitable wood preservatives to obtain satisfactory service life. Both heart and sapwood of non-durable species and only sapwood of durable species need protection against wood-destroying agencies. Wood Preservation on scientific and modern lines was introduced in India by Sir Ralph Pearson of the Indian Forest Service in the year 1908. In India, the first wood preservation plant was established at Bally in Howrah in 1854. Of the total timber extracted in India, only a very small proportion, estimated at about 5% is treated. This amounts to 0.45-0.50 million m³ of wood per annum. The total annual capacity of 140 preservation units, existing in the country at present, is estimated at 0.43 million m³ on single shift basis. IS: 401-1967 (Indian Standard - Code of Practice for Preservation of Timber) covers types of preservatives, their brief descriptions, methods of treatment, and the type and choice of treatment for different species of timber for a number of uses. This standard includes only such preservatives and methods of treatment which have given satisfactory results under Indian condition of service. According to this standard, whatever process of treatment is adopted, timber for treatment should be sound and should be dried to an appropriate moisture content (generally not more than 15% for open tank and 25% for pressure processes). All the wood working etc should be done prior to treatment. In case of timbers, specially some conifers having non-durable heartwood which is refractory to treatment, when treating thick members like railway sleepers, beams, piles, etc, incision of all the surfaces, other than the ends, to a depth of 12-20 mm is necessary.
M C Tewari

Exposure monitoring of creosote vapors
1989 - IRG/WP 3511
Creosote oils contain hundreds of compounds. During impregnation and handling of treated wood the main component in the vapors released in air is naphthalene. Other main components are alkyl naphthalenes, indene, phenol and its methyl derivatives, benzothiophene, diphenyl, acenaphthalene and fluorene. In the measurement of creosote vapors, naphthalene can be used as an indicator agent. One of the major urinary metabolites of naphthalene is 1-naphthol. To explore the relation between naphthalene concentration in the air and 1-naphthol in the urine of exposed workers we monitored air concentrations and collected urine samples from six men over a working week. 1-Naphthol concentrations in urine samples were analyzed by GC as a pentafluorobenzylbromide derivative. The average concentration of 1-naphthol in the Monday morning samples was 0.1 mg/l, in the Monday afternoon 3.1 mg/l, in the Friday morning 0.4 mg/l and in the Friday afternoon 2.9 mg/l.
P Heikkilä, M Loutamo, V Riihimäki, M Romo

Long-term performance of a "wax" type additive for use with water-borne pressure preservative treatments
2000 - IRG/WP 00-40159
Field performance results are updated for matched CCA treated decking boards with and without an emulsion water repellent additive incorporated with the initial pressure treatment. Decks have been exposured for over 9 years in Harrisburg, NC. Boards were evaluated for in-service and laboratory performance for water repellent efficacy, as well as additive loadings in the boards after this exposure. All results support that these additives can provide long-term protection against many of the physical defects that develop in pressure treated wood during exposure.
A R Zahora

Patent on the use of tannic acid and ferric chloride against marine borers, etc
1982 - IRG/WP 495
R Mitchell, T D Sleeter

Diffusion treatment plants (Latin America - Africa)
1974 - IRG/WP 333
B N Prasad

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