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New insights from NMR, FTIR, X-ray diffraction and physical chemistry into digestive processes in the wood-boring marine crustacean Limnoria quadripunctata
2010 - IRG/WP 10-10732
This paper summarises preliminary findings of a multi-technique exploration of the degradation of lignocellulose in the marine isopod Limnoria quadripunctata. Scanning electron microscopy revealed connections between the digestive gland and the hindgut that would permit the exchange of fluids between the two organs while the food mass is retained in place within the hindgut. This enables enzymes t...
G P Malyon, S LaBarre, N Kervarec, P Carey, J McGeehan, X Xie, A Klüppel, S M Cragg


A Comparison of the Performance of Related Copper Based Preservatives against Soft Rot
2010 - IRG/WP 10-30540
The performance of pine and beech wood treated with either a soluble copper + quat (ACQ type D) preservative system or a particulate copper + quat system was evaluated in unsterile soil using the European standard ENV 807 soft rot decay test procedure. In addition, to compare soft rot performance of soluble and particulate copper directly without the influence of co-biocides, beech and pine test...
M Ray, D Dickinson, K Archer


Copper nanoparticles in southern pine wood treated with a micronised preservative: Can nanoparticles penetrate the cell walls of tracheids and ray parenchyma?
2010 - IRG/WP 10-30547
This study tests the hypothesis that copper nanoparticles can penetrate the cell walls of southern pine wood treated with a micronised preservative. We examined the nanodistribution of particles in tracheid and ray parenchyma cell walls using state-of-the-art HR (High Resolution)-TEM and HR-STEM (Scanning Transmission Electron Microscope)-EDX. These devices are capable of atomic-scale resolution. ...
H Matsunaga, Y Kataoka, M Kiguchi, P Evans


Non-destructive evaluation of wood decay
2011 - IRG/WP 11-20479
Evaluation of wood decay is often prone to subjective assessment. Standard rating scales are based on human perception of decay, often in addition to weight loss measurements. Especially the assessment of graveyard specimens or other long term testing material that has to be monitored regularly on a non-destructive basis, is challenging. In this paper two techniques are presented that can deliver ...
J Van den Bulcke, I De Windt, N Defoirdt, J Van Acker


Copper Nanoparticles in Southern Pine Wood Treated with a Micronised Preservative: Nanodistribution of Copper in the Pit Membrane and Border of an Earlywood Bordered Pit
2011 - IRG/WP 11-30566
Copper nanoparticles can penetrate the cell walls of unlignified parenchyma cells in southern pine wood treated with a micronised wood preservative, but they are excluded from lignified tracheid walls. This paper extends these observations to include the cell wall layers of the bordered pit. Focused ion beam and ion milling were used to make an ultra-thin section of the cell wall layers of an earl...
H Matsunaga, Y Kataoka, M Kiguchi, P Evans


Further Studies on the Distribution of Copper in Treated Wood Using an XRF Microscope Technique
2011 - IRG/WP 11-40549
There are two distinct forms of copper in aqueous copper based wood preservative systems that are currently used in the United States for treatment of southern pine lumber. These are systems using either soluble copper (typically amine based) or the more recent particulate or “micronized” copper as the primary biocide. Studies reported last year showed that there were distinct differences in...
A Zahora


Plywood under the scanner: linking moisture dynamics and 3D structure
2012 - IRG/WP 12-20491
Plywood is highly esteemed as a construction material. Yet, the influence of moisture on both strength and durability are important factors. Especially the dynamics of moisture desorption and absorption should be taken into account when assessing the quality of a panel, which is a fact for all panel materials. This paper therefore focuses on the monitoring of the moisture dynamics of plywood subje...
J Van den Bulcke, I De Windt, N Defoirdt, J Van Acker


Accessibility of Wood Cell Walls to Well-defined Platinum Nanoparticles
2012 - IRG/WP 12-20494
Copper nanoparticles are found in the walls of parenchyma cells in southern pine sapwood treated with a micronised wood preservative, but they are absent from tracheid walls. Hence, we hypothesized that small nanoparticles can penetrate the walls of unlignified parenchyma cells, but are excluded from lignified tracheid walls. This paper tests this hypothesis by treating pine sapwood with an aqueou...
H Matsunaga, Y Kataoka, M Kiguchi, P D Evans


Nano structural properties of La2O3-Beech Wood Flour With XRD technique
2012 - IRG/WP 12-40607
This research was considered to study various properties of the Lanthana mixed with beech wood flour (BWF), as a new structure. For this purpose, La2O3 powders in the BWF have been obtained by sol-gel method using simultaneous gelation of all cations. La2O3 - BW samples are analysed by X-ray diffraction .The obtained results showed the formation of nano crystalline La2O3 phases. The average crys...
M Ghorbani Kokandeh, I Bahamni, A Bahari


Analysis of decay progress anisotropy by X-ray computer tomography
2012 - IRG/WP 12-20501
Wood has a serious handicap as structural materials that it is vulnerable to decay by fungi. A weather exposed bridge has a possibility of an abrupt fall down, and wooden houses with heavily decayed structural members are easily destroyed by large earthquakes. To avoid such damages, a new predicting method on the decay progress in timber structures, and also its strength losing behavior along with...
K Maeda, M Ohta


Observation of Boring Process of Larvae of the Bamboo Powder-post Beetle (Dinoderus minutus)
2014 - IRG/WP 14-10821
The bamboo powder-post beetle Dinoderus minutus is a major pest of felled bamboo in Japan. X-ray computer tomography (CT) was applied to non-destructively trace the movement of the larvae of this beetle inside the infested bamboo samples. The bamboo samples were prepared from pieces of the Japanese timber bamboo Phyllostachys bambusoides culms that were enclosed with adult D. minutus beetles for a...
H Watanabe, Y Yanase, Y Fujii


Scanning Transmission X-ray Microscopy as a tool for examining chemical changes in wood cell walls due to enzymatic activity
2014 - IRG/WP 14-20556
As development of techniques for examining enzymatic activity on solid, complex biological materials, is considered to be an important factor in further development of enzyme applications and for understanding the decay of plant materials, this study explores applicability of Scanning Transmission X-ray Microscope (STXM) for determining chemical changes in enzymatically treated samples at the cell...
D Jeremic, R Goacher, R Yan, C Karunakaran, E R Master


Modern Instrumental Methods to Investigate the Mechanism of Biological Decay in Wood Plastic Composites
2014 - IRG/WP 14-40674
Various instrumental techniques were used to study the fungal decay process in wood plastic composite (WPC) boards. Commercial boards exposed near Hilo, Hawaii (HI) for eight years in both sun and shadow locations were inspected and tested periodically. After eight years of exposure, both boards were evaluated using magnetic resonance imaging (MRI), while a selected area of the board exposed in sh...
G Sun, R Ibach, M Gnatowski, J Glaeser, M Leung, J Haight


Non-destructive monitoring of structure and moisture dynamics of plywood exposed outdoors to improve service life prediction and fit-for-purpose design
2015 - IRG/WP 15-20570
Plywood is an important construction material yet prone to water uptake, which can decrease strength and increase decay risk. To predict service life and improve fit-for-purpose design, it is crucial to understand the moisture behavior and structural changes of plywood. In this research, several plywood specimens were exposed outdoors for approximately one year. During this period, the moisture di...
W Li, J Van den Bulcke, I De Windt, M Dierick, J Van Acker


Effect of natural variability of European Oak wood on heat treatment process and potential implication on wood durability
2015 - IRG/WP 15-40693
Environmental pressures appeared in France and in most European countries during the last decade has led to the development of more environmentally acceptable preservation methods. In this context, wood heat treatment has been one of the most investigated alternative method during the last years. Treated at temperatures ranging between 180 and 220°C, wood components undergo more or less important...
J Hamada, A Pétrissans, F Mothe, M Pétrissans, P Gérardin


Impact of early lignification of ray parenchyma cells on the treatability of Scots pine sapwood
2015 - IRG/WP 15-40706
The wood anatomy of Scots pine sapwood can influence its treatability. A microscopic analysis on the wood material from four different stands in Northern Europe was performed using tangential sections from the outer part of Scots pine sapwood. Single correlations of the ray composition and lignification state of the ray parenchyma showed the influence of these factors on radial penetration depth a...
K Zimmer, A Treu


Preparation of Calibration Standards for the Analysis of Pentachlorophenol in Treated Wood by X-ray Fluorescence
2016 - IRG/WP 16-20591
The primary purpose of this project was to develop a method for preparing calibration standards that can be used by the wood treating industry to calibrate X-ray fluorescence instrumentation. Calibration standards of penta/P9-oil in southern yellow pine that cover the retention range of 0.2 to 0.9 pcf (0.6 to 1.9 %) were successfully prepared. A detailed procedure for mixing penta in treating sol...
L L Ingram Jr, H M Barnes, R Shmulsky, D Jeremic


Nondestructive analysis of oviposition of the bamboo powderpost beetle Dinoderus minutus using acoustic emission and X-ray CT
2017 - IRG/WP 17-10889
The bamboo powderpost beetle Dinoderus minutus is a major pest of dry bamboo culms in Japan. In this study, acoustic emission (AE) and X-ray computed tomography (CT) was applied to the nondestructive analysis of the ovipositional behavior of adult D. minutus beetles inside bamboo pieces. Newly mated adult females were individually exposed to oviposition bamboo pieces prepared from culms of Phyllos...
H Watanabe, Y Yanase, Y Fujii


Controlled deposition of copper nanoparticles using wood inherent architecture as natural template
2017 - IRG/WP 17-40783
As one of the most abundant renewable biomass resources, wood can be used as templates for synthesizing functional nanoparticles with controlled shapes and sizes. In this study, copper nanoparticles were synthesized with controlled shapes and sizes using poplar wood as the natural inexpensive and renewable templates. The crystal structure and morphologies of the copper nanoparticles were character...
Youming Dong, Kaili Wang, Yutao Yan, Jianzhang Li, M Hughes, Shifeng Zhang


Use of x-ray microdensitometry for assessing the resistance to the fungus C puteana of a hybrid larches population
2018 - IRG/WP 18-10923
The aim of this research was to utilize the X-ray microdensitometry to determine the natural durability and its variability of a hybrid larch population. The method was applied on slices obtained by increment cores collected on standing trees before cutting them down. The methodology was discussed also in order to propose as a new screening method especially suited for trees populations. X-ray mic...
S Palanti, F Alderighi, F Stefani, J P Charpentier, L E Pâques


Difference of wood decay manner between brown-rot species
2019 - IRG/WP 19-10938
Wood blocks (Cryptomeria japonica) which were decayed by a Polyporales white-rot fungus (Trametes versicolor) and brown-rot fungi (Fomitopsis palustris, F. pinicola, and Wolfiporia cocos), respectively, were analyzed by X-ray diffraction and infrared spectroscopic methods followed by multivariate analysis. In the analyses, the differences in the cellulose crystallinities and infrared spectral patt...
R Kondo, Yo Horikawa, S Nakaba, K Ando, M Yoshida


Visualization of Feeding Process of Larvae of the Wood-boring Beetles Using X-ray Computer Tomography
2019 - IRG/WP 19-10953
X-ray computer tomography (CT) was applied to observe the movement of the larvae of the wood-boring beetles Lyctus brunneus, Lyctus africanus, and Heterobostrychus aequalis inside the infested wood specimens. The larvae bred with artificial diet were inserted into the hole of wood specimens of rubber wood Hevea spp. or Japanese oak Quercus crispula. The wood specimens with larvae were scanned usin...
Y Yanase, H Watanabe, I Fujimoto, T Yoshimura, Y Fujii


Using X-ray micro-CT to evaluate density loss in anobiid infested wood
2019 - IRG/WP 19-10956
Considering the relevance of wood borers in construction, the present study had as main objective the evaluation of the impact of anobiid damage on timber elements by establishing an empirical correlation between lost material percentage (LM%, consumed by beetles) and apparent density (original – OTD and residual – RTD). Since the beetles’ attack produces a diffuse damage with a set of tunne...
J L Parracha, M F Pereira, A Maurício, P Faria, L Nunes


Validation by micro-computed tomography of an assessment method to measure the residual strength of anobiids infested timber
2019 - IRG/WP 19-20650
In this article a quantitative correlation study of pine timber structural elements, which have been subject to attack by anobiids, is presented. The main objective of the study was to establish a valid empirical correlation between the lost material percentage (consumed by beetles) and original/residual apparent density. Since the beetles’ attack produces a diffuse damage with a set of tunnels ...
J L Parracha, M F Pereira, A Maurício, P Faria, L Nunes


Exploring the use of X-ray micro CT as a tool for the monitoring of moisture production and mass loss during lab-based fungal degradation testing
2019 - IRG/WP 19-20654
Bio-based building materials, such as wood and wood-engineered products, are susceptible to degradation by decay fungi. In-depth knowledge on the intricate material-fungus relationship as well as performance data for many bio-based building materials are still lacking, and especially knowledge on how a material’s structure and moisture properties affect the degradation process is missing. Althou...
L De Ligne, J Van den Bulcke, A De Muynck, J M Baetens, B De Baets, L Van Hoorebeke, J Van Acker


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