IRG Documents Database and Compendium


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Role of Global Cooperation in Wood Protection for Conserving Forest Resources
2007 - IRG/WP 07-50249
The current uses of treated wood are discussed along with the emerging concerns for continued use of these products. The issues of new chemicals, treatments for wood based composites, migration of chemicals from treated wood, and the disposal of these products at the end of their useful life are all outlined. The potential for the IRG to serve as the focus for research discussion as well as coll...
J J Morrell, G Deroubaix


Potential for using dip/supercritical fluid treatments for wood impregnation
2004 - IRG/WP 04-40276
While supercritical fluid impregnation offers tremendous potential for impregnating wood species that resist conventional liquid preservative treatments, the resulting treatments are often not uniform among samples in a charge or between charges. One factor that influences treatment is the dynamic change in pressure that occurs during introduction of the biocide laden supercritical fluid into the ...
Sung-Mo Kang, J J Morrell


Internal pressure development within Oriented Strand Board during supercritical fluid impregnation
2000 - IRG/WP 00-40175
Supercritical fluids (SCF) offer an attractive alternative to conventional treatment processes for delivering material into wood, but there are many unanswered questions concerning the technology. One major concern is the potential for the development of excessive pressure gradients in the wood that might exceed the material properties and lead to crushing or other pressure-induced damage. Previou...
G Oberdorfer, P E Humphrey, R J Leichti, J J Morrell


A novel method for delivering fluids into bolted wooden components.
2004 - IRG/WP 04-40280
The paper describes the development of a washer that enables fluids such as wood preservatives and adhesive resins to be delivered to bolted wooden components in-situ. The system was developed to meet the criteria of low cost and the ability to tolerate inaccurate drilling of holes in the wooden members....
G S Sawyer, B Tole


Effect of fatty acid removal on treatability of Douglas-fir
1993 - IRG/WP 93-40008
Treatment of Douglas-fir with chromated-copper-arsenate (CCA) poses a major challenge. Several hypotheses based on the anatomical aspects as well as chemical reactivity of the preservative formulations with cell wall constituents and deposits have been proposed. Techniques to prevent pit aspiration or slow fixation reactions have, however, not significantly improved treatment. The presence of high...
S Kumar, J J Morrell


Chemical analysis for TBTN in LOSP-treated wood and preservative fluids
1994 - IRG/WP 94-20027
Tributyltin napthenate (TBTN) is being substituted for tributyltin oxide (TBTO) in LOSP preservative formulations because its lower reactivity/better stability allows co-formulation with synthetic pyrethroids. Better stability may reduce molecular degradation both in-service and during analysis. It was considered necessary to check whether TBTO analysis methods were suitable for use on TBTN treate...
D P Wraight, M J Kennedy


Alternative technologies for wood wastes recycling - Part B: Biotreatment of PCP- and creosote-treated wood
1998 - IRG/WP 98-50101-18 b
Alternative technologies have been investigated to detoxify treated wood. Two classes of organic compounds are studied. Creosote-treated wood are classified in France as dangerous wood wastes. A conventional incineration could be provided for these wood wastes but the cost of this elimination could be very high (> 2000 FFR/ton). For these reasons, we have tested two kinds of new processes as al...
S Legay, P Marchal, G Labat


Bending properties of TCMTB-treated Southern pine sapwood using supercritical carbon dioxide impregnation process
1997 - IRG/WP 97-40080
The effects of elevated pressure and treatment with thiocyanomethylthiobenzothiazole (TCMTB) on the bending properties of Southern pine sapwood were evaluated at pressures ranging from 1,800 to 3,600 psi. All bending properties were affected to some extent by supercritical fluid treatment. Modulus of elasticity and work to maximum load were not significantly affected by pressure levels. Modulus of...
Gyu-Hyeok Kim, S Kumar, E S Demessie, K L Levien, J J Morrell


Termite Field Tests of Various Timber Species Treated with permethrin using supercritical carbon dioxide
2005 - IRG/WP 05-10560
Termite field tests were conducted on permethrin-treated Eucalyptus obliqua heartwood, Pinus radiata sapwood and P. radiata LVL. The permethrin was impregnated using either supercritical carbon dioxide (scCO2) or light organic solvent preservative (LOSP) systems. Comparative permethrin retentions were most accurately achieved in P. radiata sapwood, where no difference between impregnation systems ...
A Qader, L J Cookson, J W Creffield, D Scown


Cellular and fractural failure after supercritical fluid impregnation of four wood species
2004 - IRG/WP 04-10503
Supercritical fluids (SCFs) have been investigated for delivering biocides into sawn wood. Pressure differentials during treatment may exceed the compressive or tensile strength perpendicular to grain, creating a potential for transverse deformations that exceed elastic strain limits. Wood treated by SCF processing with CO2, a potential biocide carrier, was inspected macroscopically and microscopi...
M E Anderson, R J Leichti, J J Morrell


Supercritical fluid impregnation of Douglas-fir heartwood with cyproconazole using temperature induced deposition
2003 - IRG/WP 03-40259
A limited understanding of the fundamental aspects of supercritical fluid (SCF) impregnation in wood remains an obstacle to the development of this technology. Developing a better understanding of the effects of various process parameters on treatment results would facilitate more rational development of SCF impregnation. In this project, the effect of treating period and specimen length on su...
Sung-Mo Kang, J J Morrell


Supercritical fluid treatment: Effects on bending strength of white spruce heartwood
1993 - IRG/WP 93-20008
The effects of supercritical carbon dioxide on wood strength were evaluated using white spruce heartwood, a species known to be especially susceptible to collapse during exposure to higher pressures. The effects of pressures of 2000 or 3600 psig and temperatures of 40 or 80°C were evaluated using 30 or 60 minute exposure periods. No significant differences were noted in modulus of rupture or modu...
S M Smith, J J Morrell, E Sahle-Demessie, K L Levien


Alternative technologies for wood wastes recycling - Part A: Supercritical extraction of PAH compounds from wood wastes
1998 - IRG/WP 98-50101-18 a
Alternative technologies have been investigated to detoxify treated wood. Two classes of organic compounds are studied. Creosote-treated wood are classified in France as dangerous wood wastes. A conventional incineration could be provided for these wood wastes but the cost of this elimination could be very high (> 2000 FFR/ton). For these reasons, we have tested two kinds of new processes as al...
L Schrive, C Perre, G Labat


Applicability of supercritical carbon dioxide to the preservative treatment of wood-based composites
2001 - IRG/WP 01-40199
Treatability of five structural-use wood-based composites (medium density fiberboard, hardwood plywood, softwood plywood, particleboard and oriented strand board) was evaluated when supercritical (SC) carbon dioxide (CO2) was used as a carrier solvent. Treatments were conducted at three temperature 32 levels (25, 35 and 45°C) and two pressure levels [80 kgf/cm2 (7,845 kPa) and 120 kgf/cm2 (11,768...
M Muin, A Adachi, K Tsunoda


Preservative treatment of wood-based composites with a mixture formulation of IPBC-silafluofen using supercritical carbon dioxide as a carrier gas
2003 - IRG/WP 03-40251
Wood-based composites treated with a mixture formulation of a fungicide, 3-iodo-2-propynyl butylcarbamate (IPBC) and a termiticide, silafluofen using supercritical carbon dioxide (SC-CO2) as a carrier solvent were tested for their resistance to decay and termite attack in the laboratory. The treatment solution was prepared by mixing both biocides (IPBC 10 + silafluofen 1) with a co-solvent, ethano...
K Tsunoda, M Muin


Performance of Oriented Strandboard, Medium Density Fiberboard, Plywood, and Particleboard Treated with Tebuconazole in Supercritical Carbon Dioxide
2005 - IRG/WP 05-30364
The performance of oriented strandboard (OSB), medium density fiberboard (MDF), particleboard and plywood treated with tebuconazole using supercritical carbon dioxide was investigated over a 48 month exposure under harsh above ground conditions in Hilo, Hawaii. Samples treated to low retentions (<0.20 kg/m3) tended to experience decay at rates that were only slightly lower than those found wit...
J J Morrell, M N Acda, A R Zahora


Development of preservative treatment method using sub and super critical carbon dioxide
2007 - IRG/WP 07-40385
Significant efforts have been devoted for developing biocide impregnation method into wood materials using supercritical fluid. Developing better understandings of fluid phase and its effect on treatment results would facilitate a more rational development of supercritical fluid (SCF) impregnation. In this project, the preservative treatabilities under super- and sub-critical fluid conditions we...
Myeung-Won Cho, Sung-Mo Kang, Gyu-Hyeok Kim


Antifungal Activities of Three Supercritical Fluid Extracted Cedar Oils
2009 - IRG/WP 09-30501
The antifungal activities of three supercritical CO2 (SCC) extracted cedar oils, Port-Orford-cedar (POC) (Chamaecyparis lawsoniana), Alaska yellow cedar (AYC) (Chamaecyparis nootkatensis), and Eastern red cedar (ERC) (Juniperus virginiana L), were evaluated against two common wood decay fungi, brown-rot fungi (Gloeophyllum trabeum) and white-rot fungi (Trametes versicolor). The statistical analysi...
Tianchuan Du, T F Shupe, Chung Y Hse


Interactions between wood and propiconazole in supercritical carbon dioxide
2009 - IRG/WP 09-40461
Understanding the movement and deposition of biocides in wood is a fundamental aspect of the supercritical wood impregnation process and a key issue in developing the process e.g. to handle wood of larger dimensions. Previous research on supercritical wood impregnation frequently reports of a biocide concentration gradient in impregnated samples i.e. a lower concentration of biocides in the core o...
A W Kjellow, O Henriksen


Supercritical impregnation of wood with siloxane
2012 - IRG/WP 12-30595
This paper describes the effect of supercritical impregnation with siloxane on the water repellency of Scots pine (Pinus sylvestris) sapwood samples. Samples were impregnated with a low amount of siloxane dissolved in supercritical carbon dioxide using isopropanol as a co-solvent. Siloxane retention (i.e. weight percent gain (WPG)) of the treated samples was 1.3 % (w/w) as found by mass balance. T...
A Kjellow, F Imsgard, J Fernandes, O Henriksen, E Klaassen, R Wagner, J Delis


Field performance of wood impregnated with siloxanes using supercritical carbon dioxide
2013 - IRG/WP 13-40632
This paper presents preliminary results from a 13-month field test containing pine sapwood samples (Pinus sylvestris) impregnated with a mixture of siloxane and organic biocides using supercritical carbon dioxide as carrier. Samples were exposed above ground at a Danish field test site using matched non-treated sapwood controls for every treated sample. All samples were painted before exposure. Pi...
A Kjellow, F Imsgard, J Fernandes, R Wagner, J Delis


Full-scale impregnation of wood with siloxane using supercritical carbon dioxide
2014 - IRG/WP 14-40659
Full-scale impregnation of wood with siloxane was carried out using supercritical carbon dioxide as solvent. A batch of 3530 kg of Scots pine sapwood was impregnated to a retention of approximately 1.3% siloxane. The treatment also consisted of a simultaneous impregnation with organic biocides. The performance of the wood was evaluated in terms of capillary water uptake according to a modified EN ...
A Kjellow, F Imsgard, J Fernandes, R Wagner, J Delis