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Comparison between the Hylotrupes bajulus strains of different European laboratories
1980 - IRG/WP 1118
In several European countries, wood preservatives of the same formulation are subjected for the quality label to particular tests according to standards established by the CEN. The different laboratories which carry out these tests have had their cultures for many years. The insects are kept in optimal nutritional and climatic conditions and have always mated amongst themselves. On the one hand, eradicant tests made with the same preservative in different laboratories have not always yielded the same results, and on the other hand, the Comitte of European Homologation has been trying to establish a single label for the European Community according to which it will be possible to carry out tests by any national laboratory of the participating countries. If the results are satisfactory, this will enable an approval certificate to be provided for the sale of these products throughout the countries of the Community. It is very important to be certain that the behaviour of insects and the insecticide resistance of the different insect strains are identical. For this, the best test seemed to be the determination of the toxic value of the wood preservatives against Hylotrupes bajulus (Linnaeus) new-hatched larvae, according to the European standard EN 47.
Proposal for further work on accelerated ageing
1988 - IRG/WP 2314
A comparison of soft rot, white rot and brown rot in CCA, CCP, CCF, CCB, TCMTB and benzalkonium chloride treated Pinus radiata IUFRO stakes, after 9-15 years exposure at five test sites in New Zealand
1991 - IRG/WP 1485
The aim of this study was to determine if decay type varies significantly between five field trial test sites of different soil type, aspect and climate in 9-15 year old, replicate CCA, CCF, CCP. CCB, TCMTB and AAC treated IUFRO stakes. A visual on-site assessment of decay type on every test stake was made and observations confirmed by microscopical examination. Regression analyses were used to determine significant differences of percentage frequency of occurrence of each rot type between sites and preservatives. Large differences in percentage frequency of occurrence of rot type were evident between sites. One site was dominated by brown rot (85%) and two were dominated by soft rot (99 and 91%). The fourth site had intermediate proportions of brown rot (40%) and soft rot (71%) but had the second highest occurrence of white rot (32%) (highest = 37%; lowest = 11%). The fifth site was distinct in that a large proportion of stakes (69%) had both well established brown rot and soft rot. Stakes at the other four sites tended to have only one rot type. Some highly significant preservative effects were also found. Possible causes of these differences are discussed in terms of inter-site soil type, climate and other differences.
R N Wakeling
Finishes for outdoor timbers
1975 - IRG/WP 378
Field trial with poles of Scots pine treated with six different creosotes
1996 - IRG/WP 96-30115
In the middle of the 50's field trials with creosote-treated poles were started in France, Germany and Sweden. The trials were initiated by WEI (Western-European Institute for Wood Preservation). Six different creosotes were used and 40 poles per creosote were installed at each test field. Results after 39 years of exposure in Simlangsdalen, Sweden are reported. Poles treated with a heavy creosote were less decayed than poles treated with medium-heavy creosotes. Poles treated with a light creosote were most decayed.
Wood preservatives: Field tests out of ground contact. Brief survey of principles and methodology
1976 - IRG/WP 269
This paper contains the following spots: 1.: The general need for field tests. 2.: Interests and limits of field tests in ground contact. 3.: Various methods in use for out-of-ground contact field tests. 4.: Fungal cellar tests are they an alternative to above-ground decay exposure tests? 5.: Conclusions.
Collaborative soft rot tests. Names and addresses of collaborators
1973 - IRG/WP 231
Improvements of monitoring the effects of soil organisms on wood in fungal cellar tests
1996 - IRG/WP 96-20093
Accelerated testing the durability of preservative treated timber in a so called "fungal cellar" or "soil-bed" to evaluate its performance in ground contact is widespread practice. In order to obtain a more accurate and reproducible estimate of preservative performance, several institutes, among them the BAM in Berlin, have routinely carried out static bending tests in addition to visual examination. These tests were usually performed with a defined maximum load or deflection path regardless of the remaining degree of elasticity of the test specimens. Recent studies at the BAM revealed that by modifying the method, i.e. by restricting the applied load to the non-destructive interval for each individual test specimen, the calculated modulus of elasticity (MOE) reflect the changing strength properties caused by biological deterioration and allow within a relatively short time valuable predictions on the service life of the treated timber in soil contact.
I Stephan, S Göller, D Rudolph
Co-operative studies on determining toxic values against wood-destroying Basidiomycetes: Progress report to May 1989
1989 - IRG/WP 2339
This document reports progress on the co-operative study between nine laboratories set up following the proposals contained in Document IRG/WP/2316. Results have been received from two laboratories. Toxic values data have been established successfully using the test fungus Coniophora puteana but problems have been encountered with the other test fungi.
A F Bravery, J K Carey
Collaborative soft rot tests: PRL tests of Cu/Cr/As preservative using method of Document No: IRG/WP/208
1973 - IRG/WP 223
These tests were undertaken as a preliminary to the next series of collaborative soft rot tests. An interim report has already been presented at Berlin in 1972 as Document No: IRG/WP/211
J K Carey, J G Savory
Current techniques for screening initial formulations against Basidiomycetes and soft rot
1978 - IRG/WP 2103
J D Thornton, H Greaves
Japan's comments on ISO/DIS 12583-1/2
1996 - IRG/WP 96-20100
The paper describes an accelerated field test for the evaluation of timber preservative formulations against subterranean termites. The method has been adopted by the South African wood preservation industry as a screening method for the approval of wood preservatives for use under SA conditions. The method which is based upon the fungal cellar test offers a rapid means of evaluating the comparative performance of new wood preservative formulations in an environment that accurately reflects field conditions.
P Turner, D Conradie
Moisture content levels and decay of hemlock
1986 - IRG/WP 1287
As a model of decay conditions of wooden members in wooden houses, a decay test was set up in which samples of western hemlock (Tsuga heterophylla) under 4 moisture levels were examined. Each week the samples were weighed and if the weights indicated that their moisture contents were lower than the expected levels, distilled water was added. Every 8 weeks 3 samples from each condition were oven dried at 60°C for 48 hours, up to 48 weeks. After 48 weeks, 3 samples from each condition were oven dried every 16 weeks. The results obtained were as follows: After examining the samples for 96 weeks at 27°C, the mean weight loss of the hemlock samples kept at about 50-100% moisture content level was larger than those of the other levels. If the samples were dried every 8 weeks, the amount of decay in them was not significant. Decay was also not significant in the samples kept at approximately 20-30% moisture content level.
Marine testing of selected waterborne preservatives
1987 - IRG/WP 4137
In 1978 a marine test was established at West Vancouver, B C. to determine the performance of selected waterborne preservatives. The preservatives in test were chromated-copper-arsenate (CCA-C), ammoniacal copper arsenate (ACA), a modified formulation of ACA which contained a higher copper content (modified ACA), ammoniacal copper zinc arsenate (ACZA) and ammoniacal zinc arsenate (AZA). The wood species used for the test was red pine. After eight years in test the CCA is providing excellent performance at all retentions, while the modified ACA is showing significant deterioration only at the lowest level. The ACA is performing quite well although it shows signs of surface deterioration at all retention levels. The performance of the ACZA is rated as unsatisfactory at retentions below 32 kg/m³ while AZA was considered to be unsuitable for use in the marine environment.
J N R Ruddick
Synergistic effect of boron on Streptomyces rimosus metabolites in preventing conidial germination of sapstain and mold fungi
1992 - IRG/WP 92-1565
We evaluated the synergistic effect of boron (4% BAE solution of Tim-Bor or 4% boric acid) on Streptomyces rimosus metabolites in preventing spore germination of sapstain and mold fungi using plate bioassay, Southern yellow pine and sweetgum block tests, and green pine log sections: sapstain -- Ceratocystis coerulescens, Ceratocystis minor, and Aureobasidum pullulans; mold fungi -- Aspergillus niger, Penicillium spp, and Trichoderma spp. Inhibition of spore germination in plate bioassay by metabolites with boron was more effective than without added boron. Treatment of wood samples with the mixture of boron and unconcentrated metabolites also resulted in the synergistic effect and completely inhibited spore germination of sapstain and mold fungi.
S C Croan, T L Highley
Fungicidal activity of some organic solvents, copper carboxylates and their complexes with 2-aminoethanol
1997 - IRG/WP 97-30136
We evaluated the activity of eight organic solvents against wood - rotting fungus Trametes versicolor in order to choose the most appropriate one for rapid screening tests of some copper(II) carboxylates and their adducts with 2-aminoethanol. Their activity against the selected fungus was classified in the following order: chloroform > N,N-dimethylformamide > acetonitrile > methanol > dimethyl sulfoxide > ethanol > acetone. The non-polar white spirit did not dissolve in the growth medium and the results could not be directly compared with the results for other solvents. As an appropriate solvent for screening of the tested copper(II) carboxylates, dimethyl sulfoxide (DMSO) was chosen. Minimal inhibitory concentration against Trametes versicolor of the screened carboxylates was in the concentration range of 1x10-4 to 1x10-3 mol/l. Coordinated amine ligands slightly, and not significantly, decreased fungicidal properties of the tested carboxylates.
M Petric, F Pohleven
On Donkioporia expansa (Desm.) Kotl. & Pouzar
1986 - IRG/WP 1285
Donkioporia expansa is found more often in houses than realised until now. Virulence tests according to EN 113 show not only an attack of oak, but also of other hardwoods and even soft-woods.
Soil virulence tests using Scots pine sapwood
1973 - IRG/WP 222
Following the tests reported in Document No: IRG/WP/210, in which soils from different laboratories were investigated for virulence, supplementary tests have been carried out using Scots pine sapwood and an extended incubation period.
J K Carey, J G Savory
Essais biologiques sur poteaux traités à la Wolmanit C.B. suivant le procédé Boucherie modifé
1974 - IRG/WP 336
D Lapetite, C Jacquiot, J Campredon
Protocol for evaluation and approving new wood preservative
1985 - IRG/WP 2159
M E Hedley, J A Butcher
Results of stake tests on wood preservatives (Progress report to 1974)
1975 - IRG/WP 361
A number of field stake trials on preservative-treated wood have been carried out at Princes Risborough Laboratory from 1928 to the present day, and many of the tests still continue. This paper presents in detail the results obtained to date, covering about 15 000 individual test stakes exposed over the period.
D F Purslow
Evaluation of new creosote formulations after extended exposures in fungal cellar tests and field plot tests
2000 - IRG/WP 00-30228
Although creosote, or coal tar creosote, has been the choice of preservative treatment for the railroad industry since the 1920s, exuding or "bleeding" on the surface of creosote-treated products has been one incentive for further enhancements in creosote production and utility (Crawford et al., 2000). To minimize this exuding problem, laboratories such as Koppers Industries Inc., USA, and Commonwealth Scientific and Industrial Research Organization (CSIRO), Division of Chemical and Wood Technology, Melbourne, Australia, have developed changes in processing of coal tar that produce distillates with fewer contaminants. This "clean distillate" is then used to formulate "clean creosote" as a preservative. These new, unique creosote formulations are being investigated as part of a program to enhance the use of regionally important wood species in the United States. Four retention levels of each of two new creosote formulations creosote, one pigment-emulsified creosote (PEC) and one creosote formulation that meets the AWPA Standard C2-95 for P1/P13 creosote (AWPA, 1995a), were applied to two softwood species and two hardwood species. Two laboratory procedures, the soil-block and fungal cellar tests (accelerated field simulator), were used to evaluate the four creosote formulations. These procedures characterized the effectiveness of the wood preservatives. The soil-block tests were used to determine the minimum threshold level of the preservative necessary to inhibit decay by pure cultures of decay fungi. In general, the soil block tests showed there was little difference in the ability of the four creosote formulations to prevent decay at the three highest retention levels as summarized in a previous report by Crawford and DeGroot (1996). The soil-block tests will not be discussed in this report. Fungal cellar tests expose treated wood to mixtures of soil-borne fungi that promote accelerated attack. Crawford and DeGroot (1996) discussed the evaluation of the creosote formulations after 17 months of exposure in the USDA Forest Service, Forest Products Laboratory (FPL), fungal cellar. At that point in time data from the fungal cellar tests showed that softwoods are protected better than hardwoods for all four formulations of creosote tested. This report will discuss exposure of the fungal cellar stakes upto 36 months. In addition, field stake tests are being used to verify service life of the new creosote formulations in vivo. Results from accelerated tests are indicative of field performance, but the correlation between laboratory and field results is still being investigated. Field stake tests are regarded as critical, long-term evaluations that provide results most directly related to the performance of treated products in service. In this study, we report on the performance of the creosote formulations after five years of exposure in field tests.
D M Crawford, P K Lebow, R C De Groot
Laboratory decay test of Burmese in and kanyin treated with three wood preservatives
1982 - IRG/WP 3210
Laboratory decay tests were performed on samples of In (Dipterocarpus tuberculatus Roxb.) and Kanyin (Dipterocarpus alatus Roxb. and Dipterocarpus turbinatus Gaertn f.) pressure treated with three wood preservatives - copper arsenic additive (CAA - a variation of ammoniacal copper arsenate), Arquad C-33 (a waterborne quaternary ammonium formulation), and tributyltin acetate (TBTA) dissolved in ethanol. Pressure treatments with each preservative involved a 0.5 - 1 hour vacuum followed by a 4 hour period of pressure. This resulted in a very variable treatment because of the inherent difficulty in treating these woods. The decay tests entailed a slightly modified form of the AWPA M10-77 standard soil-block test using three brown-rot and three white-rot fungi. The untreated In and Kanyin samples were moderately susceptible to decay though weight losses were very variable and some samples of Kanyin (usually the densest and least permeable) were naturally resistant. At the concentrations tested CAA was the most effective in reducing weight losses incurred in the soil-block tests. TBTA was successful in controlling decay caused by all but two of the test fungi. It is suggested that preservative retentions for TBTA conforming to those included in the Candadian standard for bis (tributyltin) oxide would exceed the toxic limit for all the fungi tested
J N R Ruddick, R S Smith, A Byrne
Field tests out of ground contact in France: Definition of the test procedure and preliminary results after 18 months
1981 - IRG/WP 2161
Laboratory evaluation of chemicals as termiticides
1986 - IRG/WP 1293
Laboratory procedures are described for screening chemicals against subterranean termites. Fast-acting compounds with persistent termiticidal activity are identified in tests using a soil substrate, and slower-acting bait toxicants are evaluated in a series of tests using cellulose substrates.
S C Jones