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Utilization of thermodesorption coupled to GC-MS to study kinetics of thermodegradation of different wood species
2011 - IRG/WP 11-40559
Thermdesorption coupled to Gas Chromatography coupled to Mass Spectroscopy (TD-GC-MS) has been investigated to identify volatile degradation products generated during wood heat treatment by mild pyrolysis. For this purpose, wood samples of different softwood and hardwood species have been heat treated under nitrogen for different temperatures comprised between 180 and 230°C during 15 min. in the ...
K Candelier, M Chaouch, S Dumarçay, A Pétrissans, M Pétrissans, P Gérardin


Limited variability in biological durability of thermally modified timber using vacuum based technology
2011 - IRG/WP 11-40567
The SmartHeat® thermal timber treatment is a new technology based on the process parameters being steered very precisely mainly due to the vacuum applied and heating system involved. Timber treated with this technology shows a potential for less variability of biological durability in one batch. Several batch treatments were sampled and assessed on statistical variability of decay resistance agai...
J Van Acker, S Michon, J Van den Bulcke, I De Windt, B Van Swaay, M Stevens


Effects of nano-silver on brittleness of heat-treated solid woods
2011 - IRG/WP 11-40572
The present study is aimed at the effect of heat-treatment of normal as well as nano-silver-impregnated Populus nigra, Populus deltoides, and Fagus orientalis on brittleness. Specimens were impregnated with 200 ppm water-based solution of nano-silver particles under 3 bars in a pressure vessel using empty-cell process. For heat treatment, both nano-silver-impregnated and normal specimens were kept...
H Reza Taghiyari, B Moradi Malek, A Karimi


The overview of ISPM 15 implementation in Croatian wood-working companies
2011 - IRG/WP 11-30576
Croatia is a small European county, but in the same time a great country according to it’s tradition in the forestry and wood working industry. However, around 48% of it’s territory is afforested. As the export is one of the main directions in the Croatian development conception, the production and distribution of wood package intended for the international trade, is one of the most important ...
R Despot, V Jambrekovic, M Hasan


Effects of oil types and treatment temperature on the properties of wood subjected to thermal modification in oil medium
2012 - IRG/WP 12-40574
The effect of the use of oil as a medium of heat transfer during thermal modification of different species of wood has been widely investigated with different results accruing with regards to the various end-use properties of the materials. However very little have been done on the effect of oil types as well as its interaction with treatment temperature on the resultant properties of the material...
L Awoyemi, M M Apetogbor, A A Oteng-Amoako


Influence of heat treatment intensity on the structural integrity of 14 timber species
2012 - IRG/WP 12-40586
Thermally modified timber (TMT) is characterized by improved durability and dimensionally stability, but strength properties, especially the dynamic ones, are compromised at the same time. Because dynamic standard tests require high efforts and time, the high-energy multiple impact (HEMI) –test was developed for the fast and reliable characterisation of the structural integrity of TMT, showing a...
C R Welzbacher, C Brischke, G Maier


Relationships between heat treatment intensity and some conferred properties of different European softwood and hardwood species
2012 - IRG/WP 12-40593
Effect of treatment intensity on conferred properties like elemental composition, durability, anti swelling efficiency (ASE) and equilibrium moisture content (EMC) of different European softwood and hardwood species subjected to mild pyrolysis at 230°C under nitrogen for different durations has been investigated. Independently of the wood species studied, elemental composition is strongly correl...
M Chaouch, S Dumarçay, A Pétrissans, M Pétrissans, P Gérardin


The Effects of Industrial-Scale Heat Treatment and Impregnation with Boron Compounds on Water Uptake and Tangential Swelling of Some Wood Species
2012 - IRG/WP 12-40599
This study evaluated the effects of boron impregnation and heat treatment on water uptake and tangential swelling of spruce (Picea orientalis), pine (Pinus nigra), beech (Fagus orientalis) and poplar (Populus deltoides) wood species. The samples (10 x 5 x 40 - tangential x radial x longitudinal cm) were impregnated with 4 % boric acid and 4 % borax according to the ASTM D-1413 standard method. Aft...
A Can, S Yildiz, Ü C Yildiz


Development of a quality control assessment method to predict properties of heat treated wood
2012 - IRG/WP 12-40611
Heat treatment has been used to improve properties of non durable European species. Chemical modification of some of the wood components provides improved dimensional stability and biological performance against decay fungi while mechanical properties such as modulus of rupture are reduced. Quality control of commercially made thermally treated wood is one of the major challenges to allow its indu...
M Chaouch, K Candelier, S Dumarcay, A Pétrissans, M Pétrissans, P Gérardin


Differences between heat treated Pinus pinaster heartwood and sapwood
2012 - IRG/WP 12-40617
Heat treatment is a well known process to improve the durability and dimensional stability of less noble woods. The treatment can be applied for heartwood unlike the traditional treatments based on impregnation due to the difficulty of impregnating heartwood. Pure sapwood and pure heartwood samples were treated in an oven at 190ºC and 200ºC for 2h, 4h and 6h. Dimensional stability, measured a...
B Esteves, L Nunes, I Domingos, H Pereira


Hygroscopicity of wood after polyethylene glycol (PEG) impregnation and/or heat treatment
2013 - IRG/WP 13-40623
The hygroscopicity of wood after polyethylene glycol (PEG) impregnation and/or heat treatment was investigated by testing the water uptake, equilibrium moisture content (EMC) at various relative humidity levels, and contact angle of the poplar wood surface. The results showed that: (1) At the first moment, the heat treatment at temperatures lower than 160 ℃ did not reduce the water uptake be...
Weiyue Xu Yuan Zhu, Jinzhen Cao


Influence of Heat Treatment Medium on Fungal Resistance of Beech Wood
2013 - IRG/WP 13-40643
Hydrothermal treatment of beech wood (Fagus orientalis) performed in acidic, neutral and alkaline buffered mediums in 160 and 180°C. White rot fungi (Coriolus versicolor) and brown rot fungi (Coniophora puteana) were used to determine the influence of heat treatment mediums on the behaviour of fungal resistance. White rot of wood digest lignin rather than cellulose; while brown rot digests the ce...
A Talaei, A Karimi, M-F Thévenon


Durability of alternatives to CCA-treated wood - Results from field tests after 11 years exposure
2013 - IRG/WP 13-30633
The present study was initiated as a consequence of restrictions against the use of CCA-type wood preservatives in Sweden in the 1990s. New copper-based formulations were introduced on the market and to some extent, also alternatives to preservative-treated wood, such as thermally and chemically modified and linseed oil treated wood as well as heartwood of non-tropical naturally durable wood s...
P Larsson Brelid, M-L Edlund


Improving dimensional stability of thermally treated wood by secondary modification – potential and limitations
2014 - IRG/WP 14-40664
The potential of treating thermally modified wood with melamine resin to improve the dimensional stabilization is tested in this research. Two different boards of poplar (Populus ssp.) were cut into two halves. One half of each board was thermally modified (T1 and T2) in a commercial process, the other half was used as untreated reference material. The material was thermally modified using the vac...
G Behr, K-C Mahnert, S Bollmus, H Militz


Development of new wood treatments combining boron impregnation and thermo modification - Effect on decay and termites durability
2014 - IRG/WP 14-40666
Environmental pressures appeared in most European countries during the last decade has lead to the development of more environmentally acceptable preservation methods. In this context, wood heat treatment has been one of the most investigated alternative methods during the last years. Treated at temperatures ranging between 180 and 220°C, wood components undergo more or less important chemical mo...
S Salman, A Pétrissans, M-F Thévenon, S Dumarçay, B Pollier, P Gérardin


The Physical Properties of Heat Treated Fir Wood and Outdoor Durability
2014 - IRG/WP 14-40677
Wood might be easily susceptible to degrade by biotic and abiotic factors. Therefore, wood should be protected from fungi, insects and other degradation factors by applying treatment methods. Especially, for the wood have used in the external environment. Chemical treatment methods have some disadvantages such as use of toxic chemicals (Arsenic and chromium) and treatability of refractory wood spe...
O E Özkan, H Vurdu, A Temiz, G Köse


Effect of natural variability of European Oak wood on heat treatment process and potential implication on wood durability
2015 - IRG/WP 15-40693
Environmental pressures appeared in France and in most European countries during the last decade has led to the development of more environmentally acceptable preservation methods. In this context, wood heat treatment has been one of the most investigated alternative method during the last years. Treated at temperatures ranging between 180 and 220°C, wood components undergo more or less important...
J Hamada, A Pétrissans, F Mothe, M Pétrissans, P Gérardin


Investigation of Dimensional Stability and Coating Performance of Different Heat-Treated Poplar Wood Before and After Accelerated Aging
2015 - IRG/WP 15-40702
In this investigation, coating performance of heat-treated poplar wood (Populus tremuloioes) in different environments, before and after accelerated aging was studied. Specimens with 150×100×20 mm and 20×20×20 mm in dimensions were prepared. Heat treatments were performed in air, steam and linseed oil media. Specimens were coated by alkyd based stain. Adhesion strength before and after aging, ...
A Talaei, D Ansari Movahed, G Rassam


Evaluating the Effects of Post Dip-Treatment Laser Marking on Resistance to Feeding by Subterranean Termites
2016 - IRG/WP 16-10854
Dip-treatment of wood packing materials is often used instead of pressure treatment mainly because of issues relating to simplicity and cost. Packaging boxes fabricated for the United States Army are required to be dip-treated for at least one minute in an approved preservative solution prior to use. These boxes are expected to have a service life of up to 20 years in a wide variety of environment...
R A Arango, B Woodward, S Lebow


Characterization of waste from Pinus radiata generated during industrial thermal-treatment
2016 - IRG/WP 16-20586
The thermal-treatment is an established chemical-free process to modify wood, improving the durability and physical properties of wood through its service life. During the hydro-thermolysis several reactions from wood components occur, releasing volatile and non-volatile compounds from wood to the chamber. Once the process is accomplished, solid residues agglomerate below the wood load and gaseous...
R Herrera, D Thomas da Silva, R Llano-Ponte, J Labidi


How intraspecific radial variability of the European Oak’s may influence mild pyrolysis process and durability of the material
2016 - IRG/WP 16-40725
Last decades wood is promoted as building material. Unprotected wood exposed to outdoor conditions undergoes a variety of degradation induced essentially by fungi attacks. Heat treatment of wood by mild pyrolysis (180°C T 240°C under inert atmosphere) is a preservation process with a weak environmental impact, and therefore, is viewed as an interesting alternative to the chemical impregnation me...
J Hamada, A Pétrissans, F Mothe, M Pétrissans, P Gérardin


Modifying wood with paraffin wax emulsion impregnation and thermal modification: hydrophobization effect and mechanism of the combined treatment
2016 - IRG/WP 16-40726
The aim of this study was to enhance the water repellency of wood by a combined treatment of paraffin wax emulsion (PWE) impregnation and thermal modification. Two different treating procedures were used to modify the southern pine (pinus spp.). One is first PWE impregnation and then thermal modification, another is first thermal modification and then PWE impregnation. The treated samples were imm...
Wang Wang, Jinzhen Cao, Cong Chen


Dynamic mechanical analysis of viscoelastic properties of heat treated glycerol-impregnation poplar wood
2016 - IRG/WP 16-40732
The viscoelastic properties of glycerol-impregnated poplar wood after heat treatments at various temperatures were examined by dynamic-mechanical analysis. The spectra of storage modulus (E’) and loss tangent (tgδ) in the frequency at 10 Hz were measured at the temperature range from -100 to 300℃. Compared to no peak in E’ spectra and two relaxation processes in tanδ spectra of...
Li Yan


Formation of hydrophobic wood surface by means of thermal treatment and surface modification with alkyl ketene dimer (AKD)
2016 - IRG/WP 16-40738
One of the major shortcomings of wood-based materials compared to technical materials is attributed to their poor dimensional stability in changing climates and in contact with liquid water. Heat treatment induces chemical change with a consequent decreasing of reactivity of the material showing unwanted surface inactivation. Alkyl ketene dimer (AKD) is a widely used sizing agent in papermaking, w...
T Lovaglio, T Meints, L Todaro, W Gindl-Altmutter


Weathering protection of European hardwoods through double modification
2017 - IRG/WP 17-30715
Beech and poplar were thermally modified, treated with melamine resin and both treatments were combined. The weathering performance (cracks and general appearance) of modified beech and poplar was assessed in natural weathering and correlated to material properties such as work in bending (WB) and Brinell hardness. In addition, the equilibrium moisture content after exposure of 12 months and subse...
G Behr, A Gellerich, S Bollmus, H Militz


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