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Determination of bis-(N-cyclohexyl-diazeniumdioxy)-copper in different matrices by photometer, thermal energy analyzer and HPLC
1999 - IRG/WP 99-20179
For the quantitative analysis of bis (N-cyclohexyl-diazeniumdioxy)-copper (Cu-HDO) three analytical methods are used. The employment of the different methods depends on the matrices involved. For several years now, the colorimetric determination of Cu-HDO by photometer has been applied to solutions and concentrates of wood preservatives. In principle, the technique consists of a quantitative conve...
J Wittenzellner, W Hettler, M Maier


Determination of fungitoxic value of preservatives in laboratory wood-block tests. Part 2: Statistical estimation
1989 - IRG/WP 2327
Laboratory modified agar-block tests were made to determine the fungitoxic value of the wood preservative CCA against the test fungus Serpula lacrymans using statistical methods. With the aid of statistical computer programmes based on the least square method. the regression equation was found for the dependence between sample mass loss and preservative retention both in terms of percentage and fo...
J Wazny, J D Thornton, K J Krajewski


Determination of fungitoxic value of preservatives in laboratory wood-block tests. Part 1: Standard procedures
1989 - IRG/WP 2326
By applying a modified agar-block method, a comparative analysis was made on the toxic value of the wood preservative CCA against the test fungus Serpula lacrymans. The procedure applied to determine the results accounted for different standards: EN (Toxic limit), ASTM (threshold retention), GOST (threshold retention and protection probability), PN (toxic doses) and JIS (value of efficiency). Desp...
J Wazny, J D Thornton


Preliminary observations on tributyltin treated Scots pine sapwood using 119Sn (Mössbauer and NMR) spectroscopic techniques
1984 - IRG/WP 3312
119mSn Mössbauer data are presented for bis(tributyltin) oxide, tributyltin ethanesulphonate, bis(tributyltin) carbonate and tris(tributyltin) phosphate, both in the pure form and in Scots pine sapwood. The structures proposed for these compounds, in the solid state, are supported by 119Sn nuclear magnetic resonance spectroscopy.
R Hill


Inter-laboratory comparison of assessment methods for wood preservatives against subterranean termites: Determination of protection threshold limits for CCA
1999 - IRG/WP 99-10317
In 1996, several institutes conducted laboratory bioassays on the efficacy of unleached Pinus radiata specimens treated with copper-chromium-arsenic (CCA) and copper naphthenate (Cu Naph) at retentions of 0.5, 1.0, 2.0 and 4.0 kg/m3 (total salt for CCA; elemental copper for Cu Naph) against a range of species of subterranean termites (IRG/WP/96-10174). Each participant employed the standard test m...
J W Creffield, M Lenz


Determination of toxicity data for preservatives against Basidiomycetes by measuring the reduction in compression strength of wood
1988 - IRG/WP 2297
Blocks of Pinus radiata D. Don were treated to 12 retention levels with CCA and NaPCP. These were exposed for 12 weeks in agar jars to the dry rot (brown rot) Serpula lacrymans (Schum. ex Fr.) S.F. Gray. After mass loss determination, the same blocks were tested for reduction in compression strength parallel to the grain. Using both these parameters, together with interpolated 6 week strength loss...
J Wazny, J D Thornton


A comparison of analytical and visual techniques used for assessment of weathering properties of chromium and copper azole treated timber
1994 - IRG/WP 94-20023
The weathering properties of preservative treated timber were studied by measuring surface lignin loss and by microscopic examination after weathering, and results were related to qualitative assessments of visual appearance after weathering. Measurement of relative rates of delignification of untreated and preservative treated timber obtained by FTIR analysis, and weight loss determined on thin v...
J A Cornfield, M D C Hale, G Fettis


The use of low cost X-ray fluorescence instruments in the determination of copper chromium and arsenic in preservative treated wood
1987 - IRG/WP 2278
Internal quality control in timber treatment plants can be pursued by analysis of preservative treatment solutions and treated timber. Treaters must proceed with costly and lengthy analyses through analytical laboratories. An alternative approach for the timber treater, is to use low cost analysers (L.C.A.'s) based upon x-ray fluorescence. Detailed comparisons have been made between stand...
J Norton, L E Leightley


Determination of thermal degradation of isothiazolone treated wood
1997 - IRG/WP 97-30154
Wood treated with 4,5-dichloro-2-n-octyl-4-isothiazolin-3-one was the subject of thermal degradation study. The study included burning isothiazolone treated wood under various temperatures with and without oxygen. The result showed that no harmful combustion products, such as polychlorinated dibenzo-p-dioxins, polychlorinated dibenzo-p-furans and polychlorinated biphenyls, were detected. These fin...
Bing Yu


A determination of the toxic level of ACQ2100 wood preservative for the powder post borer Lyctus brunneus (Stephens)
1994 - IRG/WP 94-20029
The sapwood of two Lyctus susceptible Australian hardwoods, messmate (Eucalyptus obliqua L'Herit.) and black bean (Castanospermum australe A. Cunn. et Fraser ex Hook) were pressure impregnated with ACQ2100, a wood preservative, to produce replicates of a range of retentions. Preservative retentions were determined by solution weight uptake at treatment and chemical analyses of selected sa...
A R Moffat


Hole delimination inside round timber via ultrasonic techniques
1990 - IRG/WP 2358
A fast and economic circular scanning method to localize and evaluate holes inside round timber is presented. This method consists in measuring transit times of the ultrasonic wave by fixing the transmitter probe in the perimeter of the sample, then moving the receiver probe every ten degrees until completion of the circle. The scanning is done with a cheap and light instrument. Tests are made wit...
G Prieto, A Fernández Cancio


Quantitative Determination of Cyproconazole in Wood treated with Tanalith CY
2007 - IRG/WP 07-20369
The HPLC method has been widely applied to quantitative determination of cyproconazole in preservative solutions. However, HPLC assay has not been successfully employed to determine cyproconazole content in treated wood. Some extractives from treated wood hinder cyproconazole determination because they have a similar retention time to that of cyproconazole on an HPLC chromatogram. In addition, ...
I Momohara, T Miyauchi, M Mori


Determination of the lethal dose of fipronil for workers of Coptotermes formosanus (Isoptera: Rhinotermitidae
2007 - IRG/WP 07-10616
This document is a combination of two articles previously submitted to the journal, Sociobiology. Lethal dose of fipronil was determined in two experiments: topical application and contact with treated sandy loam. In the topical application the toxicity of fipronil was evaluated against workers of a laboratory colony of Coptotermes formosanus Shiraki. Fipronil was applied by the microsyringe to t...
K Tsunoda, R Yamaoka


The uses of Molecular techniques in studying Australian subterranean termites Genus Coptotermes
2008 - IRG/WP 08-10669
This study focuses on applying molecular tools in studying the phylogeny of the Coptotermes, especially from the Australian region, by using a combined data set of three mitochondrial genes, viz. 16S, COII, COI, comprising a total of about 2000 base pairs. This study will address these following specific questions: i. Does molecular phylogenetics reveal any new species and show any previously ...
H M Badawi, B M Ahmed (Shiday), J R J French, M P Schwarz


Termite taxonomy and distribution with particular reference to climate change in Africa
2010 - IRG/WP 10-10738
Termites constitute an integral component of various ecosystems in Africa. Termites are also amongst the most difficult of the insects to study because of their cryptic behaviour. There are around 2600 species of termites (Isoptera) in 280 genera which have been described worldwide and about 39% of the total termite species are found in Africa. Some termite species are well known pests of agricul...
P O Y Nkunika, B M Ahmed Shiday, G W Sileshi, J R J French, P Nyeko, S Jain


Determination of a fixation time of wood preservatives: A discussion paper
2010 - IRG/WP 10-20436
The intention of that paper is to initiate a discussion on the basis of a French method in combination with a German approach regarding the need of a method for the determination of a fixation time and especially to obtain input as well as ideas concerning a possible test design. Since no harmonised European approach exists up to now concerning the determination of a fixation time, CEN TC 38 (2009...
E Raphalen, E Melcher


Service life prediction of wooden components – Part 1: Determination of dose-response functions for above ground decay
2010 - IRG/WP 10-20439
Scots pine sapwood (Pinus sylvestris L.) and Douglas fir heartwood (Pseudotsuga menziesii Franco) specimens were exposed in double layer field trials at 24 different European test sites under different exposure conditions (in total 28 test sets). The material climate in terms of wood moisture content (MC) and wood temperature was automatically recorded over a period of up to eight years and compar...
C Brischke, A O Rapp


TMT–Interlab–Test to establish suitable quality control techniques - Structure and first results
2010 - IRG/WP 10-40503
As a result of growing quality demands from manufacturers and end-consumers of thermally modified timber (TMT) recent scientific research activities are increasingly focussed on modification mechanisms and by this on the development of suitable quality control methods. To deepen the knowledge in modification mechanisms and to obtain a larger variety of scientific data for TMT depending on the trea...
C R Welzbacher


Determination of Equilibrium Moisture Content (EMC) of wood in the neighboring Countries of Iran
2011 - IRG/WP 10-40540
The mean value of annual temperature and relative humidity of 33 cities in Azerbaijan, Armenia, Turkmenistan, Afghanistan, Pakistan, Oman, United Arab Emirates, Bahrain, Qatar, Kuwait, Iraq and Turkey were determined using climatic data of the past 11 years. The EMC values were calculated using the Hailwood-Horrobin sorption model and its annual fluctuation, together with Temperature and relati...
A A Enayati, H Z Hosseinabadi


Thermally modified timber (TMT) for decking applications – determination of relevant surface properties
2011 - IRG/WP 11-40544
In recent years thermally modified timber (TMT) entered various market segments. It is used for facades, horticultural equipment, garden furniture, and also for kitchen and bathroom cabinets. However, flooring turned out to be the most important application for TMT, either as interior parquet or as exterior decking. Besides durability and dimensional stability, which had been the initial target pr...
L Meyer, C Brischke, C R Welzbacher


Determination of Izod Impact Strength on Wood: A Suitable Method to Detect Fungal Decay in Protective Effectiveness-Screenings of Wood Preservatives
2012 - IRG/WP 12-20484
For testing a large number of different substances regarding fungicide properties, the reduction of the decay test duration is advantageous. In the present paper the suitability of a method for testing plastics using an impact testing machine was examined. The results clearly show that the fungal attack of European beech by the white-rot fungus Trametes versicolor leads to a decrease of izod imp...
H Delenk, M Zauer, A Wagenführ


NIR spectroscopy for rapid determination of permethrin or bifenthrin retention in P. radiata sapwood
2013 - IRG/WP 13-20507
Near infrared spectroscopy of permethrin or bifenthrin treated radiata pine (P. radiata D.Don) has been used to develop calibration models to later predict the active retention in unknown samples. Calibrations were developed for both a laboratory NIR and a portable NIR using laboratory-prepared calibration samples at a range of target retention levels. Correlations were established between the act...
R Meder, N Ebdon


Determination of the natural durability of solid wood against wood-destroying fungi - a European round-robin test
2013 - IRG/WP 13-20511
In Europe the durability of wood against wood-destroying basidiomycetes is tested according to CEN/TS 15083-1 (2005). Hitherto existing experience with this standard is quite heterogeneous and results from previous round-robin tests have stayed unreported or have been reported incompletely. In particular the need for natural pre-weathering of the test specimens to allow potential detoxification of...
C Brischke, C R Welzbacher, A Gellerich, S Bollmus, M Humar, K Plaschkies, W Scheiding, G Alfredsen, J Van Acker, I De Windt


Developing Analytical Methods for Determination of Quaternary Ammonium Compounds (DDAC) using HPLC and HPLC-MS (Application to treating solution and preservatives treated wood)
2013 - IRG/WP 13-20516
Korea preservative treating industry has mainly used alkaline copper quaternary (ACQ) expected over 80% of market share in Korea. ACQ employs dodecyl dimethyl ammonium chloride (DDAC) and benzyl dimethyl dodecyl ammonium chloride (DBAC) for active ingredient along with copper. The strongly increasing domestic applications for wood preservatives require developing accurate and reproducible analytic...
Sung-Mo Kang, Kwon-Min Kim, Won-Mo Koo, Myeong-Won Cho


Extraction and analysis of DNA from green and seasoned timber as basic methods for determination of wood species and origin
2013 - IRG/WP 13-20523
Against the background of the European timber trade regulation EUTR, commenced to law by March 2013, the determination of wood species and tracing of its origin is getting a great importance. A promising approach for establishing fast and reliable tracking systems for wood products is DNA analysis. A critical point is the extraction of analysable DNA from the wood and its lignified cell walls. Thu...
K Jacobs, H Mende, W Scheiding


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