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Assessment of the Envelope Effect of Three Hot Oil Treatments: Resistance to Decay by Coniophora puteana and Postia placenta
2006 - IRG/WP 06-40344
Timber of Corsican pine (Pinus nigra var. maritima) and Norway spruce (Picea abies) was treated in hot linseed oil, rapeseed oil and a proprietary resin derived from linseed oil. The samples were immersed in oil or resin under reduced pressure at temperatures of 180°C and 200°C. Very high uptakes of the oils or resin were recorded for pine, while spruce showed lower weight percent gains, below 20%. Treated blocks were exposed to two brown rot fungi, Coniophora puteana (BAM 15) and Postia placenta (FPRL 280). The effect of using a therm-oxidatively cured resin or a drying oil (linseed) was compared with the use of the non-drying rapeseed oil. The resin treated blocks had a lower weight loss at the end of the experiment than blocks from the two oil treatments. It is believed that the polymerization of the resin immediately after treatment assists in reducing the accessibility of the timber to fungal decay. To assess the extent to which this is an envelope treatment, a simple variation on the BS EN113 test method was used to expose untreated surfaces. Sticks of timber which had been treated with the linseed oil or the resin were crosscut to expose un-cured faces on the end grain, and exposed to fungi in the same manner as the standard EN113 test. The effect of cutting open the envelope treatment was an increase in weight loss when compared to the equivalent fully sealed blocks.
M J Spear, C A S Hill, S F Curling, D Jones, M D C Hale

Development of Wood Modification – High melting point wax and hot oil treatments
2016 - IRG/WP 16-40768
This study covers an introduction to the projects where new facilities were created for developing wood modification. In this new research environment it is possible to treat wood with versatile equipment. First modifications with this equipment are going to be done in high temperature and pressure using high melting point waxes and hot oils. Earlier studies, tests and commercial products show that different waxes and oils can be used to treat and impregnate wood. Goal of this study is to find out promising process parameters and suitable high melting point waxes and oils to modify products those are made out of most common Nordic timber species.
H Turunen, L Linkosalmi, J Peura, O Paajanen

Principles and procedure of the planeing test
1981 - IRG/WP 2162
Small end-sealed samples of pine-sapwood (1.5 x 2.5 x 5 cm³) are treated by brushing and afterwards different parts of the treated surface are removed. The remaining part of the sample is tested against either insects or fungi. If no attack occurs sufficient amounts of biocides have been penetrated at least beyond the zone which has been removed. In spite of some problems the test seems the only suitable method, to evaluate organic solvent preservatives, mainly those containing resins, for simple treating methods.
H Willeitner, M Gersonde

Effects of various preservative treatments on the mechanical and physical properties of plywood
1993 - IRG/WP 93-40007
The technical properties of plywood are related to both the intrinsic characteristics of its composing wood species and the quality and performance of the glue bond which acts as an interface between veneer sheets. Consequently mechanical and physical testing and glue bond strength analysis offer an appropriate means for studying the effect of preservative treatments on the overall quality of plywood. A range of boards was treated with waterborne and oilborne preservatives. Changes in modulus of elasticity, modulus of rupture and tensile strength were noted as well as variations in physical properties. Analysis of the glue bond strength was done by shear strength testing and determination of the amount of wood failure after different ageing procedures.
J Van Acker, M Stevens

Preventing fungal attack of freshly sawn lumber using cinnamon extracts
2007 - IRG/WP 07-30432
The potential for using cinnamon oil as an anti-mold and stain compound was investigated on ponderosa pine sapwood. Cinnamon oil was highly effective when used in ethanol, but its activity declined when it was mixed with only water. Attempts to enhance water solubility with surfactants improved solution stability, but had no apparent effect on biological activity. Further studies with other co-solvents are planned
Shujun Li, C Freitag, J J Morrell

Remedial treatment of wood attacked by insects
1981 - IRG/WP 3175
A review is presented of remedial treatments against wood-boring insects in wood in service. Preconditions and fundamental principles of insect control are compared with the control of fungal attack and reasons are given for the fact that remedial treatments against insects are more commonly applied than against fungi. With regard to insect control measures with a simultaneous preventive effectiveness, information is given on preservatives, control measures as well as on testing the effectiveness of preservatives with eradicant action. An evaluation of 40 tests according to EN 22 or DIN 52164 revealed that a mean depth of effectiveness of 15 mm is obtained at mortality rates of 80-84% of Hylotrupes larvae. At a mortality rate of below 75% the mean depth of effectiveness was about 10 mm and above 90% it was about 27 mm. Among the control measures without any preventive effectiveness fumigation and hot-air treatments are referred to. With regard to biological control measures, practical results are not yet available.
H Kühne

Effects of surfactants and ultrasonic energy on the treatment of wood with chromated copper arsenate
1977 - IRG/WP 3108
Sugar pine stakes 1'' x 1" x 16" were treated by a hot-water bath followed by soaking in cold CCA solution for 10 to 30 minutes. A similar number of stakes were treated by a cold-cold bath. Half of the stakes were subjected to ultrasonic energy during the CCA bath. The mean absorption for stakes given the hot-cold bath was 18.52 pcf (297 kg/m³) and 4.64 pcf (74 kg/m³) for those given the cold-cold bath. The rates of absorption were o.323 pcf (5 kg/m³) per minute and 0.053 pcf (0.85 kg/m³) per minute, respectively. The relationship between absorption in pounds per cubic foot (Y) and soaking time in minutes (X); Y = 12.27+0.323 X, was linear and significant. The linear relationship for the cold-cold treatment was poor (r = 0.305). Neither ultrasonic energy, nor its interaction with soaking time, had a significant effect on solution absorption for either the hot-cold or cold-cold treatments. In a second series, the stakes were treated in the CCA solution with a 3-minute dip, a 48-hour cold soak, and Lowry pressure. Half of the stakes were treated in the solution to which a surfactant had been added. The interacting effect of surfactant and method of treatment was significant. The highest absorption was obtained when the specimens were treated with the solution containing the surfactant by the Lowry method, 35.13 pcf (563 kg/m³). In comparison, the absorption was 22.55 pcf (361 kg/m³), 36 percent lower, when surfactant was not used. The surfactant had a beneficial effect on the results of the 3-minute dip, but not the 48-hour soak.
C S Walters

Properties of hot oil treated wood and the possible chemical reactions between wood and soybean oil during heat treatment
2005 - IRG/WP 05-40304
Thermal treatment with hot oil as the heating media based on the original idea from oil-heat treatment in Germany was investigated. The treatment was mainly carried out at 200ºC and 220ºC for 2 hours and 4 hours, and the wood species were mainly spruce and fir. This paper focuses on the difference between soybean oil and palm oil and the possible chemical reactions between wood and soybean oil. Generally palm oil was slightly better than soybean oil in improving the moisture resistance properties of heat-treated wood. But soybean oil treated wood appeared to have better decay and mould resistance. The mass loss of wood treated in soybean oil at 220ºC for 4 hours was below 20 % after exposure to Gloeophyllum trabeum in a soil block test, so the treated wood can be classified as “Resistant” according to ASTM D 2017 standards. Natural weathering exposure also shows that soybean oil treated wood is more mould resistant than palm oil treated wood. In order to investigate the effects of absorbed oil on the properties of treated wood and the possible reactions between wood and oils, extraction of different vegetable oil treated wood with chloroform and other solvents was carried out. The results suggest that part of the soybean oil could undergo chemical reactions with wood that renders it of low extractability.
Jieying Wang, P A Cooper

The effect of oil-borne preservative treatments on the shear strength of FRP/wood composite adhesive bonds
2003 - IRG/WP 03-40265
Reinforcement of structural wood components with Fiber Reinforced Polymer (FRP) will enhance the beam’s strength, but actual data on long-term durability is sparse, not well documented or not readily accessible. In this study, bond properties of FRP-wood composite materials were investigated following treatment with creosote or copper naphthenate preservatives. The properties investigated included stress and the percentage of wood failure experienced in shear (ASTM 1998). When tested in a wet condition (following a vacuum/pressure soak), creosote-treatment adversely affected the wood failure values associated with specimens fabricated with a pultruded FRP composite sheet (E-glass fiber, bonded with urethane). When these tests were conducted with samples under ambient conditions, the shear strength of this material was also adversely affected by creosote. In addition, both creosote- and copper napthenate-treatment adversely affected the shear strength of a SCRIMP™ fabricated FRP material (carbon fiber, vinyl ester matrix).
B Herzog, B Goodell, R Lopez-Anido

Application of paint primers after light organic solvent preservative treatment
1986 - IRG/WP 3381
The application of three alternative paint primers is investigated, including a slow-drying oil-based primer, a fast-drying oil-based primer, and a fast-drying water-based primer. The treatment schedules employed, in particular the evacuation period after treatment, have a marked effect on subsequent paintability. Priming can potentially be carried out immediately after treatment with approved Timber Preservation Authority schedules, providing that (1) a fast-drying primer is employed (either water-based or oil-based), (2) solvent recovery by evacuation is continued for an extended period (45 min, c. -85 kPa) immediately after treatment, and (3) either the Lowry or the Bethell process is employed.
P Vinden

Characterizing long term leaching behaviour of copper from preservative treated wood in a practical exposure scenario
2011 - IRG/WP 11-50278
To investigate the prediction of the long term emission of copper from preservative treated wood in a Use Class Class 3 scenario, treated boards were exposed vertically above ground to natural weather conditions. The study included two products; an amine copper ACQ-type formulation, air-dried after treatment to a 22 kg/m3 retention, and the same formulation which was hot oil vacuum dried after treatment. During a six year study period run-off emissates were continuously collected and their content of copper determined by chemical analysis at intervals. The total emission of copper was approximately 2 g/m2 exposed wood for the ACQ treated, air dried boards whereas the hot oil vacuum dried boards had a copper emission which was ten times lower at 0.2 g/m2 in total after six years. Approximately 50 % more leachate was collected from underneath hot oil dried boards, presumably due to increased water repellency of the oil treated surface; this is considered to be the reason for the reduced emission of copper. The prediction of long term emission after six years was possible from short term measurements after two years, using logarithmic extrapolation.
T Mark Venås, M Klamer

Tar-oil uptake vs time in immersion treatment of short pine posts: A simple technique applicable to rural communities of Papua New Guinea
2012 - IRG/WP 12-40608
Pinus caribaea and Araucaria cunninghamii logs ca. 100 mm in diameter were shortened to lengths 25-30 cm, conditioned to at/below fibre saturation point (FSP) for immersion/dip treatment using a hot- and- cold bath open- tank process. Before oven-drying and subsequent treatment, individual test specimens were numbered, their green weights and volumes, and dry weights recorded for basic density, void volume, preservative uptake and retention determination. The poles were bundled and immersed (dipped) in a drum containing light tar-oil creosote. The tar-oil creosote with pine specimens was heated to boiling for 30 minutes and flames were extinguished with water to allow cooling. The cooling conditions, (dip time period for treatment) varied from 1, 5, 15 and 24 hours. Theoretically, a vacuum was created in wood during heating and when cooled, tar-oil was drawn into the wood’s anatomical structures. The experiment results indicated that tar-oil uptake and retention increased with dip time until available void volume was filled and no further uptake occurred. In this case, the preservative uptake and retention were proportional with square-root of dip time. The technique was simple with basic materials required for hot and cold bath treatment. This treatment technique is more appropriate for application at rural community level for treatment of utility posts/poles.
B K Gusamo, R Tulo

Termiticidal Effect of Bitumen and Creosote oil Treatments on Selected Nigerian Wood Species
2016 - IRG/WP 16-30689
Termites attack has been a major threat to wood materials in construction. The study investigated the termiticidal effect of bitumen and creosote oil mixture on the resistance of some commonly used indigenous wood species namely: Celtis zenkeri, Terminalia ivorensis, Albizia lebbeck, Cola gigantea and Terminalia superba to termites in Akure, Ondo State, Nigeria. The wood species were obtained from a sawmill in Akure South Local Government Area of Ondo State, Nigeria. The wood samples were separated into five samples each for sap and heartwood using 35 × 35 × 450 mm dimension. Thereafter, they were treated with mixture of bitumen and creosote using hot treatment method. The preservative absorption by the wood samples was determined, coupled with the weight loss of the wood after exposure to termites’ attack in the graveyard for 12 months. Macrotermes sybhylinus was identified as dominating termite species in Akure environ. Weekly visual observations of the stakes were carried out as specified in ASTM D3345-80 Standards for 12 months. The wood samples were withdrawn after 12 months of exposure to termites and weight loss due to attack was estimated. The field test results showed that treatment with bitumen and creosote oil mixture greatly increased the resistance of the five wood species to termites attack. It was also observed that heartwood portion of wood species were resistant to termites attack. The Analysis of variance indicated that there was significant difference between the resistance of treated and untreated samples at 5 % level of significance. From the results obtained, it was evident that bitumen and creosote oil mixture in 70:30 proportions proved very effective as a preservative for protecting wood against termites attack.
Termiticidal Effect of Bitumen and Creosote oil Treatments on Selected Nigerian Wood Species

Proposed method for out-of-ground contact trials of exterior joinery protection systems
1981 - IRG/WP 2157
Methods for testing the efficacy of preservative treatments for exterior joinery are described using the format of a European Standard. Commercially used treatments applied to jointed test units (L-joints) which are then protected by conventional finishes are exposed to normal outdoor hazards out of ground contact. Assessment is made a) by determining eventual failure through decay and b) by destructive examination of replicate treated and untreated units, after increasing time intervals, rating comparative performance in terms of wood permeability increase and the progress of microbial colonisation.
J K Carey, D F Purslow, J G Savory

Comparative response of Reticulitermes flavipes and Coptotermes formosanus to borate soil treatments
1991 - IRG/WP 1486
Eastern (Reticulitermes flavipes [Kollarl]) and Formosan (Coptotermes formosanus Shiraki) subterranean termite workers (Isoptera: Rhinotermitidae) were exposed to borate-treated sand in an indirect exposure tunneling assay in the laboratory. In the ten day assay period, both termite species readily penetrated sand containing 5000, 10000, or 15000 ppm (wt. of compound / wt. of sand) disodium octaborate tetrahydrate (Tim-BorÒ) or zinc borate (Firebrake ZB-FineÒ). With Reticulitermes flavipes, significant mortality (85-93%) resulted from workers tunneling through sand treated with 5000 ppm disodium octaborate tetrahydrate (higher concentrations were also effective), or 15000 ppm zinc borate. Responses of Coptotermes formosanus workers were lesser and more variable, with only concentrations of 10000 and 15000 ppm zinc borate resulting in mortality 70-89%) significantly different from that in the control groups. These results suggest that differences between these two species in tunneling behavior may reduce exposure of Coptotermes formosanus to the borate-treated sand.
J K Grace

Granitgard used as a partial and perimeter barrier in the protection of buildings against subterranean termites
1995 - IRG/WP 95-10114
The graded granite subterranean termite physical barrier, commercially marketed as Granitgard, has a Certificate of National Accreditation issued by the Australian Building Codes Board, and is included in Australian Standards. After several years in developing the specifications and installation techniques for Granitgard, it may be used to protect almost all footing designs. Granitgard can be simply placed around slab penetrations and buildings perimeters to provide a durable, long-life subterranean termite barrier. This paper discusses the development of partial and perimeter applications of Granitgard around buildings, and the advantages of using a termite barrier that removes the need for costly and dangerous chemical retreatments.
D M Ewart, J R J French

IRG/COIPM INTERNATIONAL MARINE TEST - to determine the effect of timber substrate on the effectiveness of water-borne salt preservatives in sea-water. Progress Report 2: Report of treatment and installation in Australia
1978 - IRG/WP 440
The purpose of this test and the procedures to be followed have been fully set out in documents distributed by the International Research Group on Wood Preservation and numbered IRG/WP/414 and IRG/WP/420. The prescriptions set out in these two documents have been closely followed.
J Beesley

Field test evaluation of preservatives and treatment methods for fence posts
1985 - IRG/WP 3347
This work presents the field test results after fifteen years exposure of Eucalyptus saligna fence posts treated with six different preservatives and five treatment methods. All the combinations with oil-borne preservatives presented the best results and among the waterborne preservatives, the fence posts treated by immersion method were with the lowest performance in the field test.
G A C Lopez, E S Lepage

Pinus and Eucalyptus fenceposts treated with creosote and solvex tar by hot and cold open-tank process
1987 - IRG/WP 3455
A comparative study of the behaviour of two different wood preservatives, creosote and solvex-tar, was made, using two wood species, Pinus pinaster Ait and Eucalyptus globulus Labill, by the hot and cold open-tank process. Results showed that the creosote behaved better in relation with the uniformity of its distribution in wood. On the other hand, better results were obtained on Pinus for both preservatives.
M V Baonza Merino

Soft rot penetration - Effect of groundline maintenance treatment on poles in sevice
1983 - IRG/WP 3263
R S Johnstone

Progress towards controlling soft rot of treated hardwood poles in Australia
1977 - IRG/WP 289
H Greaves

Protocol for evaluation and approving new wood preservative
1985 - IRG/WP 2159
M E Hedley, J A Butcher

Field tests out of ground contact in France: Definition of the test procedure and preliminary results after 18 months
1981 - IRG/WP 2161
M Fougerousse

Dimensional stability and decay resistance of hot-melt self-bonded particleboard by surface benzylated pine chips
1991 - IRG/WP 3652
Akamatsu (Pinus densiflora Sieb. et Zucc: Japanese red pine) particles were pretreated with 40% NaOH solution and benzylated with benzyl chloride, and the surface of particle was converted into meltable materials. Hot-melt self bonded particleboard having smooth and high glossiness surface was prepared by hot pressing at 150°C and 1.96 MPa without using any conventional adhesives. Dimensional stability and decay resistance of the benzylated particleboard were evaluated. Particleboards made of benzylated particles having more than 38% of weight percent gain (WPG) showed that dimensional stability and decay resistance were superior to the conventional particleboard made by using phenolformaldehyde resin as a binder, because hydroxyl groups of wood were substituted by hydrophobic benzyl groups with benzylation. Though bending strength of the board was a little lower than control board due to the damage of benzylated particles during benzylation, its internal bonding strength was very high, because the hot-melting strengthened the inter-particle bonding.
M Kiguchi, K Yamamoto

Fire resistance of preservative treated fence posts
1994 - IRG/WP 94-30033
Pine fence posts were pressure treated separately with CCA-C, CCA-wax, CCA-oil and creosote. Treated posts and untreated controls were planted in the ground in a randomised block design, weathered for six months and then subjected to a controlled burning test using two fuel loads. Creosote treatment increased the time that posts were alight whereas CCA treatment had no such effect. However, CCA treated posts smouldered until destruction of the majority of the posts occurred. Posts treated with CCA-oil took longer for destruction to occur than posts treated with CCA-C or CCA-wax. Creosote treated posts and untreated controls did not show prolonged smouldering and consequently were not destroyed by the burning test, although their strength was reduced. A high fuel load increased the time that posts were alight and smouldering, and for CCA treated posts decreased their time to destruction.
P D Evans, P J Beutel, C F Donnelly, R B Cunningham

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