IRG Documents Database and Compendium


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Detection of incipient brown rot decay in wood by fourier transform infrared spectrometry
1987 - IRG/WP 2275
Fourier transform infrared spectrometry was evaluated as a possible method for detecting different levels of brown-rot decay in pine sapwood. By using first derivative spectra and regression analysis, an equation based on 4 absorption peaks, normalized with an internal standard peak, was developed. The correlation between weight loss and absorption was highly significant indicating that this is a ...
D D Nicholas, T Schultz


Investigation of chemical changes in acetylated beech wood during weathering
2009 - IRG/WP 09-40460
In this study Beech wood (Fagus orientalis) acetylated and has been subjected to a variety of artificial weathering conditions (water only, light only, water and light together)in difference times (0,50,150 and 300 h), then wood surface analyzed using Fourier Transform Infrared spectroscopy (FTIR).Results shown that weathering process affected the functional groups on the wood surface. Light and w...
M Akhtari, M Arefkhani


Rapid detection of the Alaska yellow cedar, Callitropsis nootkatensis (Cupressaceae) extractives using Fourier transform infrared (FT-IR) spectroscopy
2017 - IRG/WP 17-20612
Global changes in wood harvesting towards plantation species grown on much shorter rotations has the potential to markedly alter wood quality perceptions. Nowhere is this more risky than with naturally durable species where there is compelling evidence that faster grown woods tend to be less durable. The ability to non-destructively assess durability may allow growers to identify materials that re...
S Lipeh, J J Morrell


Classification of wood materials using Fourier Transform Near Infrared Spectroscopy and multivariate analysis
2011 - IRG/WP 11-20471
A distinction between preservative-treated wood and non-treated wood can be demonstrated by the combination of Fourier Transform-Near Infrared Spectroscopy (FT-NIRS) and Multivariate Analysis (MVA). This technique is non-destructive, quick, easy to use and can be portable. The calibration models for different heavy metals are set up using principal component analysis (PCA) to classify species of t...
M A Bouslamti, M A Irle, C Belloncle, V Salvador, S Hulot, B Caron, E M Qannan


Photo-discoloration and Degradation of Wood and its Stabilisation by Modification with Benzoyl Chloride
2004 - IRG/WP 04-40274
Photo degradation of Pinus roxburghii (chir pine) and Hevea brasiliensis (rubber wood) was studied under artificial accelerated weathering conditions in a Xenon test chamber. The irradiated samples were analyzed for color changes and chemical changes. Analysis of colour changes in wood surfaces by UV-Vis. irradiation was carried out using a colour measuring (CIELAB) system and chemical changes ...
K K Pandey


Prediction of Weight Percent Gain (WPG) of furfurylated wood by FT-NIR spectroscopy
2004 - IRG/WP 04-20295
Wood modification based on furfuryl alcohol improves several important wood properties, such as the resistance to fungal decay and insect attack, hardness, dimensional stability, bending strength and stiffness. The improvements of wood properties depend on the weight percent gain (WPG) due to furfurylation. Fourier transform near infrared (FT-NIR) spectroscopy was used to calibrate PLS-regression ...
M Eikenes, P O Flæte, E Ystrøm Haartveit, S Lande


Correlation between changes in colour and chemical composition during photo-degradation of wood surfaces
2005 - IRG/WP 05-40301
Changes in colour of wood (yellowing) during photo degradation or weathering reflect chemical changes in wood. Therefore, the relationship between changes in chemical composition and CIELAB colour parameters is very important to characterize photodegradation of lignocellulosic surfaces. In this study, the changes in chemical composition and yellowing due to photo-degradation was studied by expos...
K K Pandey


Longterm monitoring of termite activity on multiple feeding sites: a laboratory method intended for the determination of attractant/repellent properties of wood preservatives and baits
2001 - IRG/WP 01-20225
A method is introduced allowing the continuous monitoring of the activity of a small laboratory termite- colony at 8 different feeding sites simultaneously. The test assembly consists of a small central polycarbonate-tube containing a colonie of Reticulitermes santonensis (de Feytaud) beeing connected with 8 external feeding sites by small glass-capillaries. The termites passing through the glass ...
M Pallaske, E Graf, H Takiuchi


The influence of copper (II) chemicals on the weathering of treated wood. Part 1: ACQ treatment of wood on its weathering
1994 - IRG/WP 94-30040
Wood weathering can be accelerated by alkylammonium compound (AAC) treatment, and slowed by ammoniacal copper quat (ACQ) treatment. This study aims at investigating the influence of ACQ treatment of wood, especially the present of copper (II), on its weathering. ACQ, CCA and DDAC treated microtomed sections of southern yellow pine earlywood were prepared and naturally weathered for five periods, t...
Ruiying Liu, J N R Ruddick, L Jin


Analysis of water repellents in wood treated with water borne formulations using FTIR
2000 - IRG/WP 00-40176
The use of aqueous water repellent emulsion formulations has increased significantly in the wood treatment industry. These products are primarily used to enhance the weathering characteristics of wood products treated with water borne preservatives systems used in exterior above ground applications. They are also used in pole treatments to improve climbing characteristics and in low VOC millwork t...
P J Walcheski, L Jin


NIR spectroscopy for rapid estimation of decay resistance
2004 - IRG/WP 04-20294
In Scandinavia Scots pine (Pinus sylvestris L.) is an important commercial tree species. Its heartwood has traditionally been used in constructions exposed to risk of decay. In a laboratory experiment Scots pine wood specimens sampled from inner heartwood, outer heartwood and sapwood were exposed to the brown rot fungus Poria placenta. In general outer heartwood was more resistant than inner heart...
P O Flæte, E Ystrøm Haartveit


Rapid loss of lignin at wood surfaces during natural weathering
1992 - IRG/WP 92-2390
Thin veneers of radiata pine (Pinus radiata D. Don) were exposed to natural weathering over a period of 30 days. Incident UV radiation was monitored at the test site. FTIR internal reflectance spectroscopy was used to study the chemical changes taking place at the veneer surface during weathering. Spectra obtained show that after only 3 days exposure there was substantial delignification at veneer...
P D Evans, K J Schmalzl, A J Michell


Weathering of copper-amine treated wood
2000 - IRG/WP 00-40155
Copper ethanolamine (Cu-EA) treated southern pine (SP) were artificially weathered with a QUV Weathering Tester. The weathering regime was composed of a continuous UV-light irradiation for 2 hours followed by a water spray for 18 minutes for a total time of 1200 hours. The changes on the surface of the weathered samples were characterized by Fourier transform infrared spectroscopy (FTIR) analysis,...
J Zhang, D P Kamdem


Differentiation of Scots pine heartwood and sapwood by near infrared spectroscopy
2003 - IRG/WP 03-10459
In Scandinavia Scots pine heartwood has, in recent years, gained popularity as material for external structures exposed to moderate risk of decay. As non-durable sapwood surrounds the heartwood in pine trunks it is of crucial importance to separate this wood from the heartwood during log processing into heartwood products. Heartwood and sapwood can be differentiated by visual evaluation of colour ...
P O Flæte, E Ystrøm Haartveit


Surface characteristics of wood treated with various AAC, ACQ and CCA formulations after weathering
1991 - IRG/WP 2369
Wood samples treated with various alkylammonium compounds (AACs) as well as ammoniacal copper quat (ACQ) and chromated copper arsenate (CCA) have been studied in accelerated weathering experiments. Microscopic examination of the surfaces of these samples after exposure in a weatherometer revealed several different changes. Samples treated with didecyldimethyl ammonium chloride (DDAC) show consider...
L Jin, K J Archer, A F Preston


FTIR characterization of copper ethanolamine - wood interaction
1999 - IRG/WP 99-20154
The interaction of copper ethanolamine (Cu-EA) and wood components was studied by using Fourier transform infrared spectroscopy (FTIR). In Cu-EA treated wood, significant reduction was noticed on the band attributed to carbonyl vibration from carboxylic groups at 1735±5 cm-1 and an increase in band intensity was obtained from carbonyl in carboxylate at 1595±5 cm-1. The same observation was made ...
Jun Zhang, D P Kamdem


A spectroscopic investigation of copper ethylenediamine fixation in wood
1999 - IRG/WP 99-20160
The fixation reaction which take place between copper ethylenediamine (Cu-en) solution and wood were expolored using X-ray photoelectron spectroscopy (XPS) and Fourier Transformed Infrared Spectroscopy (FTIR). The FTIR spectra revealed that copper reacts with the carboxylic acid and phenolic groups in wood to form stable complexes. The copper ethylenediamine complexes formed in wood were identifie...
Xiao Jiang, J N R Ruddick


FTIR studies on the weathering of didecyldimethylammonium compound (DDAC) treated wood
1993 - IRG/WP 93-30013
Wood treated with alkylammonium compounds (AACs), such as DDAC, weathered more rapidly than untreated wood. In order to examine the influence of DDAC treatment of wood on its weathering, treated and untreated microtomed sections of southern yellow pine earlywood of various thicknesses, were prepared and weathered for approximately one month. The changes in these samples were monitored using FTIR. ...
R Liu, J N R Ruddick


A comparison of analytical and visual techniques used for assessment of weathering properties of chromium and copper azole treated timber
1994 - IRG/WP 94-20023
The weathering properties of preservative treated timber were studied by measuring surface lignin loss and by microscopic examination after weathering, and results were related to qualitative assessments of visual appearance after weathering. Measurement of relative rates of delignification of untreated and preservative treated timber obtained by FTIR analysis, and weight loss determined on thin v...
J A Cornfield, M D C Hale, G Fettis


Correlation between modulus of elasticity, mass losses and FTIR spectra of copper treated decayed wood
2006 - IRG/WP 06-10580
The composition of copper-based preservatives will change from copper-chromium to copper-ethanolamine, due to environmental demands. The most important drawback of copper-impregnated wood is the presence of tolerant fungal organisms that have developed an ability to degrade such preserved wood. In order to elucidate these processes, specimens (0.5×1.0×15 cm) made of Norway spruce (Picea abies) w...
M Humar, B Bucar, F Pohleven


Qualitative and quantitative assessment of chemicals used for wood durability improvement by Near Infrared Spectroscopy
2006 - IRG/WP 06-20349
The Near infrared spectroscopy (NIRS) could be a suitable technique to assess chemicals used for wood durability improvement in the forest products industry. NIRS methodology can be used to obtain results more quickly, less costly and without damaging the wood. In this study, wood samples selected from heartwood and sapwood of Maritime Pine (Pinus pinaster) were prepared to assess the artificial d...
S Zahri, F Charrier, H Baillères, B Charrier


Multivariate analysis of infrared spectra for the prediction of the mechanical performance and dimensional stability of thermally modified wood
2007 - IRG/WP 07-40367
The use of calibrated mid-infrared Fourier transform (FTIR) spectroscopy for predicting the main bending strength parameters of thermally modified wood is described for the first time. The analysis is based on the handling of OSC-filtered FTIR data from control and treated wood samples, using partial least squares (PLS) regression. Sets of Norway spruce, Scots pine and Beech wood samples were th...
M M González-Peña, M D C Hale


Influence of ring width and wood density on durability of oak heartwood
2008 - IRG/WP 08-10639
Oak (Quercus sp.) is considered as one of the most durable European wood species. The most important factor influencing oak durability was extractive content. In our work, we were interested in if oak-wood durability is affected by ring-width and related density. Therefore, oak heartwood specimens made of boards with different ring widths were exposed to five different fungal species Daedelea quer...
M Humar, P Oven, F Pohleven


Near infrared spectroscopy for the quantification of wood preservatives
2008 - IRG/WP 08-20391
Near infrared (NIR) spectroscopy is a rapid, flexible, inexpensive and non-destructive technology that has many applications, including the evaluation of many wood properties. Initial studies have indicated the potential to apply NIRS for the quantification of wood preservatives. However, further evaluation with borate and azole preservative systems has revealed that NIRS technology is challenged ...
A M Taylor, Seung H Baek, Myong K Jeong, J D Lloyd, J J Morrell


Vacuum drying of European oakwood: Color, chemistry and anti-oxidant potency of wood. Improving appearance in forest value added products
2008 - IRG/WP 08-40432
In hardwoods used for decorative and appearance purposes, wood colour is one of the most important factors of wood quality; in addition colour is related with durability and biological decay of wood. Wood discolouration during drying is mainly affected by heat, light, physiological reactions, combinations of reactions, biochemical and chemical reactions, and micro-organisms attack. In freshly fell...
S Sandoval, W Jomaa, F Marc, J-R Puiggali


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