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An effective preservative treatment of borak bamboo (Bambusa balcoona Roxb.)
1996 - IRG/WP 96-40070
Adequate penetration and retention of CCA and CCB has been obtained in predried Borak Bamboo (Bambusa balcooa Roxb.), aboundantly grown in Bangladesh, with Full Cell Pressure Process. The treated bamboo can be used as building materials, the sufficient treatability ensured its long term best utilization at ground contact and indoors. Which will keep the environmental & socio economical conditions of Bangladesh more viable and normal.
A K Lahiry, S Begum, G N M Ilias, M A Matin Sheikh, M A B Fakir, M I Hossain

A novel guide for the determination of the physical properties of wood including kiln drying and full-cell preservative treatment
2004 - IRG/WP 04-20298
An ideal flow chart for the sequential experimental determination of a range of physical properties relevant to wood drying and subsequent preservation was designed as a novel guide to assist wood scientists. In this manner, data assembly and experimental processing are shown. This was designed according to experience and published literature. Aspects emphasised in this review were the physical properties which effect the manner of processing particularly in respect to preservative treatment of wood. For this purpose a total of 93 references covering 8 topics (descriptive wood anatomy, physical properties of wood, shrinkage and swelling, wood density, moisture content, fibre saturation point, wood drying (by oven and kiln) and liquid permeability) were reviewed.
I Usta, M D C Hale

Trial to determine a suitable schedule for radial and longitudinal treatment of plug samples by comparison of changes in the fluid retention and the treated area
2001 - IRG/WP 01-40211
A full-cell process was carried out using different treatment schedules for radial and longitudinal samples because of the anisotrophy of flow. When timbers are impregnated with preservatives much better penetrations are obtained via the end grain than laterally (across the grain). Therefore, suitable schedules for radial and longitudinal flow directions were determined in an trial experiment using locally grown Sitka spruce, Queen Charlotte Islands (QCI) provenance, from Beddgelert Forest in North Wales. The full cell experimental schedules used were: initial vacuum 15 minutes at -0.84 bar and various pressure periods that was 5 bar pressure in radial flow direction for 15, 45, and 60 minutes, 3 bar pressure in longitudinal flow direction for 3, 6, and 9 minutes. No final vacuum was applied. After the treatment, the fluid uptake was calculated, and the fluid retention was determined on a whole-block basis. After fixation, plugs were dried and cut longitudinally through the centre and copper penetration was determined by spraying a 1% solution of Chrome Azurol-S on the cut surface and observing the blue colour indicative of copper. The preservative penetration was then measured by image analyser as depth (mm) and as total treated area (%). From the experimental data, it was concluded that the suitable schedules are 5 bar pressure for 45 minutes for the radial flow direction, and 3 bar pressure for 7 minutes for the longitudinal flow direction. Therefore these schedules are suggested to be used to examine the permeability of the different seed origins in both radial and longitudinal flow directions.
I Usta

A note on te seasoning, preservative treatment and suitability of debdaru (Polyalthia longifolia Benth & Hooker.) for poles
1995 - IRG/WP 95-40056
The main work is to determining the suitability of Debdaru (Polyalthia longifolia Benth.) as poles from Government and Village forests are investigated. The poles of Debdaru are easily treatable with CCA preservative by full-cell pressure method, but difficult to dry (air & kiln). Proper quality control must be maintain from procurement to treatment, specially during physical selection & drying (air & kiln) otherwise it may be discard as pole. Debdaru poles have been found suitable for power and Telecomunication lines with very keen care.
G N M Ilias, M D Rokib-ul-Hafiz

Chemical treatment of ten Amazonian timber species of low natural durability
1991 - IRG/WP 3640
The objective of this work was to evaluate the performance of 10 amazonian wood species of low natural durability, to treatment with CCA preservative (2% concentration): it was concluded that all species studied are easily treated with this preservative. The sapwood showed high absorption and total penetration. The heartwood is relatively easy to preserve, exception to Parkia nitidae (Fava), Qualea paraensis (Mandioqueiras), Erisma unicatum (Quarubarana), and Virola sp (Ucuúba), which presented some restrictions. Nevertheless, it does not mean that their treatment is impossible.
C S Neta, B F Vianez

Tilting and vacuum treatment - two methods to obtain a non-dripping freshly treated timber
1989 - IRG/WP 3535
Modern impregnation plants are designed to prevent spread of impregnation solutions from the plant through leakage, etc. It is also important that freshly treated timber does not spread solutions through dripping on the storage area. To prevent this, the impregnation procedure is terminated with a vacuum period. In many plants in Sweden this period is minimized or even excluded to gain time. Instead the freshly treated timber is tilted for some time before it is transported to the storage area. To evaluate the effect of these two methods to get a non-dripping freshly treated timber a small study was carried out by the Swedish National Testing Institute (SP) together with the Swedish Wood Preservation Institute (SWPI).
I Johansson, M-L Edlund

Effects of concentration and temperature of CCA and CCB on wood strength of Turkish fir (Abies bornmulleriana Mattf.)
2009 - IRG/WP 09-40450
The purpose of this study was to present evidence for the effects of concentration and temperature of solutions of water-borne preservatives (chromated copper arsenate, CCA and chromated copper boron, CCB) on the static bending properties (modulus of elasticity, MOE and modulus of rupture, MOR) of Turkish fir (Abies bornmulleriana Mattf.). Wood samples were mechanically tested after a mild full cell preservative treatment with 2.5 and 3.0% CCA and CCB solutions heated to 30 and 40 °C.Untreated controls were included for comparison.The experimental data indicated that heating the solutions of both CCA and CCB caused a greater shift in the fluid uptake, i.e. it increased with temperature up to 30 ºC, but at 40 ºC it was lower than that of unheated controls. In absolute terms, the fluid uptake of either preservative solutions was higher particularly in lower concentrations. CCB treatment had a greater fluid uptake for all cases. Results also showed that the effects of increasing concentration and temperature of both water-borne preservatives on MOE and MOR were very highly significant, while these strength properties were a significantly lower after the wood treatment with concentration of 3.0 % and heated at 40 ºC. Both MOE and MOR decreased even more by the treatment of CCB. It was therefore concluded that the strength properties of Turkish fir based on MOE and MOR were affected to a small extent by the full-cell vacuum/pressure wood treatment by using CCA and CCB with the concentrations of 2.5 and 3.0 % heated at 30 and 40 ºC. The worst case was 3.0% CCB treatment at 40 °C which resulted in a 5.0% reduction in MOE and a 5.2% reduction in MOR.
I Usta, M Hale

Chapter 11 - Preservation of talla bamboo
2007 - IRG/WP 07-10635-11
Researches revealed that the talla bamboo (Bambusa tulda Roxb.)) in Bangladesh could be full-cell pressure treated with CCA in green and dry conditions. The dry bamboo gives higher loading absorptions than green one when impregnated at same treating conditions. Also higher absorptions are obtained at nodes rather than internodes. Adequate penetration and retention results for ground and water contact uses are only possible by treating bamboos pre-dried to 10-15% MC. The green bamboo is easily treatable for indoor and overhead outdoor uses. The service life of this socio-economically important bamboo can easily be increased at least two times than nominal by CCA treating either green or dry bamboo. Two small holes made before pressure treatment in each internode will give split-free bamboo.
A K Lahiry

Chapter 12 - Treatment Groups of Bamboo
2007 - IRG/WP 07-10635-12
Study on distribution of CCA in three major bamboo species in Bangladesh, full-cell pressure treated at green and dry conditions revealed two treatment groups and some treating principles. Higher adequate treatment for ground and water contact use is only possible by treating problematic bamboo species pre-kiln dried up to half of its FSP and non-problematic species pre-dried up to FSP (20% MC). The non-problematic species can be treated in green conditions for indoor and overhead outdoor uses. Two smallest holes made before treatment in each internode will give split-free bamboo.
A K Lahiry

Comparison of cubic and plug samples for preparation and data assembly in permeability study
2000 - IRG/WP 00-20197
In order to determine if plug experimental samples (PES: 30 x 15 mm2 diameter) could be used for inspection of wood permeability characteristics, radial and longitudinal flow directions were prepared according to either PES or cubic experimental samples (CES: 100 x 20 x 20 mm3) from the sapwood zone of Sitka spruce and treated by tanalith-C according to full-cell process. Results from the two preparation techniques agreed in the test to determine the mean percentage of void volume filled by liquid both radially and longitudinally, while the preparation process (i.e. machining, sealing, etc.) of the experimental samples and the period of the data collection was quite longer in CES than that for PES in either flow direction.
I Usta

Natural durability transfer from sawmill residues of white cypress (Callitris glaucophylla). - Part 3: Full penetration of the refractory sapwood of white cypress
2000 - IRG/WP 00-40167
The heartwood of white cypress, Callitris glaucophylla, is renowned for its termite resistance and durability against decay. The sapwood, which can represent up to 30% of log volume, is non-durable and refractory to conventional preservative treatment. Previous work ascribes the lack of permeability to oily deposits within tracheids and ray cells. Environmental scanning electron microscopy was used to investigate ultrastructural aspects of sapwood permeability. Several pre-treatment processes to improve permeability were tested with limited success. Solvent drying allowed preservative penetration but damaged the structure of the timber. Neither, long term water soaking nor an oscillating pressure/vacuum cycle had any effect on porosity to water-borne treatments. Through extensive modifications to a standard VPI process we can now repeatedly achieve full penetration with organic solvent-based wood preservative solutions into white cypress sapwood. Effects of this process on the strength of the timber are being evaluated. Work is continuing as to the most effective and efficient treatment schedule and the latest results will be presented at IRG 31.
M J Kennedy, L M Stephens, M A Powell

Analysing the characteristic role of moisture content for drying and fluid flow in Sitka spruce. - Part 1: The drying process of sapwood and heartwood of two different thickness of Sitka spruce using a kiln. - Part 2: Effects of moisture content on longitudinal permeability of Sitka spruce in vertical variation of the tree
2000 - IRG/WP 00-40173
The characteristic role of the moisture content in Sitka spruce (Picea sitchensis (Bong.) Carr.) that grown in the United Kingdom was examined by this study on the basis of (1) the reduction of moisture content in two different thickness of sapwood and heartwood by kiln drying process, and (2) the effects of moisture content to the longitudinal void volume filled of tanalith-C by the full-cell process from base (1 m) to apex (3 m) of the tree in sapwood zone. Accordingly, conclusions on indication of the drying process of sapwood and heartwood, and vertical variation of longitudinal flow with effects of moisture were listed separately: (1) Comparison of Drying Characteristic of Sapwood and Heartwood: The two different thickness (300x30x30 mm3 and 300x20x20 mm3) of sapwood and heartwood of Sitka spruce was dried using the suggested drying schedule in kiln. The reduction of moisture was schematically diagrammed according to sapwood and heartwood stakes. The reduction of moisture followed the same downward trend that sapwood (S) loses more moisture than heartwood (H) although the small stakes of S and H lost moisture rapidly compared with the large ones. (2) Vertical Variation of Moisture Content and Longitudinal Permeability: The 90 kiln dried defect free sapwood stakes (150x25x25 mm3) of Sitka spruce was taken from base to apex of the trees at 1, 2 and 3 m above ground level. After having the determination of moisture content in each experimental stake, the treatment was carried out by the full-cell process with CCA preservative (Tanalith-C) using a model pressure treatment plant. Significant differences observed among the tree heights from 1 to 3 m showing that slightly increases of moisture content from base to apex and conversely decreases of longitudinal void volume filled by preservative fluid.
I Usta

Water-based water repellents for treatment of wood
1987 - IRG/WP 3446
The water uptake by wood can be reduced by treatment with a water repellent. The water repellents most commonly used are solvent based. In the present work a new type of water repellent that is water-based has been investigated. Two different treatments have shown an effect of the same order as a commercial solvent based product. The cellular distribution of the water repellents has been investigated and for one of the formulations a more uniform distribution can be seen at the impregnated surface. Use of water as a solvent would be advantageous due to lower cost and non-toxicity.
I G Svensson, G Hägglund, I Johansson, W B Banks

Copper naphthenate-treated Southern Pine pole stubs in field exposure. -Part 2: Chemical characterization of full size pole stubs 12 years after treatment
2000 - IRG/WP 00-30246
This study examines the influence of pre-treatment and post-treatment steaming on the character and physio-chemical nature of copper naphthenate in hydrocarbon solvent treated pine in larger, pole diameter, pole stub-length samples. This work is the continuation of two projects that began almost a decade ago. Previous reports indicated that certain morphological changes might occur in small laboratory steamed samples of copper naphthenate treated southern pine. Toluene-methanol extraction, UV-Vis spectroscopy, X-ray diffraction (XRD) and environmental scanning electron microscopy (ESEM) were used to investigate the nature and properties of the copper naphthenate present in the wood after 12 years of exposure. The formation of solid cuprous oxide occurred regardless of pre- or post-steaming conditioning.
H M Barnes, D P Kamdem, M H Freeman

The effects of density on vertical variation of permeability of Sitka spruce within tree
2000 - IRG/WP 00-40156
Tree improvement of Sitka spruce is a combination of silviculture and tree breeding aimed at producing higher quality products including increased growth rate and timber yield, and wood density. It is useful to know annual ring structure and density distribution when studying the quality of wood, grading it, or determining how the wood structure affects residual flow in softwoods. Since density is a factor under genetic control, the study in this article details the effects of density on longitudinal and radial permeability of Sitka spruce from base to apex. Comparison of overall means of both longitudinal and radial void volume filled (%) suggest that longitudinal permeabilities were almost the mirror image of those for the radial permeability along the tree trunk.
I Usta.

A behaviour of CCA penetration of fir (Abies bornmulleriana Mattf.) at different ramp times and constant vacuum/pressure applications
2006 - IRG/WP 06-40346
A behaviour of CCA penetration of Bornmulleriana fir (Abies bornmulleriana Mattf.) at different ramp times and constant vacuum/pressure applications was illustrated for the main flow directions by the experimental pictures.
I Usta, R Despot, M Hasan

Leaching of copper, chromium and arsenic from CCA-treated slash pine heartwood
1994 - IRG/WP 94-50020
Drying green slash pine with any of three high temperature drying schedules produced a product in which both the sapwood and the heartwood could be penetrated with CCA using a modified Bethell treatment schedule. Required H3 retentions were achieved in both sapwood and heartwood, from 200 litres per m³ charge uptake. Post-treatment fixation/drying was accomplished by three different regimes, including an accelerated fixation. Although acceptable preservative penetration and retention was achieved in the heartwood, arsenic fixation (as determined by both AWPA procedure E11-87 and U.S. EPA TCLP procedure) was inferior to that attained in the sapwood. TCLP leachates from 1 cm³ heartwood blocks contained up to 4.5 mg/l arsenic, very close to the maximum value (5.0 mg/l) currently permitted in Australia for arsenic waste disposal. Though there are clear advantages in achieving heartwood penetration, caution must be exercised to ensure that this step does not compromise the accepability of the product. No process modification could be accepted if it introduced possibilities of exceeding safe disposal limits for sawdust and offcuts, or building site contamination.
M J Kennedy, G Palmer

Preservation of two Indonesian timber species for marine environment purposes
1994 - IRG/WP 94-10079
This paper deal with the experiment of CCA full cell processed two non-durable Indonesian species for placed in the marine environment. 80 samples of 5 x 5 x 60 cm³ dried durian (Durio zibethinus) and mahogany (Swietenia mahagony) timber were CCA-full cell processed using 4 combination treatment of: without steaming; one hour steaming; 3% and 5% CCA solution concentration. 40 samples of them were field tested in the sea water in Rambut island beach near by Jakarta. The results shows that mahogany very difficult to treat and not recommended to be placed in marine environment, while CCA retention in durian timber could reach 29.91 kg/m³ and meet the requirement of retention for timber to be placed in marine environment. After two month field test in sea water full cell processed drian with 5% CCA solutin concentration could prevent marine borers attack.
P Permadi, I M Padlinurjaji, F Rasmita

Wood protection processes in the Asean countries
1994 - IRG/WP 94-40034
This paper presents the wood processing practices in the Asean countries composing Indonesia, Malaysia, Philippines, Singapore, and Thailand except Brunei. The development of wood preservation industry in these countries started as early as 1922 to 1960. As in other industrial countries, treatment pressure with creosote of utility poles, railway sleepers, and marine pilings are the prime commodities that require long term protection. The introduction of water-borne preservatives covered the treatment of sawn timber and other lignocellulosic materials. It covers the historical background and development of the industry in each country, treatment processes both pressure and non-pressure of commodities e.g. power poles, railway sleepers, marine pilings, housing components, furniture, and other lignocellulosic materials requiring protection against biological deterioration. Technical problems are common and varied due to different treatment standard specifications and preservatives specially water-borne types. The pollution aspect of preservating plants and the prohibition and control of some wood preservatives is a growing concern of the environmentalists. Wood preservation in the Asean countries will stay on and geared towards the treatment of industrial tree plantations, rubberwood, palms and bamboos.
F R Siriban

The multi-phase pressure (MPP) process. One stage CCA treatment and accelerated fixation process - Concepts proved by repetitive pilot plant treatments
1997 - IRG/WP 97-40079
Twenty-four charges of radiate pine roundwood or sawn timber were treated using the MPP Process and hot CCA solution. Treated timber met the CCA retention and penetration requirements of the NZ Timber Preservation Council for Hazard Classes H3 to H5. The objectives of the trials were: (1) To "stress" CCA solution by repetitive heating, treating and cooling to determine its stability in the process; (2) to determine any effects of pre-drying regimes on the standard of treatment; (3) to determine the extent of fixation influenced by various treatment variables. At the finish of the trials, the working solution was clear with no propensity to sludging. Preservative element ratios remained constant throughout the trials. Wood moisture content at the time of treatment had, not unexpectedly, most effect on degree of fixation achieved. Kickback liquid contamination with residual CCA and organic carbon was greater when wood moisture contents were high.
A J Pendlebury, J A Drysdale, K Nasheri, H Pearson, M E Hedley

A study on the pressure impregnation of Eucalyptus globulus fence posts with CCA preservatives. Part 1
1988 - IRG/WP 3470
This paper describes the impregnation with CCA preservatives by full-cell process of Eucalyptus globulus fence-posts. Several treatments were made for different times of initial vacuum and treating pressure, with fence-posts from two coppice plantations (1st and 2nd rotations), assembled into three diameter classes: small, medium, large. The results concerning the absorption and lateral penetration of the product reveal that impregnation of Eucalyptus globulus though difficult is often possible. The highest average values were recorded in the small diameters, yet the standard deviation in all three classes is quite remarkable. Moreover fence-posts from the 1st rotation stand show a better behaviour with the treatment. There seems to be no significant correlation between absorption and initial vacuum or treating pressure times.
D De Sousa Castro Reimão, L Nunes

Investigation of temperature effect on fixation of Celcure preservative (ACC) in beech (Fagus orientalis)
2001 - IRG/WP 01-40200
In this research, the fixation speed of Celcure 2% (ACC) preservative salt, under temperature of 17°C, 27°C and 50°C, on intact and stained wood specimens of beech was investigated. For this purpose, blocks of wood with 5x5x7 cm dimensions were prepared and saturated with 2% ACC concentration by full-cell process. The specimens were put in three incubators at the above-mentioned temperatures. For measuring the percentage of fixation through time, the specimens were extracted by using hydraulic pressure equipment, under 69 Mpa pressure. The pH of extraction was measured with the method of diphenyl Carbazid and by using spectrophotometer. This measurement was done continuously and the amount of 6- valence chromium concentration present in the extract was compared with the amount of chromium concentration in the primary solution and then the percentage of fixation was calculated. The results showed that the decrease in 6-valence chromium is accompanied with increase of pH, this is due to absorption of positive hydrogen ion by 6-valence chromium for reduction to 3-valence chromium and also ion-exchange of active components with wood during the primary phase of fixation. Also, the time necessary for reaching complete fixation in intact and stained wood in the fixation temperature conditions of 17, 27 and 50°C were 1075, 501, 109 hours, respectively. In general, the results showed that temperature has effective role in accelerating of fixation process and in this respect, intact and stained wood did not show significant statistical difference.
A Karimi, M Ghorbani

Effect of treating process on efficacy of CCA in a laboratory decay test
1990 - IRG/WP 3628
Test samples of Pinus radiata sapwood measuring 40x40x500 mm³ were treated with a range of concentrations of the copper-chrome-arsenate (CCA) formulation "Tanalith C" using Rueping (empty cell), Lowry (empty cell) and Bethell (full cell) treatment processes. Samples were then reduced to 40x40x7 mm³ test blocks and exposed to the decay fungus Coniophora puteana using an agar/block technique. Replicate blocks were analysed for preservative components. Regression analyses of percentage weight losses of test blocks against total Cu+Cr+As retentions (TAE) showed differences in efficacy of the preservative when applied by the three different processes, the order of effectiveness being Bethell > Lowry > Rueping. Two hypotheses are proposed to explain the results: (1) Disproportionation within the wood of preservative salts when applied by empty cell processes, (2) Differences in distribution of preservative elements following treatment by the three processes.
M E Hedley, K Nasheri, J G Van der Waals

A study on the pressure impregnation of Eucalyptus globulus fence-posts with CCA preservatives. Part 2
1989 - IRG/WP 3514
This paper describes the second part of a study on pressure impregnation of Eucalyptus globulus fence-posts with CCA preservatives presented at the IRG 19th Meeting. Fence-posts of three diameter classes, were treated, considering only one treatment schedule. The results show possibility of vacuum-pressure impregnation of blue gum fence-posts, with diameter less than 9 cm, though mainly by longitudinal penetration, which is usually conditioned by the length of the fence-post.
L Nunes, D De Sousa Castro Reimão

Notes on a wood preservation industry in Medan, North Sumatera, Indonesia
1987 - IRG/WP 3405
This paper deals with a descriptive account on the development of a wood preservation industry in Medan, North Sumatera (Indonesia). The industry was established in 1974 when the State Owned Electicity Corporation decided to use wooden power poles for their distribution network in North Sumatera province. However, the use of wooden power poles was discontinued in 1981, so as the preservation industry was severely affected. Some notes on the results of the full cell process, particularly on the percentage of over- and under-charged treatment, is also described in this paper.
N Supriana, A Murad

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