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Further Studies on the Distribution of Copper in Treated Wood Using an XRF Microscope Technique
2011 - IRG/WP 11-40549
There are two distinct forms of copper in aqueous copper based wood preservative systems that are currently used in the United States for treatment of southern pine lumber. These are systems using either soluble copper (typically amine based) or the more recent particulate or “micronized” copper as the primary biocide. Studies reported last year showed that there were distinct differences in...
A Zahora


Use of X-Ray Micro-Computed Tomography to Visualize Copper in Preservative Treated Wood
2012 - IRG/WP 12-20488
This study tests the hypothesis that X-ray micro-computed tomography will be able to visualize the distribution of copper in wood treated with a micronized wood preservative containing copper carbonate. A small wood block measuring 12 x 12 x 19 mm was cut from a 2.4 m x 51 mm x 51 mm southern pine batten that had been treated with a micronized wood preservative. Tomograms of the wood block were ob...
P D Evans, A Limaye, H Averdunk, M Turner, T J Senden, M A Knackstedt


Plywood under the scanner: linking moisture dynamics and 3D structure
2012 - IRG/WP 12-20491
Plywood is highly esteemed as a construction material. Yet, the influence of moisture on both strength and durability are important factors. Especially the dynamics of moisture desorption and absorption should be taken into account when assessing the quality of a panel, which is a fact for all panel materials. This paper therefore focuses on the monitoring of the moisture dynamics of plywood subje...
J Van den Bulcke, I De Windt, N Defoirdt, J Van Acker


Accessibility of Wood Cell Walls to Well-defined Platinum Nanoparticles
2012 - IRG/WP 12-20494
Copper nanoparticles are found in the walls of parenchyma cells in southern pine sapwood treated with a micronised wood preservative, but they are absent from tracheid walls. Hence, we hypothesized that small nanoparticles can penetrate the walls of unlignified parenchyma cells, but are excluded from lignified tracheid walls. This paper tests this hypothesis by treating pine sapwood with an aqueou...
H Matsunaga, Y Kataoka, M Kiguchi, P D Evans


Nano structural properties of La2O3-Beech Wood Flour With XRD technique
2012 - IRG/WP 12-40607
This research was considered to study various properties of the Lanthana mixed with beech wood flour (BWF), as a new structure. For this purpose, La2O3 powders in the BWF have been obtained by sol-gel method using simultaneous gelation of all cations. La2O3 - BW samples are analysed by X-ray diffraction .The obtained results showed the formation of nano crystalline La2O3 phases. The average crys...
M Ghorbani Kokandeh, I Bahamni, A Bahari


Analysis of decay progress anisotropy by X-ray computer tomography
2012 - IRG/WP 12-20501
Wood has a serious handicap as structural materials that it is vulnerable to decay by fungi. A weather exposed bridge has a possibility of an abrupt fall down, and wooden houses with heavily decayed structural members are easily destroyed by large earthquakes. To avoid such damages, a new predicting method on the decay progress in timber structures, and also its strength losing behavior along with...
K Maeda, M Ohta


Visualization of Copper in the Voids and Cell Walls of Treated Wood using X-Ray Micro-Computed Tomography
2013 - IRG/WP 13-40640
This study extends our observations of the distribution of copper in treated wood. A small wood block was cut from a southern pine batten that had been treated with a particulate-copper preservative and similar sized block was cut from a batten that had been treated with a copper-amine preservative. Both blocks were imaged using X-ray micro-computed tomography. We obtained tomograms of each treate...
P D Evans, A Limaye, H Averdunk, M Turner, T J Senden


Observation of Boring Process of Larvae of the Bamboo Powder-post Beetle (Dinoderus minutus)
2014 - IRG/WP 14-10821
The bamboo powder-post beetle Dinoderus minutus is a major pest of felled bamboo in Japan. X-ray computer tomography (CT) was applied to non-destructively trace the movement of the larvae of this beetle inside the infested bamboo samples. The bamboo samples were prepared from pieces of the Japanese timber bamboo Phyllostachys bambusoides culms that were enclosed with adult D. minutus beetles for a...
H Watanabe, Y Yanase, Y Fujii


Scanning Transmission X-ray Microscopy as a tool for examining chemical changes in wood cell walls due to enzymatic activity
2014 - IRG/WP 14-20556
As development of techniques for examining enzymatic activity on solid, complex biological materials, is considered to be an important factor in further development of enzyme applications and for understanding the decay of plant materials, this study explores applicability of Scanning Transmission X-ray Microscope (STXM) for determining chemical changes in enzymatically treated samples at the cell...
D Jeremic, R Goacher, R Yan, C Karunakaran, E R Master


Non-destructive monitoring of structure and moisture dynamics of plywood exposed outdoors to improve service life prediction and fit-for-purpose design
2015 - IRG/WP 15-20570
Plywood is an important construction material yet prone to water uptake, which can decrease strength and increase decay risk. To predict service life and improve fit-for-purpose design, it is crucial to understand the moisture behavior and structural changes of plywood. In this research, several plywood specimens were exposed outdoors for approximately one year. During this period, the moisture di...
W Li, J Van den Bulcke, I De Windt, M Dierick, J Van Acker


Effect of natural variability of European Oak wood on heat treatment process and potential implication on wood durability
2015 - IRG/WP 15-40693
Environmental pressures appeared in France and in most European countries during the last decade has led to the development of more environmentally acceptable preservation methods. In this context, wood heat treatment has been one of the most investigated alternative method during the last years. Treated at temperatures ranging between 180 and 220°C, wood components undergo more or less important...
J Hamada, A Pétrissans, F Mothe, M Pétrissans, P Gérardin


Impact of early lignification of ray parenchyma cells on the treatability of Scots pine sapwood
2015 - IRG/WP 15-40706
The wood anatomy of Scots pine sapwood can influence its treatability. A microscopic analysis on the wood material from four different stands in Northern Europe was performed using tangential sections from the outer part of Scots pine sapwood. Single correlations of the ray composition and lignification state of the ray parenchyma showed the influence of these factors on radial penetration depth a...
K Zimmer, A Treu


Preparation of Calibration Standards for the Analysis of Pentachlorophenol in Treated Wood by X-ray Fluorescence
2016 - IRG/WP 16-20591
The primary purpose of this project was to develop a method for preparing calibration standards that can be used by the wood treating industry to calibrate X-ray fluorescence instrumentation. Calibration standards of penta/P9-oil in southern yellow pine that cover the retention range of 0.2 to 0.9 pcf (0.6 to 1.9 %) were successfully prepared. A detailed procedure for mixing penta in treating sol...
L L Ingram Jr, H M Barnes, R Shmulsky, D Jeremic


Nondestructive analysis of oviposition of the bamboo powderpost beetle Dinoderus minutus using acoustic emission and X-ray CT
2017 - IRG/WP 17-10889
The bamboo powderpost beetle Dinoderus minutus is a major pest of dry bamboo culms in Japan. In this study, acoustic emission (AE) and X-ray computed tomography (CT) was applied to the nondestructive analysis of the ovipositional behavior of adult D. minutus beetles inside bamboo pieces. Newly mated adult females were individually exposed to oviposition bamboo pieces prepared from culms of Phyllos...
H Watanabe, Y Yanase, Y Fujii


Controlled deposition of copper nanoparticles using wood inherent architecture as natural template
2017 - IRG/WP 17-40783
As one of the most abundant renewable biomass resources, wood can be used as templates for synthesizing functional nanoparticles with controlled shapes and sizes. In this study, copper nanoparticles were synthesized with controlled shapes and sizes using poplar wood as the natural inexpensive and renewable templates. The crystal structure and morphologies of the copper nanoparticles were character...
Youming Dong, Kaili Wang, Yutao Yan, Jianzhang Li, M Hughes, Shifeng Zhang


Use of x-ray microdensitometry for assessing the resistance to the fungus C puteana of a hybrid larches population
2018 - IRG/WP 18-10923
The aim of this research was to utilize the X-ray microdensitometry to determine the natural durability and its variability of a hybrid larch population. The method was applied on slices obtained by increment cores collected on standing trees before cutting them down. The methodology was discussed also in order to propose as a new screening method especially suited for trees populations. X-ray mic...
S Palanti, F Alderighi, F Stefani, J P Charpentier, L E Pâques


Difference of wood decay manner between brown-rot species
2019 - IRG/WP 19-10938
Wood blocks (Cryptomeria japonica) which were decayed by a Polyporales white-rot fungus (Trametes versicolor) and brown-rot fungi (Fomitopsis palustris, F. pinicola, and Wolfiporia cocos), respectively, were analyzed by X-ray diffraction and infrared spectroscopic methods followed by multivariate analysis. In the analyses, the differences in the cellulose crystallinities and infrared spectral patt...
R Kondo, Yo Horikawa, S Nakaba, K Ando, M Yoshida


Visualization of Feeding Process of Larvae of the Wood-boring Beetles Using X-ray Computer Tomography
2019 - IRG/WP 19-10953
X-ray computer tomography (CT) was applied to observe the movement of the larvae of the wood-boring beetles Lyctus brunneus, Lyctus africanus, and Heterobostrychus aequalis inside the infested wood specimens. The larvae bred with artificial diet were inserted into the hole of wood specimens of rubber wood Hevea spp. or Japanese oak Quercus crispula. The wood specimens with larvae were scanned usin...
Y Yanase, H Watanabe, I Fujimoto, T Yoshimura, Y Fujii


Using X-ray micro-CT to evaluate density loss in anobiid infested wood
2019 - IRG/WP 19-10956
Considering the relevance of wood borers in construction, the present study had as main objective the evaluation of the impact of anobiid damage on timber elements by establishing an empirical correlation between lost material percentage (LM%, consumed by beetles) and apparent density (original – OTD and residual – RTD). Since the beetles’ attack produces a diffuse damage with a set of tunne...
J L Parracha, M F Pereira, A Maurício, P Faria, L Nunes


Accumulation of copper in parenchyma cells in southern pine wood treated with micronized and amine-copper preservatives
2019 - IRG/WP 19-20657
Our previous research used X-ray micro-computed tomography to examine the micro-distribution of copper in southern pine wood treated with a micronized wood preservative (MCA) and an amine-copper preservative (ACQ). We found that copper in wood treated with MCA was mainly concentrated in fusiform rays (rays containing resin canals), and in vertical (axial) resin canals. A similar, although not iden...
D Feng, M L Turner, A Limaye, M A Knackstedt, P D Evans


Using X-ray scattering to elucidate the mechanisms behind the moisture and fungal decay resistance of epoxybutene modified wood
2019 - IRG/WP 19-40854
Chemical modification of the hydroxyl groups of wood can improve the properties of wood by providing moisture and biological resistance, as well as dimensional stability. Southern pine solid wood was chemically modified to various weight percentage gains (WPG) with epoxybutene (EpB, 8%-38% WPG). After modification, specimens were extracted with a toluene: ethanol (2:1) solution for 2 hours or wate...
R E Ibach, N Plaza


Exploring the use of X-ray micro CT as a tool for the monitoring of moisture production and mass loss during lab-based fungal degradation testing
2019 - IRG/WP 19-20654
Bio-based building materials, such as wood and wood-engineered products, are susceptible to degradation by decay fungi. In-depth knowledge on the intricate material-fungus relationship as well as performance data for many bio-based building materials are still lacking, and especially knowledge on how a material’s structure and moisture properties affect the degradation process is missing. Althou...
L De Ligne, J Van den Bulcke, A De Muynck, J M Baetens, B De Baets, L Van Hoorebeke, J Van Acker


Analysis of larval development and feeding of an Anobiid beetle using X-ray computed tomography
2020 - IRG/WP 20-10961
Priobium sp., an anobiid beetle, can attack wood used for historic constructions in Japan. Its life history and feeding biology, especially larval development and behavior, are poorly understood because the beetles are hidden inside wood most of the time. We used X-ray computed tomography (CT) to regularly scan wood blocks infested with the larvae of the Priobium sp. and observed the process of ...
H Watanabe, R Kigawa, Y Fujiwara, Y Fujii


Combining MRI and X-ray CT to monitor fungal decay of plywood and OSB in a lab test
2022 - IRG/WP 22-20683
Bio-based building materials, such as wood and wood-engineered products, are susceptible to degradation by decay fungi. In-depth knowledge on the intricate material-fungus relationship as well as performance data for many bio-based building materials are still lacking, and especially knowledge on how a material’s structure and moisture properties affect the degradation process is missing. Althou...
L De Ligne, T Núñez Guitar, C Vanhove, J Van Acker, J Van den Bulcke


Measurement of copper concentration in Cu-HDO treating solutions by handheld XRF
2022 - IRG/WP 22-20685
Copper based preservatives diluted in water dominate the wood preservative industry around the world. Periodically measurements and adjustments of the concentration of treating solutions must be performed as a part of the quality control at the treatment plant to achieve desired quality of the preservative treated wood. Many analytical methods are time consuming and must be performed under laborat...
P O Flaete


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