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Visualization of Copper in the Voids and Cell Walls of Treated Wood using X-Ray Micro-Computed Tomography
2013 - IRG/WP 13-40640
This study extends our observations of the distribution of copper in treated wood. A small wood block was cut from a southern pine batten that had been treated with a particulate-copper preservative and similar sized block was cut from a batten that had been treated with a copper-amine preservative. Both blocks were imaged using X-ray micro-computed tomography. We obtained tomograms of each treate...
P D Evans, A Limaye, H Averdunk, M Turner, T J Senden


Observation of Boring Process of Larvae of the Bamboo Powder-post Beetle (Dinoderus minutus)
2014 - IRG/WP 14-10821
The bamboo powder-post beetle Dinoderus minutus is a major pest of felled bamboo in Japan. X-ray computer tomography (CT) was applied to non-destructively trace the movement of the larvae of this beetle inside the infested bamboo samples. The bamboo samples were prepared from pieces of the Japanese timber bamboo Phyllostachys bambusoides culms that were enclosed with adult D. minutus beetles for a...
H Watanabe, Y Yanase, Y Fujii


The Chelator Mediated Fenton System in the Brown Rot Fungi: Details of the Mechanism, and Reasons Why it has Been Ineffective as a Biomimetic Treatment in some Biomass Applications – a Review
2014 - IRG/WP 14-10828
The chelator-mediated Fenton (CMF) reaction requires the action of two types of chelating compounds. The first chelator, oxalate, solubilizes and then sequesters iron, and the second chelator reduces iron. Iron reduction must be controlled near the fungal hyphae to prevent damaging Fenton chemistry from occurring in that location. Similarly, iron reduction must be promoted within the wood/plant ce...
B S Goodell, M Nakamura, J Jellison


Changes in mechanical and chemical properties of wood exposed outdoors
2014 - IRG/WP 14-20550
The aim of this study was to investigate differences in certain mechanical and chemical properties of three different wood species (common beach (Fagus sylvatica), Norway spruce (Picea abies), and copper-ethanolamine (CuE) impregnated Norway spruce (Picea abies)) that were exposed in use class 3 (CEN, 2006) for periods between 4 and 30 months. The results show, that changes in the investigated me...
N Thaler, C Brischke, D Žlindra, V Vek, M Humar


Scanning Transmission X-ray Microscopy as a tool for examining chemical changes in wood cell walls due to enzymatic activity
2014 - IRG/WP 14-20556
As development of techniques for examining enzymatic activity on solid, complex biological materials, is considered to be an important factor in further development of enzyme applications and for understanding the decay of plant materials, this study explores applicability of Scanning Transmission X-ray Microscope (STXM) for determining chemical changes in enzymatically treated samples at the cell...
D Jeremic, R Goacher, R Yan, C Karunakaran, E R Master


Non-destructive monitoring of structure and moisture dynamics of plywood exposed outdoors to improve service life prediction and fit-for-purpose design
2015 - IRG/WP 15-20570
Plywood is an important construction material yet prone to water uptake, which can decrease strength and increase decay risk. To predict service life and improve fit-for-purpose design, it is crucial to understand the moisture behavior and structural changes of plywood. In this research, several plywood specimens were exposed outdoors for approximately one year. During this period, the moisture di...
W Li, J Van den Bulcke, I De Windt, M Dierick, J Van Acker


The effect of preservative treatment on mechanical strength and structural integrity of wood
2015 - IRG/WP 15-30667
The use of wood for demanding construction applications is increasing in Europe. Wooden constructions are frequently designed of susceptible conifer wood, which is endangered by wood decay fungi in wet applications. Therefore in many cases treating wood with preservatives is unavoidable to ensure the desired service life. However, chemical treatment of wood can result in changes of its mechanical ...
M Humar, D Kržišnik, C Brischke


Effect of natural variability of European Oak wood on heat treatment process and potential implication on wood durability
2015 - IRG/WP 15-40693
Environmental pressures appeared in France and in most European countries during the last decade has led to the development of more environmentally acceptable preservation methods. In this context, wood heat treatment has been one of the most investigated alternative method during the last years. Treated at temperatures ranging between 180 and 220°C, wood components undergo more or less important...
J Hamada, A Pétrissans, F Mothe, M Pétrissans, P Gérardin


Impact of early lignification of ray parenchyma cells on the treatability of Scots pine sapwood
2015 - IRG/WP 15-40706
The wood anatomy of Scots pine sapwood can influence its treatability. A microscopic analysis on the wood material from four different stands in Northern Europe was performed using tangential sections from the outer part of Scots pine sapwood. Single correlations of the ray composition and lignification state of the ray parenchyma showed the influence of these factors on radial penetration depth a...
K Zimmer, A Treu


Preparation of Calibration Standards for the Analysis of Pentachlorophenol in Treated Wood by X-ray Fluorescence
2016 - IRG/WP 16-20591
The primary purpose of this project was to develop a method for preparing calibration standards that can be used by the wood treating industry to calibrate X-ray fluorescence instrumentation. Calibration standards of penta/P9-oil in southern yellow pine that cover the retention range of 0.2 to 0.9 pcf (0.6 to 1.9 %) were successfully prepared. A detailed procedure for mixing penta in treating sol...
L L Ingram Jr, H M Barnes, R Shmulsky, D Jeremic


Fabrication and characterization of MicroPCMs filled wood-plastic composites: Effects of polyethylene glycol on melamine–formaldehyde shell material
2016 - IRG/WP 16-40728
Microencapsulated phase change materials (MicroPCMs) containing dodecanol were fabricated using melamine-formaldehyde (MF) or polyethylene glycol 200 modified melamine-formaldehyde (PMF) resin as the shell materials by in situ polymerization. Wood flour/high-density polyethylene (WF/HDPE) composites with MF shell MicroPCMs (MF-MicroPCMs) or PMF shell MicroPCMs (PMF-MicroPCMs) were prepared, respec...
Xi Guo, Jinzhen Cao


The influence of log soaking temperature and thermal modification on the properties of birch veneers
2016 - IRG/WP 16-40749
In veneer manufacture the logs are routinely soaked in heated water baths in order to soften the wood prior to peeling. The temperature of the water may vary greatly between batches; however, the influence of log soaking temperature on veneer properties has had little research attention. Uncontrolled moisture is known to cause problems in wood-based materials, while thermal modification offers a m...
S Källbom, K Laine, M S Moghaddam, A Rohumaa, K Segerholm, M Wålinder


Nondestructive analysis of oviposition of the bamboo powderpost beetle Dinoderus minutus using acoustic emission and X-ray CT
2017 - IRG/WP 17-10889
The bamboo powderpost beetle Dinoderus minutus is a major pest of dry bamboo culms in Japan. In this study, acoustic emission (AE) and X-ray computed tomography (CT) was applied to the nondestructive analysis of the ovipositional behavior of adult D. minutus beetles inside bamboo pieces. Newly mated adult females were individually exposed to oviposition bamboo pieces prepared from culms of Phyllos...
H Watanabe, Y Yanase, Y Fujii


Controlled deposition of copper nanoparticles using wood inherent architecture as natural template
2017 - IRG/WP 17-40783
As one of the most abundant renewable biomass resources, wood can be used as templates for synthesizing functional nanoparticles with controlled shapes and sizes. In this study, copper nanoparticles were synthesized with controlled shapes and sizes using poplar wood as the natural inexpensive and renewable templates. The crystal structure and morphologies of the copper nanoparticles were character...
Youming Dong, Kaili Wang, Yutao Yan, Jianzhang Li, M Hughes, Shifeng Zhang


Durability of energy efficient wooden buildings: a building physical point of view
2017 - IRG/WP 17-40812
The drive for more energy efficient and sustainable buildings resulted in an increased popularity of wooden buildings, even in countries with a masonry tradition. Often guidelines and prescriptions then are copied from other countries. Different climatic boundary conditions and tradition of finishing, though, do require different moisture tolerance criteria. This is clearly the case for water vapo...
S Roels, J Langmans


Use of x-ray microdensitometry for assessing the resistance to the fungus C puteana of a hybrid larches population
2018 - IRG/WP 18-10923
The aim of this research was to utilize the X-ray microdensitometry to determine the natural durability and its variability of a hybrid larch population. The method was applied on slices obtained by increment cores collected on standing trees before cutting them down. The methodology was discussed also in order to propose as a new screening method especially suited for trees populations. X-ray mic...
S Palanti, F Alderighi, F Stefani, J P Charpentier, L E Pâques


Difference of wood decay manner between brown-rot species
2019 - IRG/WP 19-10938
Wood blocks (Cryptomeria japonica) which were decayed by a Polyporales white-rot fungus (Trametes versicolor) and brown-rot fungi (Fomitopsis palustris, F. pinicola, and Wolfiporia cocos), respectively, were analyzed by X-ray diffraction and infrared spectroscopic methods followed by multivariate analysis. In the analyses, the differences in the cellulose crystallinities and infrared spectral patt...
R Kondo, Yo Horikawa, S Nakaba, K Ando, M Yoshida


Visualization of Feeding Process of Larvae of the Wood-boring Beetles Using X-ray Computer Tomography
2019 - IRG/WP 19-10953
X-ray computer tomography (CT) was applied to observe the movement of the larvae of the wood-boring beetles Lyctus brunneus, Lyctus africanus, and Heterobostrychus aequalis inside the infested wood specimens. The larvae bred with artificial diet were inserted into the hole of wood specimens of rubber wood Hevea spp. or Japanese oak Quercus crispula. The wood specimens with larvae were scanned usin...
Y Yanase, H Watanabe, I Fujimoto, T Yoshimura, Y Fujii


Using X-ray micro-CT to evaluate density loss in anobiid infested wood
2019 - IRG/WP 19-10956
Considering the relevance of wood borers in construction, the present study had as main objective the evaluation of the impact of anobiid damage on timber elements by establishing an empirical correlation between lost material percentage (LM%, consumed by beetles) and apparent density (original – OTD and residual – RTD). Since the beetles’ attack produces a diffuse damage with a set of tunne...
J L Parracha, M F Pereira, A Maurício, P Faria, L Nunes


Accumulation of copper in parenchyma cells in southern pine wood treated with micronized and amine-copper preservatives
2019 - IRG/WP 19-20657
Our previous research used X-ray micro-computed tomography to examine the micro-distribution of copper in southern pine wood treated with a micronized wood preservative (MCA) and an amine-copper preservative (ACQ). We found that copper in wood treated with MCA was mainly concentrated in fusiform rays (rays containing resin canals), and in vertical (axial) resin canals. A similar, although not iden...
D Feng, M L Turner, A Limaye, M A Knackstedt, P D Evans


Exploring the use of X-ray micro CT as a tool for the monitoring of moisture production and mass loss during lab-based fungal degradation testing
2019 - IRG/WP 19-20654
Bio-based building materials, such as wood and wood-engineered products, are susceptible to degradation by decay fungi. In-depth knowledge on the intricate material-fungus relationship as well as performance data for many bio-based building materials are still lacking, and especially knowledge on how a material’s structure and moisture properties affect the degradation process is missing. Althou...
L De Ligne, J Van den Bulcke, A De Muynck, J M Baetens, B De Baets, L Van Hoorebeke, J Van Acker


Using X-ray scattering to elucidate the mechanisms behind the moisture and fungal decay resistance of epoxybutene modified wood
2019 - IRG/WP 19-40854
Chemical modification of the hydroxyl groups of wood can improve the properties of wood by providing moisture and biological resistance, as well as dimensional stability. Southern pine solid wood was chemically modified to various weight percentage gains (WPG) with epoxybutene (EpB, 8%-38% WPG). After modification, specimens were extracted with a toluene: ethanol (2:1) solution for 2 hours or wate...
R E Ibach, N Plaza


Analysis of larval development and feeding of an Anobiid beetle using X-ray computed tomography
2020 - IRG/WP 20-10961
Priobium sp., an anobiid beetle, can attack wood used for historic constructions in Japan. Its life history and feeding biology, especially larval development and behavior, are poorly understood because the beetles are hidden inside wood most of the time. We used X-ray computed tomography (CT) to regularly scan wood blocks infested with the larvae of the Priobium sp. and observed the process of ...
H Watanabe, R Kigawa, Y Fujiwara, Y Fujii


Evaluation of decay and energy properties from thermally modified biomasses during fungal deterioration by NIR-spectrometry
2021 - IRG/WP 21-40922
This study is focused on the prediction of fungal weight loss (WL) and high heating value (HHV) from raw and torrefied waste lignocellulosic feedstocks, according to their exposure duration to wood-destroying fungi, using near infrared spectroscopy (NIR) and chemometrics models. Sugarcane bagasse, coffee husk, eucalyptus and pine shavings were torrefied at 290 °C in a screw reactor, during 5, 7...
B de Freitas Homem de Faria, P Santana Barbosa, J Valente Roque, A de Cassia Oliveira Carneiro, P Rousset, K Candelier, R F Teofilo


Combining MRI and X-ray CT to monitor fungal decay of plywood and OSB in a lab test
2022 - IRG/WP 22-20683
Bio-based building materials, such as wood and wood-engineered products, are susceptible to degradation by decay fungi. In-depth knowledge on the intricate material-fungus relationship as well as performance data for many bio-based building materials are still lacking, and especially knowledge on how a material’s structure and moisture properties affect the degradation process is missing. Althou...
L De Ligne, T Núñez Guitar, C Vanhove, J Van Acker, J Van den Bulcke


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